• Title/Summary/Keyword: Magnetic composite materials

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Analysis Torque Characteristics and Improved Efficiency of Permanent Magnet Multi-D.O.F. Spherical Motor (영구자석형 다자유도 구형전동기의 토크특성 분석과 효율 향상에 대한 연구)

  • Lee, Ho-Joon;Kim, Yong;Jang, Ik-Sang;Park, Hyun-Jong;Kang, Dong-Woo;Won, Sung-Hong;Lee, Ju
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.61 no.1
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    • pp.57-63
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    • 2012
  • A surfaced permanent magnet spherical motor is capable of operating as three degree of freedom that used for the joints of the robot's arm, leg, and eyes. Ongoing research like new concept is essential part of motor field, it will make a great contribution in the future the overall portion of the motor, is becoming expected. The author analysis torque characteristics in spherical motor with state of rotating and positioning. And future design direction is smaller motors with equivalent or higher output. Solutions as torque and efficiency improvements are selecting the core with special processing type like powder metallurgy materials. Their special characteristic is high permeability and low eddy current losses at high speed, so improved the torque and efficiency.

A Study on Cu-Fe Multifilamentary Composites Produced by in situ Process (in situ법(法)에 의한 Cu-Fe계(系) 다섬유상(多纖維狀) 복합재료제조(複合材料製造)에 관한 연구(硏究))

  • Shur, S.J.;Park, H.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.2
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    • pp.9-18
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    • 1991
  • Among the many maunfactured processes of producing multi filamentary composites, in situ process is widely used owing tv its simplicity and easyness of mass production. In this study, the mechanical and electromagnetic properties of Cu-Fe composite materials was investigated. The tensile strength of the Cu-Fe wires increased as the Fe content and reduction ratio were increased. The Cu-30 wt%Fe composites had the best properties in terms of figure merits compared to the other Cu-Fe composites made in this study or the commercially manufactured 6/1 ACSR cables of Cu cable. The coercivity was decreased by increasing Fe content, but the squareness was increased greatly. As increasing reduction ratio, the coercivity and squareness increased up to the maximum points, and then decreased. For example, the maximum values were obtained at $0.09mm{\phi}$ for Cu-30 wt%Fe composites and at $0.066mm{\phi}$ for Cu-45 wt%Fe composites. The magnetic property of Cu-Fe wires produced by precipitation treatment was higher than that of Cu-Fe wires produced by thermomechanical treatment. By annealing Cu-Fe wires after drawing process, the coercivity, remanence and squareness were improved.

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Preparation of PVA/Graphene Oxide/Fe3O4 Magnetic Microgels as an Effective Adsorbent for Dye Removal (폴리바이닐알코올/그래핀 옥사이드/산화철 자성 마이크로겔을 이용한 염료 제거)

  • Go, Seongmoon;Kim, Keunseong;Wi, Eunsol;Park, Rae-Su;Jung, Hong-Ryun;Yun, Changhun;Chang, Mincheol
    • Composites Research
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    • v.35 no.2
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    • pp.98-105
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    • 2022
  • In this study, polyvinyl alcohol (PVA)/graphene oxide (GO)/iron oxide (Fe3O4) magnetic microgels were prepared using a microfluidic approach and the dye adsorption capacity of the microgels was confirmed. The adsorption capacity (qe) of the gels was evaluated by varying the dye concentration, pH, and contact time with the microgels. The dyes used in this work were methylene blue (MB), crystal violet (CV), and malachite green (MG), and microgels showed the highest adsorption capacity (191.1 mg/g) in methylene blue. The microgels exhibited the highest adsorption capacity in the dye aqueous solution at pH 10 due to the presence of atomic nitrogen ions (N+) on the dye molecules. The adsorption isotherm studies revealed that the Langmuir isotherm is the best fit isotherm model for the dye adsorption on the microgels, indicative of monolayer adsorption. The kinetic analysis exhibited that the pseudo-second order model fits better than the pseudo-first order model, confirming that the adsorption process is chemisorption. In addition, the magnetic microgels showed good reusability and recovery efficiency. It was confirmed that the adsorption capacity of the gels maintains more than 70% of the initial capacity after 5 times of cycle experiments.

