• 제목/요약/키워드: M2 polarization

검색결과 641건 처리시간 0.027초

입자 크기가 PZT계 압전 후막의 물성에 미치는 영향 (Effects of Particle Size on Properties of PZT -Based Thick Films)

  • 김동명;김정석;천채일
    • 한국세라믹학회지
    • /
    • 제41권5호
    • /
    • pp.375-380
    • /
    • 2004
  • 알루미나 기판 위에 Pb(Ni$_{1}$3/Nb$_{2}$3/)O$_3$-PbZrO$_3$-PbTiO$_3$ 후막을 스크린 인쇄한 후 800∼100$0^{\circ}C$에서 소결하여 압전 후막을 제조하였다. 마모 밀과 볼 밀 분쇄법을 이용하여 입자 크기가 서로 다른 압전 분말을 제조하였으며, 압전 분말의 입자 크기가 후막의 미세구조와 전기적 성질에 미치는 영향을 조사하였다. 마모 밀링한 분말의 평균 입자 크기는 0.44 $\mu\textrm{m}$로 볼 밀링한 분말의 평균 입자 크기, 2.87 $\mu$m 보다 훨씬 작았다. 후막을 80$0^{\circ}C$에서 소결하였을 때는 마모 밀링한 분말로 제조한 후막의 입자 크기가 볼 밀링한 분말로 제조한 후막의 입자 크기보다 더 작았으며, 소결 온도가 증가함에 따라 그 차이가 점차 감소하였다. 그리고, 전체 소결 온도 구간에서 마모 밀링한 분말로 제조한 후막이 볼 밀링한 분말로 제조한 후막보다 균일하고 치밀한 미세구조를 보였다. 소결 온도가 90$0^{\circ}C$ 이상일 때, 마모 밀링한 분말로 제조한 후막이 볼 밀링한 분말로 제조한 후막보다 우수한 전기적 성질을 가졌다. 90$0^{\circ}C$에서 소결한 마모 밀링한 분말로 제조한 후막의 유전상수($\varepsilon$$_{r}$), 잔류분극(P$_{r}$), 항전계(E$_{c}$)는 각각 559, 16.3 $\mu$C/$cm^2$, 51.3 kV/cm이었다.다..

튀긴 마늘 flake 제조조건의 최적화 및 이화학적 특성 (Optimization of Manufacturing Condition for Fried Garlic Flake and the Physicochemical Properties)

  • 김경이;이은경
    • 한국식품조리과학회지
    • /
    • 제28권6호
    • /
    • pp.805-811
    • /
    • 2012
  • This study was carried out in order to optimize the manufacturing condition of fried garlic flakes as well as to investigate the physicochemical properties of the flakes. Fried garlic flake samples were prepared as follows: garlic was sliced by a thickness of 1.5 mm, 2.0 mm, 2.5 mm, which were measured by a thickness gage. The samples were fried in vegetable oil under different temperatures of $140{\sim}150^{\circ}C$, $160{\sim}170^{\circ}C$ and $180{\sim}185^{\circ}C$. The compression strength depending on the height (h) was measured in order to find the thickness effect by the rheometer (force control: 50 N, h: 3.25 mm). Moreover, the sample with 1.5 mm thickness showed crisp phenomena of the split compared with the crush shape of the 2.0 mm and 2.5 mm thick samples. The result of strength for time dependence showed a sample with a thickness of 1.5 mm, which was measured 5~9 times more than the 2.0 mm and 2.5 mm thick samples. We thought the reason that the 1.5 mm sample had less response power equivalent to compression force than the other samples. Alliin has been found to affect the immune responses in the blood, it is a derivative of the amino acid cysteine and is also quite heat stable. The LC system with a UV detection at 210 nm consists of a separation on a Zorbax TMS column and isocratic elution with water and ACN as a mobile phase. The alliin contents of raw and fried garlic flake under $140{\sim}150^{\circ}C$, $160{\sim}170^{\circ}C$ and $180{\sim}185^{\circ}C$ were 18.10 mg/mL, 14.0 mg/mL, 11.6 mg/mL and 11.1 mg/mL, respectively. The decrement of alliin content under different temperature was a small quantity hence, we confirmed that the increasing manufacturing temperature was not affected by the alliin content. Examining for the particle structure of fried garlic flakes by a polarization microscope, the color of the sample treated at $160{\sim}170^{\circ}C$ was pure yellow. Furder, the fiber shaped particle, which has an effect on the tough texture, almost did not appear compared to the different temperature conditions. Finally, the sensory test for the preference of fried garlic flake under different conditions was carried out and the scores for various sensory characteristics were surveyed. According to the physicochemical measurements and sensory evaluation, we confirmed that the optimum manufacturing condition of fried garlic flake was 1.5 mm thick at a temperature of $160{\sim}170^{\circ}C$.

