• 열처리공학회지
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• 제16권4호
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• pp.211-215
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• 2003

In this work, a new way of measuring the volume fraction of e martensite in Fe-based alloys has been proposed. Since the specific volume of ${\varepsilon}$ martensite, depending on alloy composition, is smaller than that of austenite i.e ${\gamma}$ phase, volume expansion takes place during ${\varepsilon}{\rightarrow}{\gamma}$ reverse transformation. As the amount of the volume expansion is proportional to the product of specific volume difference times the volume fraction of ${\varepsilon}$ martensite, the volume fraction of ${\varepsilon}$ martensite can be calculated by measuring the volume expansion and the specific volume difference. Such a relationship was confirmed in Fe-21Mn and Fe-32Mn-6Si alloys which undergo ${\gamma}{\rightarrow}{\varepsilon}$ martensitic transformation on cooling and by cold rolling, respectively. It was also found that the former has isotropic ${\varepsilon}$ martensite while the latter has anisotropic ${\varepsilon}$ martensite.

• 대한기계학회논문집
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• 제10권3호
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• pp.316-325
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• 1986

본 연구에서는 이상배합조직강에 있어서 피로균열진전거동의 미시조직 의존 성을 밟히기 위하여 제이상 마르텐사이트가 모상 페라이트를 둘러싼 마르텐사이트페라 이트 복합조직강을 준비하고 미시조직이 각각 다른 4종류의 시험편에 대하여 피로시험 을 실시한후 이에 의해 얻어진 피로균열진전속도를 균열휨과 균열닫힘을 통하여 검토 하였다.

• 열처리공학회지
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• 제28권4호
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• pp.200-205
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• 2015

Effects of austenite on the uniform corrosion in the solution of $1\;N\;H_2SO_4$ were investigated through the electrochemical polarization test. Two phases structures of martensite and austenite were obtained by annealing treatment at the range of $500^{\circ}C{\sim}700^{\circ}C$ for 10min. in 70% cold-rolled 202 stainless steel. Volume fraction of reversed austenite increased rapidly with an increase of annealing temperature. Uniform Corrosion was occur mainly on martensite phase in 202 austenitic stainless steel with two phase of austenite and martensite. Corrosion current density increased with an increase of volume fraction of austenite, therefore uniform corrosion was affected by volume fraction of austenite

• 한국재료학회지
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• 제25권1호
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• pp.9-15
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• 2015

The effect of retained and reversed austenite on the damping capacity in high manganese stainless steel with two phases of martensite and austenite was studied. The two phase structure of martensite and retained austenite was obtained by deformation for various degrees of deformation, and a two phase structure of martensite and reverse austenite was obtained by reverse annealing treatment for various temperatures after 70 % cold rolling. With the increase in the degree of deformation, the retained austenite and damping capacity rapidly decreased, with an increase in the reverse annealing temperature, the reversed austenite and damping capacity rapidly increased. With the volume fraction of the retained and reverse austenite, the damping capacity increased rapidly. At same volume of retained and reversed austenite, the damping capacity of the reversed austenite was higher than the retained austenite. Thus, the damping capacity was affected greatly by the reversed austenite.

• 열처리공학회지
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• 제24권1호
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• pp.23-30
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• 2011

This study was carried out to investigate the effect of aging treatment on the mechanical properties and damping capacity of 12Cr heat resistant steel with ferrite phase. While hardness values in ferrite phase was not changed, that in martensite phase was dramatically dropped in early stage of aging treatment and then gradually decreased with increase of aging time. As aging treatment was carried out, the precipitation was not detected in ferrite phase, while carbides were precipitated in martensite phase. With increasing the aging time, tensile strength eventually decreased while impact toughness increased rapidly in the early stage of aging and then gradually increased. Besides, it was confirmed that damping capacity was not changed in the early stage of aging and then gradually increased with increase of aging time.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2008년도 추계학술대회 논문집
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• pp.203-206
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• 2008

Transformation of austenite to martensite during cold rolling has been widely used to strengthen metastable austenitic stainless steel grades. Aging treatment of cold worked metastable austenitic stainless steels, including ${\alpha}'$-martensite phase, results in the further increase of strength, when aging is performed in $200^{\circ}C$ to $450^{\circ}C$ temperature range. The purpose of the present study was to evaluate the effect of time and temperature on the stress-strain behavior of cold worked austenitic stainless steels. The amount of ${\alpha}'$-martensite during cold working and aging was examined by ferrite scope and X-ray diffraction (XRD). During aging at $450^{\circ}C$ for 1hr, tensile strength dramatically increased by 150MPa. Deformed metastable austenitic steels containing the "body-centered" ${\alpha}'$-martensite are strengthened by the diffusion of interstitial solute atoms during aging at low temperature.