Ex Vivo ${1}^H$ MR Spectroscopy: Normal gastric and cancer tissue (정상 위 조직과 위암 조직의 시험관 내 수소자기공명분광)

  • Cho Ji Youn;Shin Oon Jae;Choi Ki Seung;Kim Su Hyun;Eun Choong Ki;Yang Young Il;Lee Jung Hee;Mun Chi Woong
    • Journal of Gastric Cancer
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    • v.3 no.3
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    • pp.151-157
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    • 2003
  • Purpose: In this study, we attempted to ascertain the proton magnetic resonance spectroscopy (${1}^H$ MRS) peak characteristics of human gastric tissue layers and finally to use the metabolic peaks of MRS to distinguish between normal and abnormal gastric specimens. Materials and Methods: Ex-vivo ${1}^H$ MRS examinations of thirty-five gastric specimens were performed to distinguish abnormal gastric tissues invaded by carcinoma cells from normal stomach-wall tissues. High-resolution 400-MHz (9.4-T) ${1}^H$ nuclear magnetic resonance (NMR) spectra of two gastric layers, a proper muscle layer, and a composite mucosasubmucosa layer were compared with those of clinical 64- MHz (1.5-T) MR spectra. Three-dimensional spoiled gradient recalled (SPGR) images were used to determine the size and the position of a voxel for MRS data collection. Results: For normal gastric tissue layers, the metabolite peaks of 400-MHz ${1}^H$ MRS were primarily found to be as follows: lipids at 0.9 ppm and 1.3 ppm; alanine at 1.58 ppm; N-acetyl neuraminic acid (sialic acid) at 2.03 ppm; and glutathione at 2.25 ppm in common. The broad and featureless featureless spectral peaks of the 64-MHz MRS were bunched near 0.9, 1.3, and 2.0, and 2.2 ppm in human specimens without respect to layers. In a specimen (Borrmmann type III) with a tubular adenocarcinoma, the resonance peaks were measured at 1.26, 1.36 and 3.22 ppm. All the peak intensities of the spectrum of the normal gastric tissue were reduced, but for gastric tumor tissue layers, the lactate peak split into 1.26 and 1.39 ppm, and the peak intensity of choline at 3.21 ppm was increased. Conclusion: We found that decreasing lipids, an increasing lactate peak that split into two peaks, 1.26 ppm and 1.36 ppm, and an increasing choline peak at 3.22 ppm were markers of tumor invasion into the gastric tissue layers. This study implies that MR spectroscopy can be a useful diagnostic tool for gastric cancer.

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Consolidation and magnetic properties of ferromagnetic Fe-MgO powders prepared by ball milling process (볼밀링법으로 제조된 강자성 Fe-MgO 분말의 벌크화 및 자기적 특성)

  • Chung-Hyo Lee
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.34 no.4
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    • pp.125-130
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    • 2024
  • Preparation of ferromagnetic powders for the mixture of hematite and pure Mg powders by ball milling has been investigated. Also, consolidation of the ball-milled powders was performed in a spark plasma sintering machine at 800-1,000℃. It is found that a ferromagnetic Fe-MgO composite powders are obtained by ball milling of hematite and pure Mg powders before 1 hour. The magnetization and coercivity of ball-milled samples change at the results of the solid state reaction of hematite by pure Mg during ball milling. The saturation magnetization of ball-milled samples increases with increasing ball milling time and reaches to a maximum value of 93.4 emu/g after 5 hours of ball milling. Shrinkage change after sintering of ball-milled sample for 5 hours was significant above 300℃ and gradually increased with increasing temperature up to 800℃. X-ray diffraction result shows that the average grain size of Fe in Fe-MgO bulk sample sintered at 900℃ is 50 nm. It can be also seen that the coercivity of bulk sample sintered at 900℃ is still high value of 90 Oe, indicating that the grain growth of magnetic Fe phase during sintering process tend to be suppressed.

