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Fabrication of field emitters using a filtration-taping-transfer method

  • Song, Ye-Nan;Shin, Dong-Hoon;Sun, Yuning;Shin, Ji-Hong;Lee, Cheol-Jin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.466-466
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    • 2011
  • There have been several methods to fabricate carbon nanotube (CNT) emitters, which include as-grown, spraying, screen-printing, electrophoresis and bonding methods. Unfortunately, these techniques generally suffer from two main problems. One is a weak mechanical adhesion between CNTs and the cathode. The as-grown, spraying and electrophoresis methods show a weak mechanical adhesion between CNTs and the cathodes, which induces CNT emitters pulled out under a high electric field. The other is a severe degradation of the CNT tip due to organic binders used in the fabrication process. The screen-printing method which is widely used to fabricate CNT emitters generally shows a critical degradation of CNT emitters caused by the organic binder. Such kinds of problems induce a short lifetime of the CNT field emitters which may limit their practical applications. Therefore, a robust CNT emitter which has the strong mechanical adhesion and no degradation is still a great challenge. Here, we introduce a simple and effective technique for fabrication of CNT field emitter, namely filtration-taping-transfer method. The CNT emitters fabricated by the filtration-taping-transfer method show the low turn-on electric fields, the high emission current, good uniformity and good stability. The enhanced emission performance of the CNT emitters is mainly attributed to high emission sites on the emitter area, and to good ohmic contact and strong mechanical adhesion between the emitters and cathodes. The CNT emitters using a simple and effective fabrication method can be applied for various field emission applications such as field emission displays, lamps, e-beam sources, and x-ray sources. The detail fabrication process will be covered at the poster.

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Influence of Sodium Concentrations on Growth, Physiological Disorder Symptoms, and Bed Soil Chemical Properties of 2-Year-Old Ginseng (나트륨 농도가 2년생 인삼의 생육, 생리장해 및 상토의 화학적 특성에 미치는 영향)

  • Yu, Jin;Suh, Su Jeoung;Jang, In Bae;Jang, In Bok;Moon, Ji Won;Kwon, Ki Beam;Lee, Sung Woo
    • Korean Journal of Medicinal Crop Science
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    • v.26 no.3
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    • pp.240-247
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    • 2018
  • Background: Saline soil has negative effects on the growth of most crops. Sodium is the main element that causes salt accumulation in soil. Organic materials such as cow and poultry manure, are frequently used during the preparation stage, which causes an increase in the rate of salt accumulation in the soil. Methods and Results: To investigate the influences of sodium on ginseng, $NaH_2PO_4$, $Na_2SO_4$, and NaCl were used to adjust the sodium concentrations at 0, 12.5, 25, 50, 75 and 100 mM in nutrient solution. In a 2-year-old ginseng, toxic symptoms appeared when the sodium treatment exceeded 50 mM. The sodium concentration in the leaves was 3.33%, which is more than twice as high as that of the control treated at 50 mM. As the sodium concentration increased, the root weight significantly decreased. In the 100 mM treatment, the weight decreased by 28% when compared to that of the control. The Amount of ginsenoside significantly increased with an increase in sodium concentrations. Conclusions: These results suggest that the growth of 2-year-old ginseng is negatively affected when sodium exceeds 50 mM. This result can be used for a as basis in diagnosing the physiological disorders of ginseng.

Analysis of the Change in Microstructures of Nano Copper Powders During the Hydrogen Reduction using X-ray Diffraction Patterns and Transmission Electron Microscope, and the Mechanical Property of Compacted Powders (X-선 회절 패턴 측정과 투과 전자 현미경을 이용한 구리 나노분말의 수소 환원 처리 시 발생하는 미세조직 변화 및 치밀화 시편의 물성 분석)

