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An Experimental Study on the Microstructure Characteristics of Cementitious Composites by MIP (MIP를 통한 혼합 시멘트계 재료의 미세구조 특성에 관한 실험적 연구)

  • Kim, Tae-Sang;Jung, Sang-Hwa;Chae, Seong-Tae;Lee, Bong-Chun;Woo, Young-Je;Song, Ha-Won
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.533-536
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    • 2008
  • Recently, in Korea, there has been an increasing number of research papers published which are to improve durability of concrete, particularly by analyzing correlation between diffusivity of chloride and porosity/pore size distribution. In these studies, such test methods as mercury intrusion porosimetry(MIP), gas adsorption or image analysis method are used to analyze the microstructure of materials while MIP is most widely used for concrete. This study analyzes the results of porosity and pore size distribution of paste and concrete adding fly ash or blast furnace slag by using MIP equipment which is widely used for determining micro-porosity structure of cementitious materials. A variation in porosity and pore size distribution at the curing day 3, 7 and 28 has been observed by using MIP equipment for cement paste 35%, 40%, 45%, 50%, 55%, 60% of W/C when using $300kg/m^3$ of cement, 35%, 45%, 55% of W/C when replaced 60% with blast-furnace slag, and 35%, 45%, 55% of W/C when replaced 30% with fly ash. For long-term water cured normal OPC concrete and mixed concrete replaced 60% with blast-furnace slag powder, micro-structure of the sample has been analyzed by using MIP equipment when W/C indicated 40%, 45%, 50% respectively and the binder varied $300kg/m^3$, $350kg/m^3$, $400kg/m^3$, and $450kg/m^3$.

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Characteristics of a planar Bi-Sb multijunction thermal converter with Pt-heater (백금 히터가 내장된 평면형 Bi-Sb 다중접합 열전변환기의 특성)

  • Lee, H.C.;Kim, J.S.;Ham, S.H.;Lee, J.H.;Lee, J.H.;Park, S.I.;Kwon, S.W.
    • Journal of Sensor Science and Technology
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    • v.7 no.3
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    • pp.154-162
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    • 1998
  • A planar Bi-Sb multijunction thermal converter with high thermal sensitivity and small ac-dc transfer error has been fabricated by preparing the bifilar thin film Pt-heater and the hot junctions of thin film Bi-Sb thermopile on the $Si_{3}N_{4}/SiO_{2}/Si_{3}N_{4}$-diaphragm, which functions as a thermal isolation layer, and the cold junctions on the dielectric membrane supported with the Si-substrate, which acts as a heat sink, and its ac-dc transfer characteristics were investigated with the fast reversed dc method. The respective thermal sensitivities of the converter with single bifilar heater were about 10.1 mV/mW and 14.8 mV/mW in the air and vacuum, and those of the converter with dual bifilar heater were about 5.1 mV/mW and 7.6 mV/mW, and about 5.3 mV/mW and 7.8 mV/mW in the air and vacuum for the inputs of inside and outside heaters, indicating that the thermal sensitivities in the vacuum, where there is rarely thermal loss caused by gas, are higher than those in the air. The ac-dc voltage and current transfer difference ranges of the converter with single bifilar heater were about ${\pm}1.80\;ppm$ and ${\pm}0.58\;ppm$, and those of the converter with dual bifilar heater were about ${\pm}0.63\;ppm$ and ${\pm}0.25\;ppm$, and about ${\pm}0.53\;ppm$ and ${\pm}0.27\;ppm$, respectively, for the inputs of inside and outside heaters, in the frequency range below 10 kHz and in the air.

