• Title/Summary/Keyword: Mass Measurement

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Isotope Measurement of Uranium at Ultratrace Levels Using Multicollector Inductively Coupled Plasma Mass Spectrometry

  • Oh, Seong-Y.;Lee, Seon-A.;Park, Jong-Ho;Lee, Myung-Ho;Song, Kyu-Seok
    • Mass Spectrometry Letters
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    • v.3 no.2
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    • pp.54-57
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    • 2012
  • Mass spectrometric analysis was carried out using multicollector inductively coupled plasma mass spectrometry (MC-ICP-MS) for the precise and accurate determination of the isotope ratios of ultratrace levels of uranium dissolved in 3% $HNO_3$. We used the certified reference material (CRM) 112-A at a trace level of 100 pg/mL for the uranium isotopic measurement. Multiple collectors were utilized for the simultaneous measurement of uranium isotopes to reduce the signal uncertainty due to variations in the ion beam intensity over time. Mass bias correction was applied to the measured U isotopes to improve the precision and accuracy. Furthermore, elemental standard solution with certified values of platinum, iridium, gold, and thallium dissolved in 3% $HNO_3$ were analyzed to investigate the formation rates of the polyatomic ions of $Ir^{40}$ $Ar^+$, $Pt^{40}$ $Ar^+$, $Tl^{40}$ $Ar^+$, $Au^{40}$ $Ar^+$ for the concentration range of 50-400 pg/mL. Those polyatomic ions have mass-to-charge ratios in the 230-245 m/z region that it would contribute to the increase of background intensity of uranium, thorium, plutonium, and americium isotopes. The effect of the polyatomic ion interference on uranium isotope measurement has been estimated.

A Study on Measurement Uncertainty of CMM used for Inspection of Precision Machined parts. (정밀가공 부품 검사에 사용되는 삼차원측정기의 측정불확도 연구)

  • 이갑조;오상록;김종관
    • Proceedings of the Korean Society of Machine Tool Engineers Conference
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    • 2004.10a
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    • pp.3-9
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    • 2004
  • The machining parts must be produced within the specification of drawing and those will be able to meet function and efficiency. At that time. it is necessary not only precision machine or machining technique but also the measurement technique is very important. So. the improvement of precise measurement technique is to be joined together at once with improvement of product technique. Finally. he quality and value of the parts are decided by precision measurement. This paper aims to study on he measurement uncertainty when the machined parts are inspected with 3-dimensional coordinate measuring machine. The objectives are to remove an error of measurement and to improve quality and productivity of the mass products.

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Development of magnetic field measurement system for AMS cyclotron

  • Ho Namgoong;Hyojeong Choi;Mitra Ghergherehchi;Donghyup Ha;Mustafa Mumyapan;Jong-Seo Chai;Jongchul Lee;Hoseung Song
    • Nuclear Engineering and Technology
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    • v.55 no.8
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    • pp.3114-3120
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    • 2023
  • A high-accuracy magnetic field measurement device based on a cyclotron is being developed for accelerator mass spectrometry (AMS). In this study, a magnetic field measurement device consisting of a Hall probe sensor, piezo-motor, and step motor was developed to measure the magnetic field of the AMS cyclotron magnet. The Hall probe sensor was calibrated to achieve positional accuracy by using polar coordinates. The measurement results between the ratchet gear and piezo-motor, which are the instruments used for driving the measurement device, were analyzed. The measurement result of the device with a piezo-motor exhibits a difference of 5 Gauss (0.04%) as compared with the simulation result.

Continuous Viscosity Measurement of Non-Newtonian Fluids over a Range of Shear Rates Using a Mass-Detecting Capillary Viscometer

  • Sehyun Shin;Keum, Do-Young
    • Journal of Mechanical Science and Technology
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    • v.16 no.2
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    • pp.255-261
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    • 2002
  • A newly designed mass-detecting capillary viscometer uses a novel concept to continuously measure non-Newtonian fluids viscosity over a range of shear rates. A single measurement of liquid-mass variation with time replaces the now rate and pressure drop measurements that are usually required by capillary tube viscometers. Using a load cell and a capillary, we measured change in the mass flow rate through a capillary tube with respect to the time, m(t), from which viscosity and shear rate were mathematically calculated. For aqueous polymer solutions, excellent agreement was found between the results from the mass-detecting capillary viscometer and those from a commercially available rotating viscometer. This new method overcomes the drawbacks of conventional capillary viscometers meassuring non-Newtonian fluid viscosity. First, the mass-detecting capillary viscometer can accurately and consistently measure non -Newtonian viscosity over a wide range of shear rate extending as low as 1 s$\^$-1/. Second, this design provides simplicity (i. e., ease of operation, no moving parts), and low cost.

