• Journal of the Korean institute of surface engineering
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• v.49 no.1
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• pp.62-68
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• 2016

A chromium-free Ce-based conversion coating formed by immersion in a solution containing cerium chloride and nitric acid on AZ31 magnesium alloy has been studied. The effects of acid pickling on the morphology and the corrosion resistance of the cerium conversion coating were investigated. The corrosion resistance of the conversion coating prepared on AZ31 Mg alloy after organic acid pickling was better than that of inorganic acid pickling. The morphology of the conversion-coated layer was observed using optical microscope and SEM. Results show that the conversion coatings are relatively uniform and continuous, with thickness 1.0 to $1.1{\mu}m$. The main elements of the conversion coating of AZ31 Mg alloy are Mg, O, Al, Ce and Zn by EDS analysis. The electrochemical polarization results showed that the Ce-based conversion coating could reduce the corrosion activity of the AZ31 Mg alloy substrates in the presence of chloride ions.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.11 no.6
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• pp.16-21
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• 2012

Magnesium alloy has been focussed as lightweight material owing to its high strength even though low density with aluminum alloy, titanium alloy and plastic material. Friction stir welding technique was performed by rotating and plunging a shouldered tool with a small diameter pin into the joint line between two butted plates and useful to join magnesium alloy. In this paper, the experiments of friction stir welding were done to investigate the joint characteristics of AZ31 magnesium alloy. For its evaluation, the orthogonal array method$(L_{27}(3^{13}))$ was applied with four factors of pin diameter, shoulder diameter, travel speed and rotation speed of tool and also three levels of each factor. Nine tools were worked through shoulder diameter of 9, 12, 15mm and pin root diameter of 3, 4, 5mm. In addition tensile tests were excuted for the assessment of mechanical properties for joint conditions. From the results, pin diameter, shoulder diameter, and rotating speed of tool influenced on the tensile strength meaningful, but welding speed did not influence on that by the variance analysis. Beside of that, optimum condition of tensile strength was estimated as following ; shoulder diameter:15mm, welding speed:200mm/min, rotating speed:200rpm.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.480-481
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• 2008

The aim of this work is to compare the microstructure, the texture, of an AZ31 Mg alloy processed via cold rolling process. Initial AZ31 Mg alloy sheet samples with strong {0002} texture were cut along the angles of 12.5 and 25 degrees to normal direction (ND). These specimens were rolled in room temperature condition. The microstructure was characterized by optical microscopy and the texture was measured by X-ray diffraction.

• Journal of the Korean Society for Heat Treatment
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• v.33 no.4
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• pp.180-184
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• 2020

The crystallographic texture plays an important role in both the plastic deformation and the macroscopic anisotropy of magnesium alloys. In previous study for AZ80 magnesium alloy, it was found that the main texture components of the textures vary with the deformation conditions at high temperatures. Also, the basal texture was formed at stress of more than 15-20 MPa and the non-basal texture was formed at stress of less than 15-20 MPa. Therefore, in this study, uniaxial compression deformation of AZ80 magnesium alloy was carried out at high temperature (stress of 15-20 MPa). The uniaxial compression deformation is performed at temperature of 723 K and strain rate 3.0 × 10^-3s^-1, with a strain range of between -0.4 and -1.3. Texture measurement was carried out on the compression planes by the Schulz reflection method using nickel filtered Cu Kα radiation. EBSD measurement was also conducted in order to observe spatial distribution of orientation. As a result of high temperature deformation, the main component of texture and its development vary depending on deformation condition of this study.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.3 no.1
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• pp.66-71
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• 2004

Magnesium alloys have been widely used for many structural components of automobiles and aircraft because of high specific strength and good cast-ability in spite of hexagonal closed-packed crystal structure of pure magnesium. In this study, it is studied about the forming characteristics of press forging of AZ31 magnesium alloy by MSC/MARC in case of material having one boss and MSC/Supeiforge in case of material having multi-boss with heat transfer analysis during deformation at elevated temperature. For these results it is simulated about temperature distribution, strain distribution, and stress distribution of AZ31 Magnesium alloy. During the press forging, foot regions of bosses showed greater temperature rise than other areas of AZ31 sheet. Finally the plastic strain of AZ31 sheet did not remarkably vary with increasing temperature from 373 to 473K, while it significantly increased as the forming temperature increased from 473 to 573K, which is related with the change in micro-structures, such as dynamic re-crystallization occurring during the deformation process.