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WEIGHTED VECTOR-VALUED BOUNDS FOR A CLASS OF MULTILINEAR SINGULAR INTEGRAL OPERATORS AND APPLICATIONS

  • Chen, Jiecheng;Hu, Guoen
    • Journal of the Korean Mathematical Society
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    • v.55 no.3
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    • pp.671-694
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    • 2018
  • In this paper, we investigate the weighted vector-valued bounds for a class of multilinear singular integral operators, and its commutators, from $L^{p_1}(l^{q_1};\;{\mathbb{R}}^n,\;w_1){\times}{\cdots}{\times}L^{p_m}(l^{q_m};\;{\mathbb{R}}^n,\;w_m)$ to $L^p(l^q;\;{\mathbb{R}}^n,\;{\nu}_{\vec{w}})$, with $p_1,{\cdots},p_m$, $q_1,{\cdots},q_m{\in}(1,\;{\infty})$, $1/p=1/p_1+{\cdots}+1/p_m$, $1/q=1/q_1+{\cdots}+1/q_m$ and ${\vec{w}}=(w_1,{\cdots},w_m)$ a multiple $A_{\vec{P}}$ weights. Our argument also leads to the weighted weak type endpoint estimates for the commutators. As applications, we obtain some new weighted estimates for the $Calder{\acute{o}}n$ commutator.

Second Harmonic Generation of Low Power Laser Diode Using a Ring Enhancement Cavity (고리형 Enhancement Cavity 를 이용한 저출력 반도체 레이저의 제2조화파 발생)

  • 오차환
    • Korean Journal of Optics and Photonics
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    • v.4 no.2
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    • pp.206-211
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    • 1993
  • We carried out the second harmonic generation of low power CW laser diode with maximum power of 30 mW in $LilO_3$ crystals. We used a ring enhancement cavity to increase the second harmonic conversion efficiency. The ring enhancement cavity was Composed of two flat mirrors and two concave mirrors. The focal length of concave mirrors was 25 mm, and 5 mm long and 10 mm long $LilO_3$ crystals were used. We measured the second harmonic power according to the pumping power and compared with theoretical value. We obtained 397 nm second harmonic power of about $6.6{\mu}W$ in 10 mm long $LilO_3$ crystal with the fundumental 794 nm pumping power of 28 mW.

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축전결합형 고주파 $BCl_3$/He 플라즈마를 이용한 GaAs와 AlGaAs의 건식식각

  • Lee, Seong-Hyeon;Sin, Ju-Yong;Park, Ju-Hong;Choe, Gyeong-Hun;Song, Han-Jeong;Lee, Je-Won
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.08a
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    • pp.221-221
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    • 2010
  • 본 실험에서는 축전결합형 고주파 플라즈마와 $BCl_3$와 He의 혼합가스를 이용하여 화합물 반도체인 GaAs와 AlGaAs의 건식식각에 대해 연구하였다. 공정변수로는 첫째, BCl3와 He의 혼합가스 비율을 0%에서 100%까지 변화시켰다. 둘째, 고주파 파워를 50 W에서 200W 까지 변화를 주었고, 셋째, 공정압력을 120 mTorr~300 mTorr 까지 변화시켰다. 식각 실험을 마친 시료는 표면 단차 측정기와, 주사전자현미경을 이용하여 식각률과 선택비, 표면거칠기, 표면형상에 대하여 분석을 진행하였다. 또한, 광학발광분석계 (OES)를 이용하여 건식식각 실험 중 혼합가스에 의해 발생하는 플라즈마의 발광특성에 대한 실시간 분석을 하였다. 결과에 따르면, 1) 혼합가스에서 He의 비율이 20%일 때 GaAs와 AlGaAs 시료의 식각율이 $0.7\;{\mu}m/min$$0.6\;{\mu}m/min$ 로 가장 높게 나타났다. 2) 감광제에 대한 시료의 선택비 또한 동일 조건에서 GaAs의 경우 1 : 12, AlGaAs의 경우 1:8로 가장 높게 나타났다. 3)고주파 파워의 변화에 따른 식각률의 경우 100 W에서 GaAs 의 경우 $0.6\;{\mu}m/min$, AlGaAs의 경우 $0.5\;{\mu}m/min$ 이었고, 고주파 파워가 증가할수록 식각률은 감소하였다. 4) 감광제에 대한 시료의 식각 선택비의 경우 50 W에서 GaAs 시료가 1:14, AlGaAs 시료가 1:10으로 가장 높은 선택비를 보였고 고주파 전원이 증가할수록 선형적으로 감소하였다. 5) 표면거칠기는 50~100 W 구간에서는 1.0~1.5 nm 으로 큰 증가폭이 없다가 150 W 이상에서는 3.0~5.0 nm 으로 증가하였다. 반응기의 압력이 120 mTorr에서 300 mTorr로 변화할 때 식각률과 선택비는 비교적 선형적으로 감소하였으며, 표면거칠기 또한 증가하였다. 결론적으로 $BCl_3/He$ 고주파 플라즈마에서 약 20%의 He을 포함하고 있을 때 가장 우수한 건식 식각 결과를 얻었다.