Comparison of Heating Behavior of Various Susceptor-embedded Thermoplastic Polyurethane Adhesive Films via Induction Heating (다양한 발열체가 분산된 폴리우레탄 접착 필름의 유도가열 거동 비교)

  • Kwon, Yongsung;Bae, Duckhwan;Shon, MinYoung
    • Composites Research
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    • v.30 no.3
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    • pp.181-187
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    • 2017
  • The effect of nanoscopic and microscopic Fe, $Fe_3O_4$, and Ni particles and their shapes and substrate materials on the heating behavior of thermoplastic polyurethane (TPU) adhesive films was investigated via induction heating. The heat generation tendency of $Fe_3O_4$ particles was higher than that shown by Fe and Ni particles in the TPU adhesive films. When the Fe and Ni particle size was larger than the penetration skin depth, the initial heating rate and maximum temperature increased with an increase in the particle size. This is attributed to the eddy current heat loss. The heating behavior of the TPU films with Ni particles of different shapes was examined, and different hysteresis heat losses were observed depending on the particle shape. Consequently, the flake-shaped Ni particles showed the most favorable heat generation because of the largest hysteresis loss. The substrate materials also affected the heating behavior of the TPU adhesive films in an induction heating system, and the thermal conductivity of the substrate materials was determined to be the main factor affecting the heating behavior.

Investigation of Reinforced Distribution in Fabrication Process of Metal Matrix Composites by Combined Stirring Process (복합교반법에 의한 금속복합재료의 제조공정에 따른 강화재의 분산성 검토)

  • 이동건;강충길
    • Composites Research
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    • v.14 no.5
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    • pp.1-11
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    • 2001
  • The particulates reinforced metal matrix composites(PMMC) have a number of interesting mechanical properties. including high strength and good resistance to wear at high temperature and low thermal expansion. The equipment structure to obtain the homogeneous distribution in composites are proposed for the continuous pouring of reinforcement at the desired temperature. The particulates reinforced metal matrix composites(A357/SiCp) were fabricated by the process of the combined stirring method with the various fabrication process. The combined stirring method to niform distribution of particle is consisted of two stirring force both electro-magnetic stirring generated from induction heating and mechanical stirring with graphite stirrer. PMMC billets were fabricated with the volume fractions ranged from 0% to 20% and particle sizes ranged from 14${\mu}{\textrm}{m}$ to 25${\mu}{\textrm}{m}$. It is important to cont the size of primary $\alpha$-Al solid particles because it could become the cause of the particle pushing or capture phenomena from the fact that secondary dendrite arm spacing size depends on the cooling rate during the solidification in hypoeutectic Al-Si alloy. Therefore, the effect of primary $\alpha$-Al on the reinforcement distribution in matrix alloys has been investigated. The microstructure of PMMC fabracated with various volume fractions(0%, 10%, and 20%) and particle size were observed.

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Surface Modification of Microcrystalline Cellulose (MCC) Filler for CO2 Capture (CO2 흡착 충전제 제조를 위한 microcrystalline cellulose (MCC) 입자 표면개질연구)

  • Yang, Yeokyung;Park, Seonghwan;Kim, Hanna;Hwang, Ki-Seob;Ha, KiRyong
    • Korean Chemical Engineering Research
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    • v.55 no.1
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    • pp.60-67
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    • 2017
  • In this study, we performed surface modification of biodegradable microcrystalline cellulose (MCC) to use as a filler in polyethylene (PE) composite in food packaging application. We modified MCC surface with (3-trimethoxysilylpropyl)diethylenetriamine (TPDT) silane coupling agent, which has one primary amino group and two secondary amino groups per molecule, to introduce amino groups with a carbon dioxide adsorption capability in MCC. Effects of each of the reaction conditions such as amount of TPDT introduced, swelling time, reaction temperature, and reaction time on surface modification degree of MCC were investigated by changing a variety of above reaction conditions. The amount of TPDT grafted on MCC surface and formation of chemical bonds were confirmed by Fourier transform infrared spectroscopy (FT-IR), elemental analysis (EA), X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TGA) and solid state $^{29}Si$ nuclear magnetic resonance (NMR) spectroscopy. We confirmed increase of grafted amount of TPDT on MCC with increasing reaction time, reaction temperature, and amount of introduced TPDT.