  • Ahn, Dong-Hyun;Lee, Dong Jun;Kim, Wooyeol;Park, Lee Ju;Kim, Hyoung Seop
    • Journal of Powder Materials
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    • v.21 no.3
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    • pp.207-214
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    • 2014
  • In this study, nano-scale copper powders were reduction treated in a hydrogen atmosphere at the relatively high temperature of $350^{\circ}C$ in order to eliminate surface oxide layers, which are the main obstacles for fabricating a nano/ultrafine grained bulk parts from the nano-scale powders. The changes in composition and microstructure before and after the hydrogen reduction treatment were evaluated by analyzing X-ray diffraction (XRD) line profile patterns using the convolutional multiple whole profile (CMWP) procedure. In order to confirm the result from the XRD line profile analysis, transmitted electron microscope observations were performed on the specimen of the hydrogen reduction treated powders fabricated using a focused ion beam process. A quasi-statically compacted specimen from the nano-scale powders was produced and Vickers micro-hardness was measured to verify the potential of the powders as the basis for a bulk nano/ultrafine grained material. Although the bonding between particles and the growth in size of the particles occurred, crystallites retained their nano-scale size evaluated using the XRD results. The hardness results demonstrate the usefulness of the powders for a nano/ultrafine grained material, once a good consolidation of powders is achieved.

Species Identification and Tree-Ring Analysis of Wooden Elements in Daewoong-jeon of Hwagye-temple, Seoul, Korea (서울 화계사 대웅전 목부재의 수종 및 연륜연대 분석)

  • Lee, Kwang Hee;Park, Chang Hyun;Kim, Soo Chul
    • Journal of Conservation Science
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    • v.36 no.5
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    • pp.326-332
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    • 2020
  • The this study's objective was to conduct species identification and tree-ring dating for the wood elements of Daewoong-jeon(main temple), Hwagye-temple, Seoul, Korea. Most of the wood elements were made from Pinus spp.(hard pine). However, one large beam was constructed from Abies spp.. For the tree-ring dating, cores were taken from the elements using a drill, and ring-width plots of individual samples were produced with the TSAP software program. The tree-ring dating results showed that, the date of the outermost ring of most elements (20 elements), including beams and pillars, were from AD 1839 to 1870. Among them, five elements had bark, and felling dates were AD 1868 and 1869. These dates confirmed the historical records that Daewoongjeon was rebuilt in AD 1870 from the records of hidden materials(Bokjangmul) in Jongdori by the survey 2012.

Correlation analysis of gingival recession after orthodontic treatment in the anterior region: an evaluation of soft and hard tissues

  • Lee, Jong-Bin;Baek, Soo-Jin;Kim, Minji;Pang, Eun-Kyoung
    • Journal of Periodontal and Implant Science
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    • v.50 no.3
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    • pp.146-158
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    • 2020
  • Purpose: The aim of this study was to investigate and identify the main causes of periodontal tissue change associated with labial gingival recession by examining the anterior region of patients who underwent orthodontic treatment. Methods: In total, 45 patients who had undergone orthodontic treatment from January 2010 to December 2015 were included. Before and after the orthodontic treatment, sectioned images from 3-dimensional digital model scanning and cone-beam computed tomography images in the same region were superimposed to measure periodontal parameters. The initial labial gingival thickness (IGT) and the initial labial alveolar bone thickness (IBT) were measured at 4 mm below the cementoenamel junction (CEJ), and the change of the labial gingival margin was defined as the change of the distance from the CEJ to the gingival margin. Additionally, the jaw, tooth position, tooth inclination, tooth rotation, and history of orthognathic surgery were investigated to determine the various factors that could have affected anterior periodontal tissue changes. Results: The mean IGT and IBT were 0.77±0.29 mm and 0.77±0.32 mm, respectively. The mean gingival recession was 0.14±0.57 mm. Tooth inclination had a significant association with gingival recession, and as tooth inclination increased labially, gingival recession increased by approximately 0.2 mm per 1°. Conclusions: In conclusion, the IGT, IBT, tooth position, tooth rotation, and history of orthognathic surgery did not affect labial gingival recession. However, tooth inclination showed a significant association with labial gingival recession of the anterior teeth after orthodontic treatment.