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Effects of Security Lighting Lamps on Discomfort Glare to Indoor Occupants

  • Lee, Yoon Jeong;Kim, Jeong Tai
    • KIEAE Journal
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    • v.15 no.4
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    • pp.21-28
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    • 2015
  • Purpose: Although security lights are used to secure pedestrian visibility and safety at nighttime, they can generate light trespass in the neighboring residential space. To prevent this, standards for acceptance limits on vertical illuminance and light pollution by the windows of residential buildings are presented. Method: This study thus representatively selected three types of lamps and, through an evaluation and analysis of the physical and subjective discomfort glare per lamp, proposed a discomfort glare index for each lamp. The evaluation and analysis according to the lamps were conducted through experiments. The variables were the security lights' lamps (NH 100W, MH 70W, LED 50W), installation angles ($0^{\circ}$, $20^{\circ}$), and installation distances (3m, 5m, 7m, 9m). Result: According to the results of the discomfort glare evaluation depending on the angles and distances of the security lights, the following minimum standards are proposed: for NH 100W, a discomfort glare index of 30 and an installation distance of 4m; for MH 70W, a discomfort glare index of 32 and an installation distance of 4m; and, for LED 50W, a discomfort glare index of 31 and an installation distance of 6m, respectively. In addition, this paper recommends the use of MH 70W, when the road width is 4m-6m, and LED 50W, when the road width is over 6m, respectively.

Comparative Study of the Ablation Rates of Er: YAG Laser Irradiation on Dentin and Enamel (Er:YAG 레이저를 이용한 법랑질과 상아질의 절삭율 연구)

  • Kim, Kun-A;Ahn, Yong-Woo;Ko, Myung-Yun;Park, June-Sang
    • Journal of Oral Medicine and Pain
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    • v.30 no.1
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    • pp.131-140
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    • 2005
  • The purpose of this study was to examine the ablation rate of Er: YAG laser irradiation on dentin and enamel and to observe the microscopic structures of cavities formed after ablation of enamel and dentin in using a bur and cavities formed after ablation using laser. Er:YAG laser irradiated at 200 mJ, 250mJ, 300mJ at the frequency of 20Hz, 15Hz. The following results were obtained : 1. The ablation rate of dentin groups at power of 3 W-6 W was about $1.103{\sim}2.639mm^3/sec$ and there were no significant differences between power of 4.5 W$\sim$6 W. 2. The ablation rate of enamel groups at power of 3 W-6 W was about $0.413{\sim}0.969mm^3/sec$ and there were no significant differences between power of 4 W$\sim$6 W. 3. With SEM examination of the cavity surface treated with the conventional high speed bur revealed relatively flat appearance almost covered with a debris like smear layer. 4. With SEM examination of the lased surface of dentin groups revealed no smear layer and no debris and openings of dentinal tubules were clearly opened. But the lased surfaces of the groups over 3 W were irregular and particles were loosely attached on it. 5. With SEM examination of the lased surface of enamel groups revealed severely destructed surface at the 6 W group and melting drop materials at the 3 W group. But the lased surface of 4 W group revealed clearly ablated surface. Therefore when cutting teeth using Er:YAG laser, the lasing power which can make effective ablation rate and minimize the thermal effect could be 3W at dentin and 4W at enamel. But, further studies and additional data collection will be necessary for appropriate lasing condition of Er:YAG laser.

