• Transactions of Materials Processing
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• v.15 no.3 s.84
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• pp.232-240
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• 2006

Magnesium alloys are expected to be widely used fur the parts of structural and electronic appliances due to their lightweight and EMI shielding characteristics. While the die casting has been mainly used to manufacture the parts from the magnesium alloys, the press forming is considered as an alternative to the die casting for saving the manufacturing cost and improving the structural strength of the magnesium alloy parts. However, the magnesium alloy has low formability at room temperature and therefore, in many cases, forming at elevated temperatures is necessary to obtain the required material flow without failure. In the present study, square cup deep drawing tests using the magnesium alloy AZ31 sheet were experimentally conducted at various elevated temperatures as well as room temperature, and the corresponding finite-element simulations, which calculated the damage evolution based on the Oyane's criterion, were conducted using the stress-strain relations from the tensile tests at various temperatures. The formability predictability by the finite-element analysis was investigated by comparing the predicted damage distributions over the deformed AZ31 sheet at elevated temperatures with the corresponding experimental deformations with failures.

• Proceedings of the KWS Conference
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• 2007.11a
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• pp.328-331
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• 2007

It was carried out to evaluate microstructure and mechanical properties of friction stir welded(FSW) on magnesium alloys. Two types magnesium alloy was used in this work, AZ31 wrought and AZ91 cast magnesium alloy. Microstructure near the weld zone showed general weld structures such as stir zone(SZ), thermo-mechanically affected zone(TMAZ) and heat affected zone(HAZ). In the AZ91 alloy, the SZ had a fine grain size and $\beta$ phase particles which were well distributed in matrix. It was characterized to redistribute by partial or full re-solution of the $\beta$ phase which is coarse in base metal during FSW processing. The hardness of the SZ slightly increase than the base metal in AZ31 Mg alloy.

• Corrosion Science and Technology
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• v.5 no.2
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• pp.77-83
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• 2006

The plasma electrolytic oxidation (PEO) process is a relatively new surface treatment technique that produces a chemically stable and environment-friendly electrolytic coating that can be applied to all types of magnesium alloys. In this study, the characteristics of oxide film were examined after coating the extruded AZ31 alloy through the PEO process. Hard ceramic coatings were obtained on the AZ31 alloy by changing the coating time from 10min to 60min. The morphologies of the surface and the cross-section of the PEO coatings were examined by scanning electron microscopy and optical microscopy, and the thickness of the coating was measured. The X-ray diffraction pattern of the coating shows that the coated layer consists mainly of the MgO and $Mg_2SiO_4$ phases after the oxidation reaction. The hardness of the coated AZ31 alloy increased with increasing coating time. In addition, the corrosion rates of the coated and uncoated AZ31 alloys were examined by salt spray tests according to ASTM B 117 and the results show that the corrosion resistance of the coated AZ31 alloy was superior to that of the un-coated AZ31 alloy.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.05a
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• pp.289-293
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• 2007

The effect of temperature on the forming limit diagram was investigated for AZ31B magnesium alloy sheet through the limit dome height test in the range from room temperature to $300^{\circ}C$. The formability of AZ31B sheet was improved significantly according to the increasing temperature. Also we studied the springback characteristics through the 2D draw bending test with different blank holding forces at elevated temperatures. Springback quantity was considerably reduced as temperature went up. The blank holding force in the range used, however, had little influence on springback. Experimental results obtained in this study may provide a material database for AZ31B sheet.

• Journal of the Korean institute of surface engineering
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• v.49 no.1
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• pp.62-68
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• 2016

A chromium-free Ce-based conversion coating formed by immersion in a solution containing cerium chloride and nitric acid on AZ31 magnesium alloy has been studied. The effects of acid pickling on the morphology and the corrosion resistance of the cerium conversion coating were investigated. The corrosion resistance of the conversion coating prepared on AZ31 Mg alloy after organic acid pickling was better than that of inorganic acid pickling. The morphology of the conversion-coated layer was observed using optical microscope and SEM. Results show that the conversion coatings are relatively uniform and continuous, with thickness 1.0 to $1.1{\mu}m$. The main elements of the conversion coating of AZ31 Mg alloy are Mg, O, Al, Ce and Zn by EDS analysis. The electrochemical polarization results showed that the Ce-based conversion coating could reduce the corrosion activity of the AZ31 Mg alloy substrates in the presence of chloride ions.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.149-153
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• 2008

Since magnesium alloy sheets have been employed in industrial field which requires the light weight and thin engineering components, most of researches have been focused on the formability of magnesium ahoy sheet. In warm press forming of magnesium alloy sheet, it is important to control the sheet temperature by heating the sheet in closed die. When forming a commercial AZ31 magnesium alloy sheets which are 0.5mm and 1.0mm thick, respectively, time arriving at target temperature and temperature variation in magnesium alloy sheet have been investigated. Sheet metals were mostly formed in simple shapes such as circular or rectangular. Few studies about forming of complex shapes were reported. Thus, the formability of magnesium alloy sheet for complex shapes is investigated. The process variable for a double sink shape deep drawing with circular and rectangular shape was investigated by varying temperature, velocities, and clearances. Accordingly, temperature, velocities, and clearances suitable for forming were suggested through investigating the thickness variation of the product.

• Transactions of Materials Processing
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• v.16 no.5 s.95
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• pp.364-369
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• 2007

The effect of temperature on the forming limit diagram was investigated for AZ31B magnesium alloy sheet through the limit dome height test in the range from room temperature to $300^{\circ}C$. The formability of AZ31B sheet was improved significantly according to the increasing temperature. Also we studied the springback characteristics through the 2D draw bending test with different blank holding forces at elevated temperatures. Springback quantity was considerably reduced as temperature went up. The blank holding force in the range used, however, had little influence on springback. Experimental results obtained in this study may provide a material database for AZ31B sheet.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.242-245
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• 2007

In the present investigation, the multi-stage warm drawing process was applied to the magnesium alloy AZ31 sheet to examine the feasibility of multi-stage forming process as a high formability product making process. For that purpose, a multi-stage drawing die system with heating module was developed, and the AZ31 sheets of different sizes were consecutively drawn by the multi-stage drawing die. The obtained drawn cups of AZ31 showed that the multi-stage drawing provided the better formability than the single stage drawing in terms of drawing depth without cup defects such as wrinkles or fractures. The sheet formability improvement by using the multi-stage drawing die system against the single stage was also analyzed in terms of the finite element analysis of material state variables evolution.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.480-481
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• 2008

The aim of this work is to compare the microstructure, the texture, of an AZ31 Mg alloy processed via cold rolling process. Initial AZ31 Mg alloy sheet samples with strong {0002} texture were cut along the angles of 12.5 and 25 degrees to normal direction (ND). These specimens were rolled in room temperature condition. The microstructure was characterized by optical microscopy and the texture was measured by X-ray diffraction.

• Laser Solutions
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• v.15 no.3
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• pp.11-15
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• 2012

The laser weld of AZ31 magnesium alloy was characterized with OM, EBSD and micros vickers hardness tester in experiment. EBSD analysis and micro-hardness measurements were carried out at the three regions (Equiaxed Zone, Columnar Dendrite Zone, Base Metal) of the welded AZ31Mg alloy sheets. The magnesium alloy show the rectangular shape bead in laser weld. EBSD analysis revealed that the three regions show the heterogeneous distribution of grain size and microtexture. Micro-hardness measurement also revealed that the heterogeneous distribution of microstructure contributed to the heterogeneous micro-hardness distribution in the three regions.