• Journal of Korean Society of Occupational and Environmental Hygiene
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• v.23 no.4
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• pp.333-340
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• 2013

Objectives: This study was designed to establish an accurate analytical method for asbestos in a biological sample for determining occupational asbestos-related diseases and relief of the health effects of environmental asbestos. Methods: Biological samples were obtained from lungs of rats following intratracheal instillation of asbestos(Chrysotile, anthophyllite) and were prepared according to digestion method(Wet digestion, high temperature ashing, low temperature ashing). The samples were then analyzed for asbestos fibers using a transmission electron microscope equipped with an energy dispersive X-ray spectrometer. Results: Low temperature plasma ashing removed more of the organic components and reduced fiber loss compared to the wet digestion method, making specimens so prepared more suitable for transmission electron microsocpy. Conclusions: The low temperature ashing technique is the most accurate method for analyzing asbestos in biological samples.

• Journal of electromagnetic engineering and science
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• v.17 no.4
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• pp.191-196
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• 2017

Microwave wireless power transmission (MWPT) is a promising technique for low and medium power applications such as wireless charging for sensor network or for biomedical chips in case with long ranges or in dispersive media such. A key factor of the MWPT technique is its efficiency, which includes the wireless power transmission efficiency and the radio frequency (RF) to direct current (DC) voltage efficiency of RF-DC converter (which transforms RF energy to DC supply voltage). The main problem in designing an RF-DC converter is the nonlinear characteristic of Schottky diodes; this characteristic causes low efficiency, higher harmonics frequency and a change in the input impedance value when the RF input power changes. In this paper, rather than using harmonic termination techniques of class E or class F power amplifiers, which are usually used to improve the efficiency of RF-DC converters, we propose a new method called "optimal input impedance" to enhance the performance of our design. The results of simulations and measurements are presented in this paper along with a discussion of our design concerning its practical applications.

• Journal of Electrochemical Science and Technology
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• v.4 no.1
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• pp.41-45
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• 2013

Platinum is a well known element which shows a significant electrocatalytic activity in many important applications. In glucose sensor, because of the poisoning effect of reaction intermediates and the low surface area, the electrocatalytic activity towards the glucose oxidation is low which cause the low sensitivity. So, we fabricate a nanoporous PtZn alloy electrode by deposition-dissolution method. It provides a high active surface and a large enzyme encapsulating space per unit area when it used for an enzymatic glucose sensor. Glucose oxidase was immobilized on the electrode surface by capping with PEDOT composite and PPDA. The composite and PPDA also can exclude the interference ion such as ascorbic acid and uric acid to improve the selectivity. The surface area was determined by cyclic voltametry method and the surface structure and the element were analyzed by Scanning Electron Microscope (SEM) and Energy Dispersive X-ray spectroscopy (EDX), respectively. The sensitivity is $13.5{\mu}A/mM\;cm^2$. It is a remarkable value with such simply prepared senor has high selectivity.

• Korean Journal of Metals and Materials
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• v.49 no.11
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• pp.905-909
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• 2011

The formation of front metal contact silicon solar cells is required for low cost, low contact resistance to silicon surfaces. One of the available front metal contacts is Ni/Cu plating, which can be mass produced via asimple and inexpensive process. A selective emitter, meanwhile, involves two different doping levels, with higher doping (${\leq}30{\Omega}/sq$) underneath the grid to achieve good ohmic contact and low doping between the grid in order to minimize the heavy doping effect in the emitter. This study describes the formation of a selective emitter and a nickel silicide seed layer for the front metallization of silicon cells. The contacts were thickened by a plated Ni/Cu two-step metallization process on front contacts. The experimental results showed that the Ni layer via SEM (Scanning Electron Microscopy) and EDX (Energy dispersive X-ray spectroscopy) analyses. Finally, a plated Ni/Cu contact solar cell displayed efficiency of 18.10% on a $2{\times}2cm^2$, Cz wafer.

• Nuclear Engineering and Technology
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• v.40 no.3
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• pp.225-232
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• 2008

To understand the effect of the cyclic strain rate on the environmentally assisted cracking behaviors of SA508 Gr.1a low alloy steel in deoxygenated water at $310^{\circ}C$, the fatigue surface and a sectioned area of specimens were observed after low cycle fatigue tests. On the fatigue surface of the specimen tested at a strain rate of 0.008 %/s, unclear ductile striations and a blunt crack tip were observed. Therefore, metal dissolution could be the main cracking mechanism of the material at this strain rate. On the other hand, on the fatigue surfaces of the specimens tested at strain rates of 0.04 and 0.4 %/s, brittle cracks and flat facets, which are evidences of the hydrogen induced cracking, were observed. In addition, a tendency of linkage between the main crack and the micro-cracks was observed on the sectioned area. Therefore, at higher strain rates, the main cracking mechanism could be hydrogen induced cracking. Additionally, evidence of the dissolved MnS inclusions was observed on the fatigue surface from energy dispersive x-ray spectrometer analyses. Thus, despite the low sulfur content of the test material, the sulfides seem to contribute to environmentally assisted cracking of SA508 Gr.1a low alloy steel in deoxygenated water at $310^{\circ}C$.