Development of medium resolution cross-dispersed silicon grisms in the Near Infrared ; Direct Silicon wafer bonding technique

  • Jeong, Hyeon-Ju;Wang, Wei-Song;Gully-Santiago, Michael;Deen, Casey;Pak, Soo-Jong;Jaffe, Daniel T.
    • The Bulletin of The Korean Astronomical Society
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    • v.36 no.2
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    • pp.125.2-125.2
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    • 2011
  • We are developing medium resolution cross-dispersed silicon grisms in the near IR region ($1.45{\sim}5.2{\mu}m$). The grisms will be installed in MIMIR, a multifunction instrument at the Lowel Observatory, USA. The two devices are designed to cover H and K band and L and M band simultaneously. Our goal is to make grism with R=3000 at 1.2 arcsec slit. The Silicon has high refractive index (n=3.4 at $1.5{\mu}m$) which enhances the resolving power by up to 5 times when compared to conventional material such as BK-7 (n=1.5 at 1.5 ${\mu}m$). The bonded grisms will be installed in a filter wheel for the uses switch from spectroscopic mode to imaging mode easily. Our device is compact and light weighted while it provides a decent resolving power. We produce monolithic grisms using e-beam lithography at the NASA JPL and chemically etching the grooves on the silicon prisms. Moreover, the main-disperser and cross-disperser will be contacted together by direct Si-Si bonding technique and eventually turn into one piece. The bonded pair offers more stability in terms of the layout of the spectrum and removes the Fresnel loss at the intersection of two grisms. We report on the proper wafer bonding steps through this research, and inspected the bonding quality thermally, optically and mechanically.

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SAR Data Correction Based on Calibrated-Scatterometer Measurements (보정된 Scatterometer의 측정데이터를 사용한 SAR 데이터 교정)

  • 정구준;홍진영;오이석
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.15 no.2
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    • pp.121-126
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    • 2004
  • This paper presents an SAR-data calibration technique using a well-calibrated scatterometer. At first a fully-polarimetric antenna pattern(magnitude and phase) of the antenna main-beam using a conducting sphere was measured. Then, this data were used to calibrate polarimetrically an auto-mounted network analyzer-based scatterometer system. This scatterometer system can be used to measure the accurate Mueller matrices of earth surfaces such as grass fields, rice fields and bare soil surfaces; i.e., the phase-difference parameters can be obtained as well as the radar scattering coefficients. If a polarimetrically calibrated scatterometer is operated at the same time with the SAR system, the scatterometer data can be used to correct the SAR data, especially the phase-difference parameters. It was found that the correction effect is remarkable for the degree of correlation ${\alpha}$, which is one of the phase-difference parameter, while the correction effect is negligible for the magnitude parameters(backscattering coefficients).

Inverse model for pullout determination of steel fibers

  • Kozar, Ivica;Malic, Neira Toric;Rukavina, Tea
    • Coupled systems mechanics
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    • v.7 no.2
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    • pp.197-209
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    • 2018
  • Fiber-reinforced concrete (FRC) is a material with increasing application in civil engineering. Here it is assumed that the material consists of a great number of rather small fibers embedded into the concrete matrix. It would be advantageous to predict the mechanical properties of FRC using nondestructive testing; unfortunately, many testing methods for concrete are not applicable to FRC. In addition, design methods for FRC are either inaccurate or complicated. In three-point bending tests of FRC prisms, it has been observed that fiber reinforcement does not break but simply pulls out during specimen failure. Following that observation, this work is based on an assumption that the main components of a simple and rather accurate FRC model are mechanical properties of the concrete matrix and fiber pullout force. Properties of the concrete matrix could be determined from measurements on samples taken during concrete production, and fiber pullout force could be measured on samples with individual fibers embedded into concrete. However, there is no clear relationship between measurements on individual samples of concrete matrix with a single fiber and properties of the produced FRC. This work presents an inverse model for FRC that establishes a relation between parameters measured on individual material samples and properties of a structure made of the composite material. However, a deterministic relationship is clearly not possible since only a single beam specimen of 60 cm could easily contain over 100000 fibers. Our inverse model assumes that the probability density function of individual fiber properties is known, and that the global sample load-displacement curve is obtained from the experiment. Thus, each fiber is stochastically characterized and accordingly parameterized. A relationship between fiber parameters and global load-displacement response, the so-called forward model, is established. From the forward model, based on Levenberg-Marquardt procedure, the inverse model is formulated and successfully applied.

