• 제목/요약/키워드: Magnetic powders

검색결과 347건 처리시간 0.029초

Magnetism of Nanocomposite Quartz Powder by use of MCR Method

  • Soh, Deawha;Lim, Byoungjae;Soh, Hyunjun;Mofa, N.N.;Ketegenov, T.A.;Mansurov, Z.A.
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2004년도 SMICS 2004 International Symposium on Maritime and Communication Sciences
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    • pp.113-116
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    • 2004
  • The materials showing high structure dispersion with functional properties were developed on the quartz base and those were obtained by mechano-chemical reaction technology. Depending on the processing conditions and subsequent applications the materials produced by mechano-chemical reaction show concurrently magnetic, dielectric and electrical properties. The obtained magnetic-electrical powders classified by aggregate complex of their features as segnetomagnetics, containing a dielectric material as a carrying nucleus, particularly the quartz on that surface one or more layers of different compounds were synthesized having thickness up to 10~50 nm showing magnetic, electrical properties and others. The similarity of the structure of surface layers of quartz particles subjected to mechano-chemical processing and nano-structure cluspol (clusters in a polymer matrics) material was also confirmed by the fact that the characteristics of ferromagnetic quartz of insulating nano-composite powder were changed with time, after its preparing process was completed. The magnetic permeability of the sample was decreasing within first two months down by 15~20 %. Then, the magnetic characteristics were almost stabilized steadily and continuously. The observed changes were related with defective structure of the particles, elastic stress relief, and changes of electron density and magnetic moment in deformation zones. This process of stabilization of the investigated properties could be intensified by the thermal annealing heat treatment in short time period of the nano-composite quartz powders at the temperature ranges of 100~15$0^{\circ}C$.

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고상반응법으로 제조된 Ba2Co2Fe12O22분말의 자기적 성질과 미세구조에 미치는 금속이온몰비와 열처리 온도의 영향 (Effects of Metal Ion Mole Ratio and Calcination Temperatures on Magnetic Properties and Microstructure of Ba2Co2Fe12O22 Powders Synthesized by Solid State Reaction)

  • 조광묵;남인탁
    • 한국자기학회지
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    • 제19권6호
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    • pp.216-221
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    • 2009
  • Y-type 바리움 페라이트 $Ba_2Co_2Fe_{12}O_{22}$를 고상반응법으로 제조하고 금속이온몰비($Fe^{3+}:\;Ba^{2+}:\;Co^{2+}$)와 열처리 온도가 자기적 성 질과 미세구조에 미치는 영향에 대하여 조사하였다. 상분석과 미세구조는 각각 XRD(X-ray diffractometer)와 FESEM(field effect scanning electron microscope)을 이용하여 조사하였으며 분말의 자기적 성질은 VSM(vibrating sample magnetometer)을 이용하여 조사하였다. 금속이온몰비($Fe^{3+}:\;Ba^{2+}:\;Co^{2+}$)가 6 : 1 : 1인 조성의 분말을 $1050\;{^{\circ}C}$에서 열처리하였을 때 단일 상이 합성되었으며 8 : 1 : 1인 조성의 분말을 $1200\;{^{\circ}C}$에서 열처리하였을 때 가장 높은 포화자화값(39.1 emu/g)을 나타내었다.

고에너지 볼밀링으로 제조된 나노구조 Fe-20 wt.%Si 합금 분말의 자성 특성에 미치는 결정립 크기의 영향 (Effect of Grain Size on Nanostructured Fe-20 wt.%Si Alloy Powders Produced by High-energy ball milling)

  • 김세훈;이영중;이백희;이규환;김영도
    • 한국분말재료학회지
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    • 제12권5호
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    • pp.362-368
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    • 2005
  • The structural and magnetic properties of nanostructued Fe-20 ;wt.%Si alloy powders were investigated. Commercial Fe-20 wt.%Si alloy powders (Hoeganaes Co., USA) with 99.9% purities were used to fabricate the nanostructure Fe-Si alloy powders through a high-energy ball milling process. The alloy powders were fabricated at 400 rpm for 50 h, resulting in an average grain size of 16 nm. The nanostructured powder was characterized by fcc $Fe_{3}Si$ and hcp $Fe_{5}Si_3$ phases and exhibited a minimum coercivity of approximately 50 Oe.

Compaction and Sintering Characteristics of High Energy Ball Milled Mn-Zn Ferrite Powders

  • Lee, Hyunseung;Rhee, Hoseong;Lee, Sangsoo;Chang, Si Young
    • 한국재료학회지
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    • 제31권12호
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    • pp.677-681
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    • 2021
  • The Mn-Zn ferrite powders were prepared by high energy ball milling, then compacted and sintered at various temperatures to assess their sintering behavior and magnetic properties. The initial ferrite powders were spherical in shape with the size of approximately 70 ㎛. After 3 h of ball milling at 300 rpm, aggregated powders ~230 nm in size and composed of ~15 nm nanoparticles were formed. The milled powders had a density of ~70 % when compacted at 490 MPa for 3 min. In the samples subsequently sintered at 1,273 K ~ 1,673 K for 3 h, the MnZnFe2O4 phase was detected. The density of the sintered samples had a tendency to increase with increasing sintering temperature up to 1,473 K, which produced the highest density of 98 %. On the other hand, the sample sintered at 1,373 K had the highest micro-hardness of approximately 610 Hv, which is due to much finer grains.