• Title/Summary/Keyword: MOD 법

검색결과 91건 처리시간 0.027초

Ferroelectric Properties of Bi3.25La0.75Ti3O12 Thin Films Prepared by MOD (MOD 법으로 제작된 Bi3.25La0.75Ti3O12 박막의 강유전 특성)

  • 김경태;김창일;권지운;심일운
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • 제15권6호
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    • pp.486-491
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    • 2002
  • We have fabricated $Bi_{3.25}La_{0.75}Ti_3O_12$ (BLT) thin films on the Pt/Ti/$SiO_2$/Si substrates using a metalorganic decomposition (MOD) method with annealing temperature from $550^{\circ}C$ to $750^{\circ}C$. The structural properties of BLT films examined by x-ray diffraction (XRD). From XRD analysis. BLT thin films show polycrystalline structure. The layered-perovskite phase was obtained by spin-on films at above $600^{\circ}C$ for 1h. Scanning electron microscopy (SEM) showed uniform surface composed of rodlike grains. The grain size of BLT films increased with increasing annealing temperature. The BLT film annealed at $650^{\circ}C$ was measured to have a dielectric constant of 279, dielectric loss of 1.85(%), remanent polarization of $25.66\mu C/\textrm{cm}^2$, and coercive field of 84.75 kV/cm. The BLT thin films showed little polarization fatigue test up to $3.5{\times}10^9$ bipolar cycling at 5 V and 100 kHz.

Effects of Bottom Electrode to Dielectric and Electrical Properties of MOD Derived Ferroelectric SBT Thin Films (MOD 법으로 제조한 강유전성 SBT 박막에서 하부전극이 유전 및 전기적 특성에 미치는 영향)

  • 김태훈;송석표;김병호
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • 제13권8호
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    • pp.694-699
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    • 2000
  • S $r_{0.9}$/B $i_{2.1}$/T $a_{2}$/ $O_{9}$ solutions was synthesized by MOD (metalorganic decomposition) method. SBT thin films with 2000$\AA$ thickness were prepared on Ir $O_2$/ $SiO_2$/Si and Pt/Ti/ $SiO_2$/Si substrates using the spin coating process and then investigated the dielectric and electrical properties of them. In the case of using Ir $O_2$bottom electrode the hysteresis loop was saturated at lower temperature than Pt/Ti electrode but the breakdown phenomenon was occurred at low voltage because of the rough surface morphology and porous microstructure of SBT thin films. As the results of the fatigue and imprint characteristics related to the lifetime and reliability of devices after 10$^{10}$ cycles the fatigue rates were about 10% at the Ir $O_2$and Pt/Ti bottom electrodes. Both SBT thin films with Ir $O_2$ and with Pt/Ti bottom electrodes show a slight tendency to imprint after 10$^{9}$ cycles but do not lead to a failure.e.e.

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Residual Life Assessment of mod HP Reformer Tubes Using Surface Replication Methods (표면복제를 사용한 mod HP강 개질로 튜브의 잔여수명 평가에 대한 연구)

  • Ryu, Hyung Ki;Le, Thi Giang;Bang, Hyo Jung;Yoon, Kee Bong
    • Journal of the Korean Institute of Gas
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    • 제25권5호
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    • pp.30-36
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    • 2021
  • Residual life assessment of reformer tubes of mod HP steel used in the refinery and petrochemical industry were investigated by quantitative metallographic evaluation method. Area fractions of precipitated carbides were measured by using surface replication and its relationship with the remaining life of the tube was investigated. The microstructures of the virgin and other tubes were examined using optical microscopy (OM) for service periods of 1.8, 6.0, 7.2, 8.5, 9.7, and 16.2 years at 950 ℃ and the area fractions of the precipitates were measured by image analysis using ImageJ software. As the area fraction of the precipitates increased, the residual life was decreased accordingly. The results showed that the LMP was the highest in the virgin and the LMP decreased as the service time increased and the residual life decreased. A regressional equation showing the relation between the area fraction of carbides and LMP was experimentally derived. The obtained relationship can be used with the surface replication method for on-site residual life assessment.

A pseudo Random Permutation Generator with application to random bit genefator (랜덤 치환 고속 발생기 설계 및 응용)

  • Ko, Seung-Cheol;Lee Dae-Gi
    • Review of KIISC
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    • 제3권1호
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    • pp.26-30
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    • 1993
  • 본 논문에서는Akl-Meijer가 설계한 랜덤 치환 발생기를 일반화한 알고리즘을 제안한다. Akl과 Meijer는 사이즈가 m인 치환(Permutation)과 0과 m!-1사이의 정수를 일대일 대응시키는 Knuth의 알고리즘을 이용하여, 선형 합동법 Y=X+C mod m! (C는 상수)에서 발생되는 난수와 일대일 대응되는 치환을 발생하는 치환 발생 알고리즘을 설계하였으며, 이를 응용하여, 이진 난수 발생기를 제시하였다. 본 논문에서는 선형 합동법 Y=AX+C mod m!(A, C는 상수)에서 발생되는 난수와 일대일 대응되는 치환 계산과정을 상삼각 행렬(Upper triangular matrix) 의 곱으로 변환하여 고속으로 계산하는 알고리즘을 제시한후, 이 알고리즘의 출력 치환을 n 개 결합하여 치환을 발생하는 랜덤치환 발생기를 설계한다. 또한 이의 암호적인 응용으로, 치환 발생기를 이용한 이진 난수 발생기를 제시한다.