A Cumulative Injected Fuel Mass Measurement Under a Vehicle Driven Condition using Loadcells (차량주행 모사 조건에서 로드셀을 이용한 인젝터 누적 연료 분사량 측정)

  • Cho, Seung Keun;Lee, Choong Hoon
    • Journal of ILASS-Korea
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    • v.21 no.1
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    • pp.1-6
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    • 2016
  • A gasoline injector rig which can measure cumulative injected fuel mass under a vehicle driving condition was developed. The measurement system consists of an engine control unit (ECU), data acquisition (DAQ) and injected fuel collection system using loadcells. By supplying reconstructed sensor signals which simulate the real vehicle's sensor signals to the ECU, the ECU drives injectors as if they were driven in the vehicle. The vehicle's performance was computer simulated by using $GT-Suite^{(R)}$ software based on both engine part load performance and automatic transmission shift map. Throttle valve position, engine and vehicle speed, air mass flow rate et al. were computer simulated. The used vehicle driving pattern for the simulation was FTP-75 mode. For reconstructing the real vehicle sensor signals which are correspondent to the $GT-Suite^{(R)}$ simulated vehicle's performance, the DAQ systems were used. The injected fuel was collected with mess cylinders. The collected fuel mass in the mess cylinder with elapsed time after starting FTP-75 driving mode was measured using loadcells. The developed method shows highly improved performance in fast timing and accuracy of the cumulative injected fuel mass measurement under the vehicle driven condition.

Improvement of Pesticide Sorption Measurement Method for Soils with Low Sorption (흡착력(吸着力)이 낮은 토양(土壤)에서의 농약흡착(農藥吸着) 측정법(測定法) 개발(開發))

  • Kim, Sun-Kwan;Green, Richard E.
    • Korean Journal of Soil Science and Fertilizer
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    • v.24 no.2
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    • pp.124-129
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    • 1991
  • A mass balance method which measures directly both the sorbed pesticide and equilibrium solution concentration was compared with the batch method in a hypothetical experiment to determine the precision of sorption measurement. The mass balance method was shown to improve precision of sorption measurement. The two methods were also tested experimentally on the Wahiawa soil, 0-20, 40-60 and 100-120 cm, and Salinas soil, 0-15 and 115-130 cm. The mass balance method greatly improved precision of sorption measurement on the deep Wahiawa subsoil having the lowest sorption. The coefficient of variation (CV) for $K_d$ measurement was 20.3% for the batch method and 8.4% for the mass balance method. For other soil samples tested, precision of the batch method was relatively high but was still improved by the mass balance method.

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Field measurement-based wind-induced response analysis of multi-tower building with tuned mass damper

  • Chen, Xin;Zhang, Zhiqiang;Li, Aiqun;Hu, Liang;Liu, Xianming;Fan, Zhong;Sun, Peng
    • Wind and Structures
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    • v.32 no.2
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    • pp.143-159
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    • 2021
  • The 246.8-m-tall Beijing Olympic Tower (BOT) is a new landmark in Beijing City, China. Its unique architectural style with five sub-towers and a large tower crown gives rise to complex dynamic characteristics. Thus, it is wind-sensitive, and a double-stage pendulum tuned mass damper (DPTMD) has been installed for vibration mitigation. In this study, a finite-element analysis of the wind-induced responses of the tower based on full-scale measurement results was performed. First, the structure of the BOT and the full-scale measurement are introduced. According to the measured dynamic characteristics of the BOT, such as the natural frequencies, modal shapes, and damping ratios, an accurate finite-element model (FEM) was established and updated. On the basis of wind measurements, as well as wind-tunnel test results, the wind load on the model was calculated. Then, the wind-induced responses of the BOT with the DPTMD were obtained and compared with the measured responses to assess the numerical wind-induced response analysis method. Finally, the wind-induced serviceability of the BOT was evaluated according to the field measurement results for the wind-induced response and was found to be satisfactory for human comfort.