A poroelastic model for ultrasonic wave attenuation in partially frozen brines (부분 동결된 소금물에서의 초음파감쇠에 대한 다공성탄성 모델)

  • Matsushima, Jun;Nibe, Takao;Suzuki, Makoto;Kato, Yoshibumi;Rokugawa, Shuichi
    • Geophysics and Geophysical Exploration
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    • v.14 no.1
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    • pp.105-115
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    • 2011
  • Although there are many possible mechanisms for the intrinsic seismic attenuation in composite materials that include fluids, relative motion between solids and fluids during seismic wave propagation is one of the most important attenuation mechanisms. In our previous study, we conducted ultrasonic wave transmission measurements on an ice-brine coexisting system to examine the influence on ultrasonic waves of the unfrozen brine in the pore microstructure of ice. In order to elucidate the physical mechanism responsible for ultrasonic wave attenuation in the frequency range of 350.600 kHz, measured at different temperatures in partially frozen brines, we employed a poroelastic model based on the Biot theory to describe the propagation of ultrasonic waves through partially frozen brines. By assuming that the solid phase is ice and the liquid phase is the unfrozen brine, fluid properties measured by a pulsed nuclear magnetic resonance technique were used to calculate porosities at different temperatures. The computed intrinsic attenuation at 500 kHz cannot completely predict the measured attenuation results from the experimental study in an ice-brine coexisting system, which suggests that other attenuation mechanisms such as the squirt-flow mechanism and wave scattering effect should be taken into account.

Mossbauer Studies of the $H_2$ Reduction Effects On Magnetic Properties of Sr-Ba Substituted Hexgonal Ferrite (치환형 Sr-Ba 육방 페라이트들의 자기적 성질에 수소환원이 미치는 효과에 관한 Mossbauer 분광학적 연구)

  • 박재윤;권명회;이재광
    • Journal of the Korean Magnetics Society
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    • v.9 no.1
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    • pp.35-40
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    • 1999
  • Sr substituted materials for some barium in M-type barium ferrite powder and Co-Ti substituted Sr-Ba hexagonal ferrite powder were prepared by citrate sol-gel method and 2 MOE sol-gel method these hexaferrite particles were reduced for 1hr in the hydrogen gas. The reduction temperatures were varied in the range of 250 $^{\circ}C$ to 500 $^{\circ}C$. X-ray diffraction patterns were measured using diffractometer with Cu $K_{\Alhpa}$ radiation. Mossbauer absorption spectra were measured with a constant acceleration spectrometer. We have focused on studying the origin of increasing $M_s$ by M$\"{o}$ssbauer spectroscopy. Ferrite particles which were sintered at 105$0^{\circ}C$ were found to be typical magnetoplumbite structure and single phase. XRD patterns with varying the reduction temperatures in $Sr_{0.5}Ba_{0.5}Fe_{10}O_{19}$ indicates ferrites particles become composite hexaferrites containing $\alpha$-Fe at T_{red}=350 \;$^{\circ}C$$. On the otherhand, it was found that $Co^{2+}$ ions and $Ti^{4+}$ ions in $Sr_{0.7}Ba_{0.3}Fe_{10}CoTiO_{19}$ prevent from changing $Fe^{3+}$ ions to $\alpha$-Fe during the $H_2$ reduction. Comparing Mossbauer results with XRD results, we have determined most of $\alpha$-Fe are reduced from $4f_{vi}$ sites and 12k sites of $Fe^{3+}$ ions. These $\alpha$-Fe phase bring the induced anisotropy and increase saturation magnetization $M_s$.TEX>.

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