• Journal of the Korean Society of Marine Environment & Safety
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• v.17 no.2
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• pp.155-160
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• 2011

In these days, there are increasing demands for weight reduction in many industrial fields including marine industries. Therefore, magnesium thin films for lightweight materials were prepared on magnesium alloy substrate. The influence of gas pressure and substrate bias voltages on the crystal orientation and morphology of the films was determined by using X-ray diffraction and FE-SEM, respectively. And the effect of crystal orientation and morphology of the magnesium thin films on corrosion behavior was estimated by measuring electro-chemical anodic polarization curves in deaerated 3% NaCl solution. From the results, corrosion resistance of Mg thin films was improved by controlling the crystal orientation and morphology of the films with effective use of plasma ion plating technique.

• Journal of Welding and Joining
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• v.31 no.2
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• pp.57-62
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• 2013

Magnesium has good castability and limited workability, so its products have been manufactured by almost casting processes. In this study, a pulsed Nd:YAG laser was used to butt-weld the sand casting magnesium alloys. And the effect of welding conditions such as peak power, pulse width, welding speed was evaluated in detail. As a result of this study, large underfill and plenty of spatter taken place under the conditions with high peak power. Thus, it is recommended to use low peak power and long pulse width to obtain good welds with deep penetration. It is also confirmed that the welding speed and pps(pulse per second) are directly connected at weld defects such as underfill, porosity.

• Transactions of Materials Processing
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• v.14 no.6 s.78
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• pp.520-526
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• 2005

In recent years, there has been a growth of the manufacture and application of magnesium products because of its small specific gravity as well as its relatively high strength. However, there are so many studies to assure good formability because magnesium sheet alloy is difficult to form. In this study, uniaxial tensile and biaxial tensile tests of AZ31 magnesium sheet alloy with thickness of 1.2mm were performed at room temperature. Uniaxial tensile tests were performed until $7{\%}$ of engineering strain. Lankford values and stress-strain curve were obtained. Biaxial tensile tests with cruciform specimen were performed until the breakdown of the specimen occurs. The yield loci were calculated by application of plastic work theory. The results are compared with the theoretical predictions based on the Hill and Logan-Hosford model. In this study, Hill's 1979 yield function for the case of m=2.8 and Logan-Hosford yield function for the case of M=8 give good agreements with experimental results. However, next study will be performed at warm-temperature because the specimens are broken under the $0.5{\%}$ of equivalent strain at biaxial tensile test.

• Journal of the Korean Institute of Gas
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• v.16 no.6
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• pp.1-6
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• 2012

Using the Siwek 20 L spherical explosion vessel, the explosion properties have been examined to understand the influence of magnesium content in Mg-Al alloy dusts with different concentration. For this purpose, the Mg-Al alloy dusts (volume mean diameter : $151{\sim}160{\mu}m$) with magnesium content ratio were used. As the results, the increase of Mg content in Mg-Al alloy causes an decreased minimum explosion concentration and an increased maximum explosion pressure. Also the maximum explosion pressure and maximum rate of pressure rise in Mg-Al alloy dusts mainly depended on the dust concentrations. However, for the explosion index (Kst) of Mg-Al (40:60 wt%), Mg-Al (50:50 wt%) and Mg-Al (60:40 wt%), it was founded to increase the Kst with increasing of magnesium content ratio.

• Korean Journal of Materials Research
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• v.32 no.9
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• pp.391-395
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• 2022

Research is being actively conducted on the continuous thin plate casting method, which is used to manufacture magnesium alloy plate for plastic processing. This study applied a heat transfer solidification analysis method to the melt drag process. The heat transfer coefficient between the molten magnesium alloy metal and the roll in the thin plate manufacturing process using the melt drag method has not been clearly established until now, and the results were used to determine the temperature change. The estimated heat transfer coefficient for a roll speed of 30 m/min was 1.33 × 10⁵ W/m²·K, which was very large compared to the heat transfer coefficient used in the solidification analysis of general aluminum castings. The heat transfer coefficient between the molten metal and the roll estimated in the range of the roll speed of 5 to 90 m/min was 1.42 × 10⁵ to 8.95 × 10⁴ W/m²·K. The cooling rate was calculated using a method based on the results of deriving the temperature change of the molten metal and the roll, using the estimated heat transfer coefficient. The DAS was estimated from the relationship between the cooling rate and DAS, and compared with the experimental value. When the magnesium alloy is manufactured by the melt drag method, the cooling rate of the thin plate is in the range of about 1.4 × 10³ to 1.0 × 10⁴ K/s.