REVIEW OF GROUNDWATER CONTAMINANT MASS FLUX MEASUREMENT

  • Goltz, Mark N.;Kim, Seh-Jong;Yoon, Hyouk;Park, Jun-Boum
    • Environmental Engineering Research
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    • v.12 no.4
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    • pp.176-193
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    • 2007
  • The ability to measure groundwater contaminant flux is increasingly being recognized as crucial in order to prioritize contaminated site cleanups, estimate the efficiency of remediation technologies, measure rates of natural attenuation, and apply proper source terms to model groundwater contaminant transport. Recently, a number of methods have been developed and subsequently applied to measure contaminant mass flux in groundwater in the field. Flux measurement methods can be categorized as either point methods or integral methods. As the name suggests, point methods measure flux at a specific point or points in the subsurface. To increase confidence in the accuracy of the measurement, it is necessary to increase the number of points (and therefore, the cost) of the sampling network. Integral methods avoid this disadvantage by using pumping wells to interrogate large volumes of the subsurface. Unfortunately, integral methods are expensive because they require that large volumes of contaminated water be extracted and managed. Recent work has investigated the development of an integral method that does not require extraction of contaminated water from the subsurface. We begin with a review of the significance and importance of measuring groundwater contaminant mass flux. We then review groundwater contaminant flux measurement methods that are either currently in use or under development. Finally, we conclude with a qualitative comparison of the various flux measurement methods.

Experimental Approach to Equalizing the Orifice Method with the Throughput One for the Measurement of TMP Pumping Speed

  • Lim, J.Y.;Kang, S.B.;Shin, J.H.;Koh, D.Y.;Cheung, W.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.18-18
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    • 2010
  • Methods of the characteristics evaluation of turbo-molecular pumps (TMP) are well-defined in the international measurement standards such as ISO, PNEUROP, DIN, JIS, and AVS. The Vacuum Center in the Korea Research Institute of Standards and Science has recently designed, constructed, and established the integrated characteristics evaluation system of TMPs based on the international documents by continuously pursuing and acquiring the reliable international credibility through measurement perfection. The measurement of TMP pumping speed is normally performed with the throughput and orifice methods dependent on the mass flow regions. However, in the UHV range of the molecular flow region, the high uncertainties of the gauges, mass flow rates, and conductance are too critical to precisely accumulate reliable data. With UHV gauges of uncertainties less than 15% and a calculated conductance of the orifice, about 35% of pumping speed uncertainties are experimentally derived in the pressure range of less than $10^{-6}$ mbar. In order to solve the uncertainty problems of pumping speeds in the UHV range, we introduced an SRG with 1% accuracy and a constant volume flow meter (CVFM) to measure the finite mass flow rates down to $10^{-3}$ mbar-L/s with 3% uncertainty for the throughput method. In this way we have performed the measurement of pumping speed down to less than $10^{-6}$ mbar with an uncertainty of 6% for a 1000 L/s TMP. In this article we suggest that the CVFM has an ability to measure the conductance of the orifice experimentally with flowing the known mass through the orifice chambers, so that we may overcome the discontinuity problem encountering during introducing two measurement methods in one pumping speed evaluation sequence.

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Measurement Method of HDD Absolute Unbalance Magnitude and Position by measuring the Mobility (모빌리티 측정을 통한 하드디스크의 Unbalance 검출 및 보정방법)

  • Choe Hyeon;Kim In Ung;Lee Jae Won;Jeong Yong Gu;Choe Jeong Heon
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.11a
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    • pp.340.1-340
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    • 2002
  • The unbalance exciting force induced by HDD of lately getting higher speed is directly influenced by the rotational speed and the mechanical assembly allowance between disk and spindle motor, and which gives rise to the structure borne noise of the personal computer. The absolute unbalance mass of HDD needs to be measured and adjusted by the counter mass to control the unbalance exciting force effectively in the stage of assembling the disk and spindle motor. This study introduces the measurement methods of the magnitude of the absolute unbalance mass and the position of HDD by 2 accelerometers. The absolute unbalance mass can be obtained by the acceleration responses and the mobility of the mechanical part, while the position of the unbalance mass can e obtained by the rotation acceleration orbit.

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