• Title/Summary/Keyword: Low temperature aging

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Comparison of Hardness and Damping Capacities of Mg-Al Alloy Subjected to T6 Heat Treatment and Low Temperature Long Term Isothermal Aging (T6 열처리 및 저온 장시간 등온 시효한 Mg-Al 합금의 경도 및 진동감쇠능 비교)

  • Joong-Hwan Jun
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.5
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    • pp.277-284
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    • 2023
  • Hardness and damping characteristics of fine discontinuous precipitates (DPs) microstructure generated by low temperature long term isothermal aging were investigated in comparison with those of T6 heat-treated microstructure composed of DPs and continuous precipitates (CPs) in Mg-9%Al alloy. In this study, T6 and fine DPs microstructures were obtained by isothermal aging at 453 K for 24 h and at 413 K for 336 h, respectively, after solution treatment at 693 K for 24 h. The DPs microstructure exhibited higher hardness than the T6 microstructure, which is related to the lower (α + β) interlamellar spacing of the DPs. The DPs microstructure possessed better damping capacity than the T6 microstructure in the strain-amplitude independent region, whereas in the strain-amplitude dependent region, the reverse behavior was observed. The damping tendencies depending on strain-amplitude were discussed based on the microstructural features of the T6 and DPs microstructures.

The effects of socioeconomic factors on mortality under high temperature in Seoul, South Korea (서울의 사회·경제적 요인이 고온 현상 발생 시 사망자에 미치는 영향)

  • Lee, Jisu;Kim, Man-Kyu;Park, Jongchul
    • Journal of the Korean association of regional geographers
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    • v.22 no.1
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    • pp.195-210
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    • 2016
  • The purpose of this study was to understand characteristics of groups vulnerable to extreme heat and to reduce mortality caused by high temperature. For this purpose, relationship between socioeconomic factors and mortality-threshold temperatures were studied. The study area was limited to Seoul (South Korea) and climate data from 2000 to 2010 was used. Our results indicate that mortality-threshold temperatures for regions with a high proportion of aging population and a low proportion of aging population are $27.6^{\circ}C$ and $27.9^{\circ}C$, respectively. It was also found that a relative size of welfare dependant population did not affect mortality-threshold temperatures. However, regions with a high proportion of aging and welfare dependant population experienced $0.7^{\circ}C$ lower mortality-threshold temperature than other regions. This implies that low income and older people in Seoul are more easily affected by high temperature. Thus, this study suggests that it needs a policy targeted to low income and aging population to decrease mortality rate caused by extreme heat.

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Effect of $Ta_2O_5$ Alloying on Low Temperature Degradation of 3 mol% Y-TZP ($Ta_2O_5$ 첨가가 3 mol% Y-TZP의 저온열화에 미치는 영향)

  • 김대준;최두진
    • Journal of the Korean Ceramic Society
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    • v.29 no.8
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    • pp.630-638
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    • 1992
  • Ta2O5 alloying into 3 mol% Y2O3-stabilized tetragonal ZrO2 polycrystals (3Y-TZP) increased the degradation during aging at 265℃ and the fracture toughness; both are determined by the amount of transformed m-ZrO2. It was proposed that the mechanism underlying the t→m transformation when aged at low temperatures is attributed to the reorientation of (Zzr'V ). complexes parallel to [111] lattice direction, which is accompanied by a relaxation of TZP lattice during annealing at low temperature. A small strain which results from the reorientation gives rise to a localized mechanical instability, thus lowering the nucleation barrier so that the t→m phase transformation (degradation) proceeds. The amount of transformed m-ZrO2 during aging becomes greater as the chemical free energy change related to the transformation, ΔGo, increases with increasing the Ta2O5 alloying content.

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Effects of Accelerated Iso-Thermal Aging on Elastic-Plastic Fracture Toughness and Fracture Resistance Curve by Unloading Compliance Method in SA533B Low Alloy Steel (제하 컴플라이언스법에 의한 SA533B강의 $J_1C$ 및 J-R 곡선에 미치는 열시효 영향)

  • 윤한기;차귀준
    • Journal of Ocean Engineering and Technology
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    • v.8 no.2
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    • pp.157-165
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    • 1994
  • Effect of an accelerated iso-thermal aging (375 degree C x 66days, 375 degree C x 200days) on elastic-plastic fracture resistance curve were examined in SA533B low alloy steel. Fracture toughness test are conducted by unloading compliance method at room temperature. But the apparent negative crack growth phenomenon, usually arise in partial unloading compliance test. The phenomenon of negative crack growth may be eliminated by the offset technique. There is no effect of aging on J sub(IC) and dJ/da in iso-thermal aged (375 degree C x 66 days) specimen, but there is very little effect in iso-thermal aged (375 degree C x 200 days) specimen.