폐무연솔더(Sn-Ag-Cu)의 전해재활용 시 주석과 은의 전기화학적 거동 연구 (Electrochemical Behavior of Tin and Silver during the Electrorecycling of Pb-free Solder (Sn-Ag-Cu) Waste)

  • 김민석;이재천;김리나;정경우
    • 자원리싸이클링
    • /
    • 제31권3호
    • /
    • pp.61-72
    • /
    • 2022
  • 주요성분이 Sn(93.0 %)-Ag(3.26 %)-Cu(0.89 %)로 구성되는 SAC 폐무연솔더로부터 주석과 은을 회수하기 위한 전기화학적인 방법을 연구하였다. 폐무연솔더의 건식용해, 주조를 통해 제조한 작업전극을 사용하여 분극거동 조사와 정전류 전해용해를 실시하였다. 분극시험 시 활성화영역의 산화전류피크는 전해액의 황산 농도가 높아질수록 감소하였으며, 1 molL-1 황산농도가 전해용해를 위해 가장 적절한 것으로 나타났다. 정전류 용해 시 전극표면의 부동태층인 양극슬라임이 두꺼워짐에 따라 전극전위가 지속적으로 높아졌으며, 10 mAcm-2에서 25시간동안 지속적인 전해용해가 가능한 반면 50 mAcm-2에서는 2.5 시간 이후부터 전극전위가 급상승하여 전해용해반응이 중단되었다. 정전류 전해용해 시 은은 양극슬라임에 농축되었으며, 전해액내 염소이온의 농도가 0.3 molL-1인 경우 농축율이 미첨가 조건보다 12.7% 높은 94.3%를 나타내었다. 또한 염소이온의 첨가에 의해 전해액내 주석이온의 안정성을 높이고 주석의 전착전류효율을 향상시킬 수 있었다.

Proving the Evolution of Relativistic Jet of Radio-Loud AGN, OVV 1633+382

  • Ro, Hyunwook;Sohn, Bong Won;Chung, Aeree;Krichbaum, Thomas P.
    • 천문학회보
    • /
    • 제40권2호
    • /
    • pp.37.1-37.1
    • /
    • 2015
  • It is suggested that relativistic jets associated with active galactic nuclei (AGNs) can have great impacts on the evolution of the host galaxy. However, the physical properties of AGN jets including the formation mechanism are not well known to date, and hence the AGN feedback on the host galaxy is yet poorly understood. OVV 1633+382 as a highly variable AGN source (a.k.a. blazer) with a compact core and very well developed jet components is an excellent laboratory to study the jet formation mechanism of radio-loud AGN. Near 2002, a major flare was reported at mm wavelength with a dramatic increase of the flux, which is likely to be followed by a dense and bright outflow. In order to probe the evolution of the innermost region of this radio-loud AGN, we have monitored using the Very Large Baseline Array (VLBA) and the Effelsberg 100m single-dish radio telescope in 12 epochs from 2002 and 2005. The observations were conducted at 22, 43 and 86 GHz in full polarization mode. In this work, we present the intensity and spectral index maps at 22 and 43 GHz from our monitoring observations. We probe the kinematics and geometry of individual jet components to discuss the evolution of the jet.