• Journal of the Korean Geotechnical Society
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• v.18 no.6
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• pp.129-139
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• 2002

Dielectric constant measurement has drawn much attention in the investigation of the properties and contaminations of subsurface. In this study, by varying the frequency from 75 kHz to 12 MHz, dielectric constant was measured for the weathered granite soil and Jumunjin sand having different water contents and dry density. The dielectric constant of sand showed the dispersive behavior indicating that dielectric constant decreased with frequency of an electric field. And the dielectric constant of soil increased as water content and/or dry density increased due to the decrease of air portion and/or the increase of amount of water molecules which could contribute to the development of orientation polarization. The dielectric constant of sand showed a linear relationship with the moisture density, considering both water content and dry density. At low frequency, the dielectric constants calculated by Maxwell's, Topp's and CRIM equation deviated from measured values. It could be explained by the fact that those equations did not consider dispersive behavior of dielectric constant with the frequency.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.29 no.12C
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• pp.1606-1616
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• 2004

This paper introduces a technique for generating an appropriate template signal via modeling of minimum-phase stable ARMA (Auto-Regressive Moving Average) system for coherent impulse communication systems. It has been well known that the transmitted impulse signal becomes deformed because of dispersive and resonant characteristics. Accordingly, in spite of using ideal template signal at the correlator, these impairments degrade overall performance attributed to low level of coherence. To increase the degree of coherence, our proposed scheme realizes A3U system derived by Gaussian pulse signal, which simulates the overall characteristic of transfer function in between transmit and receive wideband antennas so as to generate an appropriate template signal in a form of output. The performance of proposed scheme will be shown in results from computer simulations to verify its affirmative impact on impulse communication system with regarding several distinctively shaped antennas.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2007.11a
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• pp.53-53
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• 2007

반도체 소자의 고집적화, 미세화 화로 인해 반도체의 동작속도를 증가시키기 위하여 Cu를 이용한 금속배선이 주목받게 되었으나, 높은 압력으로 인한 보은 Cu 영역에서 과잉 디슁 현상과 에로젼을 유도하고 반도체 웨이퍼위의 low-k 물질에 손상을 줌에 따라 메탈라인 브리징과 단락을 초래할 있어, Cu의 단락인 islands를 남김으로서 표면 결항을 제거하지 못한다는 단점을 가지고 있었다. 그래서 이러한 문제점을 해결하기 위하여 기존의 CMP에 전기화학을 결합시킴으로서 낮은 하력에서의 Cu평탄화를 달성할 수 있는 ECMP (electrochemical mechanical polishing)기술이 필요하게 되었다. 따라서 본 논문에서는 전기화학적 기계적 연마(ECMP)작용을 위해, I-V 특성 곡선을 이용하여 패시베이션 막의 active, passive, transient, trans-passive영역의 전기화학적 특성을 비교 분석하였으며, Cu막의 표면 형상을 알아보기 위해 scanning electron microscopy (SEM) 측정과 energy dispersive spectroscopy (EDS)와 X-ray Diffraction (XRD) 분석을 통해 금속 화학적 조성을 조사하였다.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.14 no.4
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• pp.401-412
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• 2003

In this paper, a broadband phase shifter structure using a new switched network was proposed. A new reference network is composed of coupled lines and 45$^{\circ}$open and short stubs, which are shunted at the edge points of a main line, respectively, A delay network is composed of only a standard transmission line. It is possible to design a broadband 180$^{\circ}$phase shifter that phase dispersive characteristics by an impedance ratio R of coupled lines and greater phase dispersive characteristics by characteristic impedances Zm, Zs of a main line and stubs are used together. By considering a structure symmetry, the even and odd mode analysis was performed to obtain theoretical S-parameters of the proposed phase shifter. Also, through computer simulation on the basis of derived equations, design graphs were presented to optimally design a 180$^{\circ}$broadband phase shifter. Design graphs provide the values of characteristic impedances Zm, Zs, and I/O match and phase bandwidths. To verify electrical performances of the broadband phase shifter proposed in this paper, low different 180$^{\circ}$phase shifters, operated at the center frequency 3 GHz were designed and fabricated using design graphs, and were experimented. One of them was designed as a standard Schiffman structure to compare with electrical performances. Measured results of each phase shifter to satisfy simultaneously design conditions of I/O match （VSWR=1.15:1) and maximum phase deviation $({\varepsilon}_{{\Delta}{\phi}}＝{\pm}2^{\circ})$ were well in agreement with corresponding simulation results over impedance match and phase error bandwidths, and showed broadband characteristics.

• Advances in nano research
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• v.1 no.4
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• pp.211-218
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• 2013

A low-cost, green and reproducible citric acid assisted synthesis of nanocrystalline $Al_{0.5}Ag_{0.5}TiO_3$ (n-AAT) powder is reported. X-ray, FTIR, energy dispersive X-ray, transmission electron microscopy and scanning electron microscopy analyses are performed to ascertain the formation of n-AAT. X-ray diffraction data analysis indicated the formation of monoclinic structure. Spherical shaped particles having the sizes of 3-15 nm are found. The mechanism of nano-transformation for the soft-chemical synthesis of n-AAT has been explained using simple organic chemistry rules and nucleation and growth theory. Dielectric study revealed that AAT ceramic might be a suitable candidate for capacitor applications.