• 한국주조공학회지
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• 제13권5호
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• pp.432-440
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• 1993

Ductile cast iron has a good ductility and toughness than those of gray cast iron, because the shape of graphite is spheroidal. Also, it has been reported that, additional strengthening and toughening of the ductile cast iron can be obtainded from the proper combination of matrix structures by the heat treatment and addition of alloying elements. In this study the effect of special heat treatment and addition of alloying elements(Ni, Mo) on the multi-phase(ferrite-bainite-martensite) structures, strength and toughness of ductile cast iron were studied systematically. In water quenching from $770^{\circ}C$, the martensite volume(%) increased, but the ferrite volume(%) decreased with increment of Ni content. In as cast, pearlite volume(%) and hardness increased with increment of Mo and Ni contents. And with the increment of the destabilization austempering holding time, the bainite volume(%) increased but the martensite volume(%) decreased. As destabilization austempering holding time is same, bainite volume(%) decreased, martensite increased with the increment of Ni and Mo contents. The hardness and tensile strength decreased, but impact energy increased with the decrease of Ni and Mo contents, and increment of holding time of destabilization austempering treatment.

• Advances in materials Research
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• 제4권1호
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• pp.1-12
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• 2015

Low carbon steel of composition 0.05C - 0.18 Mn - 0.012 Si is intercritically annealed at temperatures $750^{\circ}C$, $775^{\circ}C$ and $800^{\circ}C$. The equilibrated alloys of different amounts of austenite with varying carbon contents are quenched in iced water. The same alloys are subcritically annealed at $675^{\circ}C$ and $700^{\circ}C$ for varying periods of times; the subcritically annealed alloy samples are quenched in iced water. Optical, scanning electron and transmission electron microscopy are carried out for all the samples. The dislocation structure, its distribution and density present in the above prepared duplex ferrite martensite steels are studied. The martensites are found to be highly dislocated due to lattice invariant deformation. At the same time ferrite adjoining the martensite areas also exhibits quite a high dislocation density. The high dislocation density is favorable for strain ageing and hence bakes hardenability. EDS analyses were carried out for both martensite and ferrite phases; it is found that the degree of supersaturation in ferrite together with carbon content in martensite varies with the process parameters. The microhardness test results show that the hardness values of different phases differ appreciably with process parameters. The microstructures and the corresponding microanalyses reveal that differently processed steels contain phases of varying compositions and different distribution.

• 동력기계공학회지
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• 제5권1호
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• pp.97-103
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• 2001

The present study was investigated changes of precipitation behaviour of laves phase in ferrite single phase and ferrite-martensite dual phase and the mechanical properties of 10%Cr ferritic alloys. In the ferrite phase, laves phase was mainly precipitated, whereas in the martensite phase, carbide was preferentially formed during the initial stage of aging and with increasing aging time. Laves phase and carbide were simultaneously precipitated by precipitation of laves phase at around carbide. Strength and toughness were lowered by the disk-type precipitator in the initial stage of aging and toughness was recovered with increasing of aging time and then, decreasing by precipitation of laves phase.

• 동력기계공학회지
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• 제11권1호
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• pp.115-120
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• 2007

The effect of grain size on the damping capacity of Fe-26Mn-2Al alloy studied in this paper has been investigated after changing the microstructure by cold rolling and changing grain size. Micro structures in Fe-26Mn-2Al at room temperature consist of a large quantity of austenite and a small quantity of ${\varepsilon}\;and\;{\alpha}'$ martensite. And ${\varepsilon}\;and\;{\alpha}'$ martensite was increased by increasing the degree of cold rolling. The content of deformation induced martensite was increased with increasing the degree of cold rolling. Damping capacity was linearly increased with increasing ${\varepsilon}$ martensite content, which suggests that stacking faults and ${\varepsilon}$ martensite variant boundaries are the principle damping sources. With increasing the grain size in Fe-26Mn-2Al alloy, the damping capacity was increased due to increasing the volume fraction of ${\varepsilon}$ martensite by decrement in stability of austenite phase. With decreasing the grain size, the content of deformation induced martensite was decreased and the damping capacity was decreased.