  • PDF

A Comparison of Signal Processing Techniques in Optical Current Sensor for GIS

  • Kim, Young-Min;Park, Jung-Hwan;Jee, Seung-Wook;Lee, Kwang-Sik;Kim, Jung-Bae;Park, Won-Zoo
    • 조명전기설비학회논문지
    • /
    • 제20권9호
    • /
    • pp.103-109
    • /
    • 2006
  • This research is contents about output characteristic of optic current sensor that use faraday effect. optic current sensor used in an experiment is consisted of three parts.(1) Source of light used laser diode of 1310[nm].(2) Sensor section manufactured circularly according to gas insulated switchgear. And $9/125[{\mu}m]$ standard single mode optical fiber for communication was installed winding 20 [turn] on sensor section core surroundings of diameter 31 [cm].(3) Electrical signal of PD(Photo detector) is collected using NI company's 16bit DAQ board via terminal block. Collected data analyzed by different three signal processing methods. NI company's $Labview^{TM}$ was used to signal processing software. As a result, In signal processing of optic current sensor, we could know that noise greatly more influences the error generation than fluctuation of light intensity. also, 1 class CT(current transformer) manufacture that have error rate less than 1[%] was available by removing these

$C_{22}$-quinolinium(TCNQ) langmuir-blodgett 박막의 열처리 온도에 따른 광학적 및 유전특성 (Optical and electrical properties of $C_{22}$-quinolinium(TCNQ) langmuir-glodgett films depending on the annealing temperatures)

  • 홍언식;유덕선;김태완
    • E2M - 전기 전자와 첨단 소재
    • /
    • 제8권4호
    • /
    • pp.458-463
    • /
    • 1995
  • The optical and electrical properties of $C_{22}$-Quinolinium(TCNQ) Langmuir-Blodgett films have been studied depending on the annealing temperatures. The optimal properties were investigated using UV/visible(300-800[nm]) absorption spectra and FTIR(Fourier-transformed- infrared) absorption measurements. The electrical properties were investigated in a frequency range of 10[Hz]-13[MHz]. The UV/visible absorption spectra at room temperature show that there are four characteristic peaks at 320, 380, 494 and 678[nm]. These absorption peaks decrease very rapidly above the annealing temperature of 180[.deg. C], which is due to a structural change of TCNQ. The FTIR absorption measurements strongly support the result of the UV/visible absorption spectra, because the absorption peak of TCNQ- at 2181[$cm^{-1}$ /] also decreases above 140[.deg. C]. The frequency-dependent dielectric constant shows that there is a dielectric dispersion near 1[MHz] which is due to an orientational polarization of the molecules inside the film. The overall frequency-dependent dielectric constant is higher near 80[.deg. C]. It may be due to a softness of the alkyl chains.s.

  • PDF

스크린 프린팅으로 제작된 $Pb(Zr,\;Ti)O_3$ 후막의 제작과 전기적 특성 (Preparation and Electrical Properties of Lead Zirconate Titanate Thick Films Fabricated by Screen-Printing Method)

  • 박상만;이성갑
    • 대한전기학회논문지:전기물성ㆍ응용부문C
    • /
    • 제55권9호
    • /
    • pp.429-433
    • /
    • 2006
  • PZT(80/0) powder was prepared by a sol-gel method and PZT thick films were fabricated by the screen-printing method on the alumina substrates. The coating and drying procedure was repeated 4 times. And then the PZT(20/80) precusor solution was spin-coated on the PZT thick films. A concentration of a coating solution was 0.5mol/L and the number of coating was varied from 0 to 6. The porosity decreased and the grain size increased with increasing the number of coatings. The thickness of the PZT-6(6: number of coatings) films was about $60{\mu}m$. The relative dielectric constant increased and the dielectric loss decreased with increasing the number of PZT(20/80) sol coatings. The relative dielectric constant and dielectric loss of the PZT-6 thick film were 275 and 3.5%, respectively. The remanent polarization, coercive field and breakdown strength of the PZT-6 film were $19.8{\mu}C/cm^2$, 13.7kV/cm and 130kV/cm, respectively.