Dielectric and Piezoelectric Properties of PMW-PNN-PZT System Ceramics (PMW-PNN-PZT계 세라믹스의 유전및 압전특성)

  • 윤광희;류주현;윤현상;박창엽
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.13 no.3
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    • pp.214-219
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    • 2000
  • In this paper the structural dielectric and piezoelectric properties of Pb[(M $g_{1}$2// $W_{1}$2/)$_{x}$-(N $i_{1}$3//N $b_{2}$3/)$_{0.15-x-(Zr_{0.5})}$ $Ti_{0.5}$)$_{0.85}$$O_3$ (x=0.0~0.10) ceramic were investigated with the substitution of Pb(M $g_{1}$2// $W_{1}$2/) $O_3$. According to the substitution of Pb(M $g_{1}$2//W/1/2/) $O_3$ curie temperatures were slightly decrease due to the decrease of the tetrag-onality of crystal structure and coercive fields were decreased. Up to the substitution of Pb(M $g_{1}$2// $W_{1}$2/) $O_3$ 3mol%,remnant polarization dielectric constant piezoelectric constant were increased. Dielectric constant and electro-mechanical coupling factor( $k_{p}$, $k_{31}$ ) were appeared the highest value of 2230, 0.64, and 0.38 and piezoelectric constant( $d_{33}$ , $d_{31}$ ) was the largest value of 418, 202($\times$10$^{-12}$ /C/N), respectively, when the substitution amount of Pb(M $g_{1}$2// $W_{1}$2/N) respectively, when the substitution amount of Pb(M $g_{1}$2// $W_{1}$2/) $O_3$ was 3mol%.s 3mol%.%.

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A study on the Degradation and By-products Formation of NDMA by the Photolysis with UV: Setup of Reaction Models and Assessment of Decomposition Characteristics by the Statistical Design of Experiment (DOE) based on the Box-Behnken Technique (UV 공정을 이용한 N-Nitrosodimethylamine (NDMA) 광분해 및 부산물 생성에 관한 연구: 박스-벤켄법 실험계획법을 이용한 통계학적 분해특성평가 및 반응모델 수립)