Reliability analysis of reinforced concrete haunched beams shear capacity based on stochastic nonlinear FE analysis

  • Albegmprli, Hasan M.;Cevik, Abdulkadir;Gulsan, M. Eren;Kurtoglu, Ahmet Emin
    • Computers and Concrete
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    • v.15 no.2
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    • pp.259-277
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    • 2015
  • The lack of experimental studies on the mechanical behavior of reinforced concrete (RC) haunched beams leads to difficulties in statistical and reliability analyses. This study performs stochastic and reliability analyses of the ultimate shear capacity of RC haunched beams based on nonlinear finite element analysis. The main aim of this study is to investigate the influence of uncertainty in material properties and geometry parameters on the mechanical performance and shear capacity of RC haunched beams. Firstly, 65 experimentally tested RC haunched beams and prismatic beams are analyzed via deterministic nonlinear finite element method by a special program (ATENA) to verify the efficiency of utilized numerical models, the shear capacity and the crack pattern. The accuracy of nonlinear finite element analyses is verified by comparing the results of nonlinear finite element and experiments and both results are found to be in a good agreement. Afterwards, stochastic analyses are performed for each beam where the RC material properties and geometry parameters are assigned to take probabilistic values using an advanced simulating procedure. As a result of stochastic analysis, statistical parameters are determined. The statistical parameters are obtained for resistance bias factor and the coefficient of variation which were found to be equal to 1.053 and 0.137 respectively. Finally, reliability analyses are accomplished using the limit state functions of ACI-318 and ASCE-7 depending on the calculated statistical parameters. The results show that the RC haunched beams have higher sensitivity and riskiness than the RC prismatic beams.

DESIGN OPTIMIZATION OF RADIATION SHIELDING STRUCTURE FOR LEAD SLOWING-DOWN SPECTROMETER SYSTEM

  • KIM, JEONG DONG;AHN, SANGJOON;LEE, YONG DEOK;PARK, CHANG JE
    • Nuclear Engineering and Technology
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    • v.47 no.3
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    • pp.380-387
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    • 2015
  • A lead slowing-down spectrometer (LSDS) system is a promising nondestructive assay technique that enables a quantitative measurement of the isotopic contents of major fissile isotopes in spent nuclear fuel and its pyroprocessing counterparts, such as $^{235}U$, $^{239}Pu$, $^{241}Pu$, and, potentially, minor actinides. The LSDS system currently under development at the Korea Atomic Energy Research Institute (Daejeon, Korea) is planned to utilize a high-flux ($>10^{12}n/cm^2{\cdot}s$) neutron source comprised of a high-energy (30 MeV)/high-current (~2 A) electron beam and a heavy metal target, which results in a very intense and complex radiation field for the facility, thus demanding structural shielding to guarantee the safety. Optimization of the structural shielding design was conducted using MCNPX for neutron dose rate evaluation of several representative hypothetical designs. In order to satisfy the construction cost and neutron attenuation capability of the facility, while simultaneously achieving the aimed dose rate limit (< $0.06{\mu}Sv/h$), a few shielding materials [high-density polyethylene (HDPE)eBorax, $B_4C$, and $Li_2CO_3$] were considered for the main neutron absorber layer, which is encapsulated within the double-sided concrete wall. The MCNP simulation indicated that HDPE-Borax is the most efficient among the aforementioned candidate materials, and the combined thickness of the shielding layers should exceed 100 cm to satisfy the dose limit on the outside surface of the shielding wall of the facility when limiting the thickness of the HDPE-Borax intermediate layer to below 5 cm. However, the shielding wall must include the instrumentation and installation holes for the LSDS system. The radiation leakage through the holes was substantially mitigated by adopting a zigzag-shape with concrete covers on both sides. The suggested optimized design of the shielding structure satisfies the dose rate limit and can be used for the construction of a facility in the near future.