Bioavailability of Digoxin Tablets in Healthy Volunteers

  • Lee, Chi-Ho;Park, Yun-Ju;Charies-D. Sands;Daniel-W. Jones;John-M. Trang
    • Archives of Pharmacal Research
    • /
    • 제17권2호
    • /
    • pp.80-86
    • /
    • 1994
  • The bioavailability of digoxin generic tablets manufactures in Korea (formulations A & B) wwere compared to a standard (formulation C; Lanoxin brand digoxin, Burroughs Wellcome, USA) in 12 healthy Korean male volunteers (mean age 31.4 years) in a single dose, randomized, complete block crossover study. Using a latin square design, each of the subjects was randomized to the order number and allocated to each of the three treatments of 0.5mg oral digoxin. Digoxin conc4ntrations in serum and urine samples collected for 48 hours after dosing were measured by fluoprescence polarization immunoassy and radioimmunoassy, respectively. Treatments were compared by using nonlinear least squares regession analysis to evaluate the following pharmacokinetic parameters : maximum serum concentation $(C_{max})$; time of maximum serum concentation $(T_{max})$; area under the serum concentration-time curve $AUC_{0-12}$, $C_{max}$\;and\;(AUC_{0-12})$; and cummulative urinary excretion for 0-48 hours $(CLE_{0-48}.\;Mean\;AUC_{0-12},\;C_{max},\;and\;CUE_{0-48}$ values for formulations B and C were significantly different from formulation A (P<0.001), but not significantly diffeerent form each other. Basede on $AUL_{0-12}\;and\;CUE_{0-48}$ respectively, the relative availability of formulation B was 87.5% and 89.6% and the relative availability of formultation A was 43% and 35% when compared to formulation C(the standard).

  • PDF

질소 이온이 주입된 STS 316L 스테인리스 강에서의 상변화와 집합조직이 내식성에 미치는 영향 (Influence of Phase Evolution and Texture on the Corrosion Resistance of Nitrogen Ion Implanted STS 316L Stainless Steel)

  • 전신희;공영민
    • 한국재료학회지
    • /
    • 제25권6호
    • /
    • pp.293-299
    • /
    • 2015
  • In this study, nitrogen ions were implanted into STS 316L austenitic stainless steel by plasma immersion ion implantation (PIII) to improve the corrosion resistance. The implantation of nitrogen ions was performed with bias voltages of -5, -10, -15, and -20 kV. The implantation time was 240 min and the implantation temperature was kept at room temperature. With nitrogen implantation, the corrosion resistance of 316 L improved in comparison with that of the bare steel. The effects of nitrogen ion implantation on the electrochemical corrosion behavior of the specimen were investigated by the potentiodynamic polarization test, which was conducted in a 0.5 M $H_2SO_4$ solution at $70^{\circ}C$. The phase evolution and texture caused by the nitrogen ion implantation were analyzed by an X-ray diffractometer. It was demonstrated that the samples implanted at lower bias voltages, i.e., 5 kV and 10 kV, showed an expanded austenite phase, ${\gamma}_N$, and strong (111) texture morphology. Those samples exhibited a better corrosion resistance.

마이크로캡슐화한 축전지용 수소저장합금 전극의 충·방전 특성 (Charge and Discharge Characteristics of Microencapsulated Hydrogen Storage Alloy Electrodes for Secondary Batteries)

  • 최성수;최병진;예병준;김대룡
    • 한국수소및신에너지학회논문집
    • /
    • 제3권2호
    • /
    • pp.45-54
    • /
    • 1992
  • An applicability microencapsulation, using electroless copper plating, of hydrogen storage alloy powder as an anode material for nickel-hydrogen secondary batteries was investigated. Alloys employed were $LaNi_{4.7}Al_{0.3}$ and $MmNi_{4.5}Al_{0.5}$(Mm=mischmetal) which have an appropriate equilibrium pressure and capacity. The microencapsulation of the alloy powder was found to accelerate initial activation of electrodes and to increase capacity which is about 285mAh/g for $LaNi_{4.7}Al_{0.3}$. In addition, other charge and discharge characteristics, such as polarization and flatness of charge and discharge potential, were improved due to the role of copper layer as a microcurrent collector and an oxidation barrier of the alloy powder. $MmNi_{4.5}Al_{0.5}$ alloy showed lower capacity than $LaNi_{4.7}Al_{0.3}$ because of higher equilibrium pressure. Cyclic characteristics of both alloys were somewhat poor because of mainly shedding and partial oxidation of alloy powder during the cycling. However, it was considered that the microencapsulation method is effective to improve the performances of the hydrogen storage alloy electrodes.

  • PDF