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Measurement of CTE Change in a Composite Laminate with Aging under Space Environment using Fiber Optic Sensors (광섬유센서를 이용한 우주환경하에서 복합재료 적층시편의 노화에 따른 열팽창계수변화 측정)

  • Gang,Sang-Guk;Gang,Dong-Hun;Kim,Cheon-Gon;Hong,Chang-Seon
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.31 no.10
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    • pp.21-26
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    • 2003
  • In this research, the change of coefficient of thermal expansion (CTE) of graphite/epoxy composite laminate under space environment was measured using fiber optic sensors. Two fiber Bragg grating (FBG) sensors have been adopted for the simultaneous measurement of thermal strain and temperature. Low Earth Orbit (LEO) conditions with high vacuum, ultraviolet and thermal cycling environments were simulated in a thermal vacuum chamber. As a pre-test, a FBG temperature sensor was calibrated and a FBG strain sensor was verified through the comparison with the electric strain gauge (ESG) attached on an aluminun specimen at high and low temperature respectively. The change of the CTE in a composite laminate exposed to space environment was measured for intervals of aging cycles in real time. As a whole, there was no abrupt change of the CTE after 1000 aging cycles. After aging, however, the CTE decreased a Little all over the test temperature range. These changes are caused by outgassing, moisture desorption, matrix cracking etc.

Low Temperature δ-Precipitation of Inconel 718 Alloy Wire during Cold Drawing (인코넬 718합금 선재의 냉간 인발시 δ 상 저온 석출 현상 연구)

  • Park, Jae Man;Kim, Yong Hwan;Jang, Heui Un;Chung, Won Sub
    • Korean Journal of Metals and Materials
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    • v.50 no.7
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    • pp.511-516
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    • 2012
  • Low temperature ${\delta}$-precipitation phenomenon below 2-step aging ($718^{\circ}C$, $8hr+621^{\circ}C$, 8 hr) temperature of cold drawn Inconel 718 alloy wire was investigated. The investigation was carried out on wires with a cold drawn ratio of 0, 20, 50 and 70% using OM, SEM, XRD, TEM, and DSC. In microstructures of 50 and 70% drawn wire, many precipitates were found along the grain boundaries and the twin boundaries in deformation band. From the results of the XRD and TEM analysis, the precipitates were identified as plate-like ${\delta}$-phase. From the results of the DSC analysis, it was also found that a temperature of ${\delta}$-precipitation decreases with an increase of the cold drawn ratio. We concluded that cold drawing of inconel 718 wire promotes the ${\delta}$-precipitation, and under the condition of a high drawing ratio, the ${\delta}$-phase could be precipitated at a temperature below the aging temperature ($718^{\circ}C$).

Quality improvement and aging effect of beef by low-temperature treatment of non-preferred parts of beef (비선호 부위 소고기의 저온처리에 의한 품질향상 및 소고기의 숙성효과)

  • Hyun Kyoung Kim;Soon Cheol Kim;Hyeon Jin Kim;Yeong Mi Kim
    • The Journal of the Convergence on Culture Technology
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    • v.9 no.5
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    • pp.753-760
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    • 2023
  • In this study, quality improvement of beef was attempted according to the low temperature treatment and aging period of grade 1 compared to grade 1++ beef. The fat content and shear force of beef grade 1++ were 13.03% and 114.26N, but beef grade 1 was 3.21% and 149.67N. Meanwhile, after low-temperature treatment of grade 1 beef at -26℃ for 12 hours and low-temperature aging at 0 ℃ for 14 days, the shear force was greatly reduced to 87.85N, improving overall preference, softness, dripping gravy, flavor, and chewing texture. The essential free amino acid content was as low as 22.17mg/100g in grade 1++ beef, but the contents were high at 41.31~45.11mg/100g in three samples of grade 1, and there was no change in content according to cold treatment conditions. As a specific component of beef, Taurine was 30.94~34.41mg/100g, and the difference in content was small according to beef grade, but Anserine and Creatine were low at 19.68mg/100g and 70.01mg/100g in beef grade 1++ and high at 26.38~31.23mg/100g and 154.09~167.26mg/10g in beef grade 1. The content ratio of oleic acid (c18:1)/stearic acid (c18:0) as an monounsaturated fatty acid/saturated fatty acid ratio was low at 5.29 for grade 1++ beef, but high at 6.13~6.78 for grade 1 beef. In addition, there was no trend in the content ratio of these fatty acids according to the low-temperature treatment conditions and aging period in beef grade 1. As a result of this study, it was possible to improve the quality of beef grade 1 by low-temperature treatment at -26 ℃ for 12 hours and then aging at 0 ℃ for 14 days.