  • Chang, Soon-Woong;Lee, Si-Jin;Cho, Il-Hyoung
    • Journal of Korean Society of Environmental Engineers
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    • v.32 no.1
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    • pp.33-46
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    • 2010
  • We investigated and estimated at the characteristics of decomposition and by-products of N-Nitrosodimethylamine (NDMA) using a design of experiment (DOE) based on the Box-Behken design in an UV process, and also the main factors (variables) with UV intensity($X_2$) (range: $1.5{\sim}4.5\;mW/cm^2$), NDMA concentration ($X_2$) (range: 100~300 uM) and pH ($X_2$) (rang: 3~9) which consisted of 3 levels in each factor and 4 responses ($Y_1$ (% of NDMA removal), $Y_2$ (dimethylamine (DMA) reformation (uM)), $Y_3$ (dimethylformamide (DMF) reformation (uM), $Y_4$ ($NO_2$-N reformation (uM)) were set up to estimate the prediction model and the optimization conditions. The results of prediction model and optimization point using the canonical analysis in order to obtain the optimal operation conditions were $Y_1$ [% of NDMA removal] = $117+21X_1-0.3X_2-17.2X_3+{2.43X_1}^2+{0.001X_2}^2+{3.2X_3}^2-0.08X_1X_2-1.6X_1X_3-0.05X_2X_3$ ($R^2$= 96%, Adjusted $R^2$ = 88%) and 99.3% ($X_1:\;4.5\;mW/cm^2$, $X_2:\;190\;uM$, $X_3:\;3.2$), $Y_2$ [DMA conc] = $-101+18.5X_1+0.4X_2+21X_3-{3.3X_1}^2-{0.01X_2}^2-{1.5X_3}^2-0.01X_1X_2+0.07X_1X_3-0.01X_2X_3$ ($R^2$= 99.4%, 수정 $R^2$ = 95.7%) and 35.2 uM ($X_1$: 3 $mW/cm^2$, $X_2$: 220 uM, $X_3$: 6.3), $Y_3$ [DMF conc] = $-6.2+0.2X_1+0.02X_2+2X_3-0.26X_1^2-0.01X_2^2-0.2X_3^2-0.004X_1X_2+0.1X_1X_3-0.02X_2X_3$ ($R^2$= 98%, Adjusted $R^2$ = 94.4%) and 3.7 uM ($X_1:\;4.5\;$mW/cm^2$, $X_2:\;290\;uM$, $X_3:\;6.2$) and $Y_4$ [$NO_2$-N conc] = $-25+12.2X_1+0.15X_2+7.8X_3+{1.1X_1}^2+{0.001X_2}^2-{0.34X_3}^2+0.01X_1X_2+0.08X_1X_3-3.4X_2X_3$ ($R^2$= 98.5%, Adjusted $R^2$ = 95.7%) and 74.5 uM ($X_1:\;4.5\;mW/cm^2$, $X_2:\;220\;uM$, $X_3:\;3.1$). This study has demonstrated that the response surface methodology and the Box-Behnken statistical experiment design can provide statistically reliable results for decomposition and by-products of NDMA by the UV photolysis and also for determination of optimum conditions. Predictions obtained from the response functions were in good agreement with the experimental results indicating the reliability of the methodology used.

Development of heat exchanger for underground water heat. II - Design and manufacture for heat exchanger of underground water - (지하수 이용을 위한 열교환기 개발. II - 지하수이용 냉·난방기 설계제작 -)

  • Lee, W.Y.;Ahn, D.H.;Kim, S.C.;Park, W.P.;Kang, Y.G.;Kim, S.B.
    • Journal of Practical Agriculture & Fisheries Research
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    • v.4 no.1
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    • pp.128-137
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    • 2002
  • This study was conducted to develop the heat exchanger by utilizing the heat energy of underground water(15℃), which might be used for cooling and heating system of the agricultural facilities. We developed the heat exchanger by using the parallel type plat fin tube made of Aluminum(Al 6063), which was named Aloo-Heat(No. 0247164, offered by Korean Intellectual property Office). The trial manufactures were made from Aloo-heat which was 600mm, 700mm length respectively, and It were welded to the end "U" type in order to direct flow of the underground water. The performance test was carried out under the condition of open space and room temperature with the change of flow rate of the underground water and air. The results are as follows. 1. The trial manufactures had convection heat value from 33 to 156 W/m2℃, and It was coincided with design assumption. 2. The amount of energy transfer was increased with the increment of the area of heat transfer, the air flow, the gap of temperature inlet & outlet the underground water and the air. 3. The heat value was 6,825W when the air flow was 6,000m3/h and the gap of temperature between inlet and outlet of the underground water was 6℃, and It dropped from 25.8℃ to 23.2℃(-2.6℃ difference). The convection heat value was 88.5W/m2℃. 4. The heat value was 2.625W when the air flow was 4,000m3/h and the gap of temperature between inlet and outlet the underground water was 2℃, and It dropped from 27℃ to 22.5℃(-4.5℃ difference). The convection heat value was 33.6W/m2℃. 5. Correlation values(R2) of the testing heat values of the trial manufacture type I, II, and III were 0.9141, 0.8935, and 0.9323 respectively, and correlation values(R2) of the amount of the air flow 6,000m3/h, 5,000m3/h, 4,000m3/h were 0.9513, 0.9414, and 0.9003 respectively.