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Reverse Baby-step 2k-ary Adult-step Method for 𝜙((n) Decryption of Asymmetric-key RSA (비대칭키 RSA의 𝜙(n) 해독을 위한 역 아기걸음- 2k-ary 성인걸음법)

  • Lee, Sang-Un
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • 제14권6호
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    • pp.25-31
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    • 2014
  • When the public key e and the composite number n=pq are disclosed but not the private key d in an asymmetric-key RSA, message decryption is carried out by obtaining ${\phi}(n)=(p-1)(q-1)=n+1-(p+q)$ and subsequently computing $d=e^{-1}(mod{\phi}(n))$. The most commonly used decryption algorithm is integer factorization of n/p=q or $a^2{\equiv}b^2$(mod n), a=(p+q)/2, b=(q-p)/2. But many of the RSA numbers remain unfactorable. This paper therefore applies baby-step giant-step discrete logarithm and $2^k$-ary modular exponentiation to directly obtain ${\phi}(n)$. The proposed algorithm performs a reverse baby-step and $2^k$-ary adult-step. As a results, it reduces the execution time of basic adult-step to $1/2^k$ times and the memory $m={\lceil}\sqrt{n}{\rceil}$ to l, $a^l$ > n, hence obtaining ${\phi}(n)$ by executing within l times.

The Preparation of High $J_c$ YBCO Films by DCA-MOD Method (DCA-MOD 법에 의한 High $J_c$ YBCO 박막의 제조)

  • Kim, Byeong-Joo;Kim, Hye-Jin;Yi, Keum-Young;Lee, Jong-Beum;Kim, Ho-Jin;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • 제8권1호
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    • pp.59-64
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    • 2006
  • High $J_c\;YBa_2Cu_3O_x$ superconducting films were fabricated by MOD method using fluorine-free dichloroacetic acid(DCA) as chelating solvent for preparing precursor solution. Coating solutions were prepared by dissolving Y-, Ba- and Cu-acetates in DCA solvent followed by drying in rota vapor to obtain the blue gel that is diluted in methanol and 2-methoxyethanol for adjusting the cation concentration. DCA-MOD precursor solution was coated on a single crystal(001) $LaAlO_3(LAO)$ substrate by a dip coating method with a speed of 25 mm/min. Coated films were calcined at lower temperature up to $500^{\circ}C$ in flowing oxygen atmosphere with a 7.2% humidity. Conversion heat treatment was performed at various temperatures of $780{\sim}810^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. SEM observations showed that films have very dense microstructures for the films prepared at the temperature higher than $800^{\circ}C$ regardless of diluting solvent; methanol or 2-methoxyethanol. X-ray diffraction analysis showed that YBCO grains grew with a (001) preferred orientation. A High critical current density($J_c$) of 1.28 $MA/cm^2$(@77 K and self-field) was obtained id. the YBCO film prepared using 2-methoxyethanol as a solvent.

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Effect of heating rate on calcination heat treatment of YBCO thin films by DCA-MOD method (DCA-MOD 법으로 YBCO 박막 제조시 하소열처리의 승온속도 효과)

  • Kim, Byeong-Joo;Kim, Hye-Jin;Cho, Han-Woo;Kwon, Youn-Kyung;Ryu, Jung-Hee;Lee, Hee-Gyoun;Hong, Gye-Won
    • Progress in Superconductivity
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    • 제8권2호
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    • pp.186-192
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    • 2007
  • High $J_c\;YBa_2Cu_3O_{7-x}$ superconducting films have been fabricated $LaAlO_3(100)$ substrate by MOD method using dichloroacetic acid(DCA) as chelating solvent for preparing precursor solution. Heating rate was varied in order to optimize the calcination heat treatment condition in DCA-MOD method. Coated films were calcined at lower temperature up to $500^{\circ}C$ in flowing humid oxygen atmosphere. The heating rate was calcined from $13.3^{\circ}C/min\;to\;0.28^{\circ}C/min$. Conversion heat treatment was performed $800^{\circ}C$ for 2 h in flowing Ar gas containing 1000 ppm oxygen with a humidity of 9.45%. Surface and cross sectional SEM microstructures showed that particle sizes were increased with heating rate at a calcination step. The amount of pores was increased with heating rate in the calcined films. Dense microstructure and sharp texture were developed in an YBCO films after conversion heat treatment. A high critical current density (Jc) of $1.26MA/cm^2$ (@77 K and self-field) was obtained for the YBCO film which was prepared with a heating rate of $0.28^{\circ}C/min$.

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