Study about decreasing methods of printing ink solvents residue amounts on plastic food package materials (플라스틱 포장재의 잔존 인쇄 용제 감소 방안)

  • An, Duek-Jun;Cho, Hoon-Il
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.10 no.1
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    • pp.1-6
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    • 2004
  • Amount of residual ink solvent on the packaging materials from Korea, Japan and Europe was measured and compared. The amount of packaging materials from Korea was much higher than that of Japan and Europe. To reduce the residual amounts of ink solvent, aging condition of printed packaging materials including aging time and temperature was modified and evaluated. Aging with high temperature and short time ($60^{\circ}C$ and 24 hours) was more effective for reduction of residual amount of ink solvent than that with low temperature and long time. To find out change of reduction pattern of residual amount of solvent according to plastic packaging material, several monolayer and multilayer packaging materials were selected. Among the monolayer packaging materials, the amount of EVOH and PET was lower than that of polyolefin plastic film including PE and PP. PP/EVOH/PET among the selected multilayer film showed the lowest amount of residual ink solvent on food packaging materials. Result of this research revealed that the residual amount of ink solvent can be reduced by proper selection of aging condition with and by appropriate application of mutilayer plastic film.

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A Study on the Stabilization Effects of 1-Chlorobutadiene-Butadiene Copolymer by Triazine Thiol Derivative (Triazine Thiol 유도체(誘導體)에 의한 1-Chlorobutadiene-Butadiene Copolymer의 안정화효과(安定化效果)에 관한 연구(硏究))

  • Yoo, Chong-Sun;Yamashita, S.;Paik, Nam-Chul
    • Elastomers and Composites
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    • v.22 no.2
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    • pp.109-120
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    • 1987
  • In this study, as one of the developing ways of the functional elastomer, improvement of the functionality of CB-BR was attemped through stabilization. At first the stabilization effect of CB-BR and the concentration dependancy in CB-BR were determined. Then, triazine thiol derivative(BPTT) was synthesized by reacting p-aminodiphenylamine with cyanuric chloride. Further the functional mechanism and the effects of the antioxidants were investigated using BPTT together with other various antioxidants in liquid and solid states. The results obtained are as follows: 1) The aging of CB-BR depended on the concentration and temperature. Thus, at a low temperature of $50^{\circ}C$, the aging proceeded with gel formation; at high temperature above $100^{\circ}C$ and in above 4wt% concentration, the aging occured by the formation of gel. And in concentrations below that, the aging proceeds with a decomposition caused by oxygen attacked to elastomer molecules. 2) The effect of antioxidation of CB-BR in the liquid state was at it's best when the MBIZ and BPTT were used at $110^{\circ}C$, 4hrs after the oxidation. 3) The effect of antioxidation of CB-BR in the solid state was the best choice the simultaneous use of NDBC and BPTT at $50^{\circ}C$, 30days after the oxidation.

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Aging Behavior and Effect of Heat Treatment on High Temperature Mechanical Properties in Ti-15V-3AI-3Cr-3Sn (Ti-15V-3Al합금의 시효거동과 열처리에 따른 고온 기계적 특성)

  • Lee Jae Won;Lee Back-Hee;Lee Kyu Hwan;Kim Young Do
    • Korean Journal of Materials Research
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    • v.14 no.1
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    • pp.13-18
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    • 2004
  • Titanium alloys are the one of promising candidate materials for medium high temperature parts in the aircraft, automobile, petrochemistry and electrochemistry because of their high strength with low density in medium high temperature. In this study, the effects of aging and heat treatments on the mechanical properties of Ti-15-3 alloy in medium high temperature, which was $400^{\circ}C$, were studied. Solid solution treatment was performed at $8000^{\circ}C$ of $\beta$ phase region for 1 h and the alloy was quenched in water. The alloy was aged at $5000^{\circ}C$ of $\alpha$ and $\beta$ two-phase region for 1, 2, 4, 8, ... and 100 h to increase the mechanical property. The $\beta$ single phase was observed at all parts of specimens in Ti-15-3 alloy after ST. As the aging at $500^{\circ}C$, fine precipitates of a phase was generated from matrix of $\beta$ phase and the microstructure was consisted of weaving structure such as Widmanstiitten a phase. The most suitable aging time is 24h in$ 400^{\circ}C$. At this time, strength is 1164 MPa and elongation is about 12%. In room temperature, elongation of Ti-15-3 alloy aged at $500^{\circ}C$ for 16 h is poor (=3%) in spite of high tensile strength (1458 MPa).