• Title/Summary/Keyword: Lock-in amplifier

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고자장, 저온 환경의 UHV surface magneto-optical Kerr effect 장비 구축 및 Fe/Cr(001)계의 자성특성 연구

  • Park, Yong-Seong;O, Yong-Rok;Hong, Ji-Sang;Kim, Won-Dong;Hwang, Chan-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.400-400
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    • 2010
  • 우리는 기본 진공 $10^{-11}\;Torr$의 UHV surface magneto-optical Kerr effect (SMOKE) 시스템을 quarter-wave plate를 사용하였던 기존의 방식에서 PEM (photo elastic modulator)를 사용하는 방식으로 장비의 기능을 향상시켰다. 기존 quarter-wave plate를 사용하는 방식의 경우 Kerr signal을 구하기 위해 편광자와 검광자를 수직으로 두어 광량을 0으로 만들어야 한다. 그러나 금속의 경우 대부분 가시광선 영역에서 큰 반사율 때문에 측정되는 광량이 편광자와 검광자를 거치면서 넓은 각도 범위에서 최소값을 갖기 때문에 정확한 영점을 잡는 데 한계가 있다. 이러한 단점을 해결하기 위하여 우리는 PEM을 이용한 위상변조방식을 사용하였다. 위상변조 방식은 Kerr signal과 관계된 양을 PEM을 이용하여 50 kH ($1{\omega}$)와 100 kH ($2{\omega}$)의 진동 주파수에 공조시키고 이를 Lock-in-amplifier를 사용하여 탐지하기 때문에 좋은 sensitivity를 얻을 수 있을 뿐 아니라 Kerr ellipticity와 Kerr rotation을 동시에 측정할 수 있다. 자화에 필요한 전자석은 순철로 된 코어를 제작하여 챔버에 부착하였고 10 A에서 최대 7 kOe의 고자장을 얻을 수 있어 포화자화가 큰 물질에 대해서도 필요한 자성영역까지 측정이 가능하게 하였다. 또 저온 측정을 위해 SMOKE 샘플 홀더를 개조하여 액체 질소를 이용하여 100 K 근방의 영역에서 온도를 제어할 수 있도록 저온 장치를 구성하였다. 여기에서 샘플 근처에 위차한 e-beam heater가 장착된 고온 부분과 액체 질소 냉각, 온도감지를 위한 센서, cartridge heater가 장착된 저온 부분을 sapphire plate로 분리하여 저온용 cartridge heater의 파손을 최소화하였다. 이러한 SMOKE 시스템을 구성한 후에 우리는 Fe/Cr(001)시스템의 자성특성에 대해 연구하였다. Fe/Cr 시스템은 Fe/Cr/Fe의 exchange coupling이나 bulk Cr의 복잡한 자성 특성 때문에 주목을 받아왔다. 이 연구에서 우리는 저온 및 상온에서 Cr(001) 단결정 위에 증착된 Fe 박막의 자성 특성을 보고한다.

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A Study on the Method for the Local Transmittance Measurements of the Ocular Lens (안경 렌즈의 국소적 투과율 측정을 위한 방법에 관한 연구)

  • Park, Sang-Kook;Ri, Hyeong-Cheol;Youk, Do-Jin;Sung, Duk-Yong;Kang, Sung-Soo
    • Journal of Korean Ophthalmic Optics Society
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    • v.19 no.4
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    • pp.471-477
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    • 2014
  • Purpose: We have analyzed the transmittance distribution of the ocular lens using local transmittance microscope to investigate the optical homogeneity of the lens. Methods: The transmittance of the laser which is focused on the surface of the ocular lens was measured by using the photo-detector and lock-in amplifier and analyzed. Multi-coated, uncoated, and progressive lenses were analyzed. Results: In the measurement of the progressive lens and a physical stimulated lens, local transmittance microscopy analysis showed a high degree of match with the measurement results through the optical microscope. In addition, the average value of the transmittance is reduced and the standard deviation was increased in the presence of optical defects. In unstimulated lens, there are a large impact on transmittance whether the anti-reflective coating is presence or absence in both the local transmittance microscopy and general transmittance analysis. Conclusions: The distribution of the transmittance measured by local transmission microscopy were changed when the various stimulus is applied to the lenses. These analyzes by local transmission microscopy can be utilized as a way to evaluate or determine the uniformity of the coating film or lens.

Degradation Evaluation of Mechanical Properties for 12Cr Ferrite Heat Resisting Steel by Reversible Permeability (가역투자율에 의한 12Cr 페라이트 내열강의 역학적 물성의 열화평가)

  • Ryu, Kwon-Sang;Kim, Min-Gi;Nahm, Seung-Hoon;Kim, Chung-Seok
    • Journal of the Korean Society for Nondestructive Testing
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    • v.30 no.5
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    • pp.464-470
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    • 2010
  • The integrity of the industrial equipment in use under high temperature and high pressure must be assessed by regularly measuring the degraded mechanical properties during service time. In order to nondestructively monitor the degraded mechanical properties of industrial equipment, a measuring method of the reversible permeability(RP) using surface type probe is presented. The method for measuring the RP is based on that RP is the differential value of hysteresis loop. The RP is exactly the foundation hatmonics induced in a detecting coil measured by lock-in amplifier tuned to a frequency of the alternating perturbing magnetic field. The peak of RP is measured around the coercive force. Steel material used in this work was 12Cr ferritic heat resisting steel. The eleven kinds of samples aged during different times under same temperature ($700^{\circ}C$) were prepared. Peak interval of reversible permeability(PIRP), Vickers hardness, and tensile strength measured for the aged samples decreased abruptly for short aging time (below 500 h), but the change became small at a long aging time. Vickers hardness and tensile strength linearly decreased as RIRP decreased, so the degraded mechanical properties of 12Cr ferritic heat resisting steel could be nondestructively evaluated by measuring RIRP.

Nondestructive Evaluation of Remanent Life of Turbine Rotor Steel by Measuring Reversible Magnetic Permeability (가역투자율 측정에 의한 터빈로터강의 비파괴적 잔여수명 평가)

  • Ryu, Kwon-Sang;Nahm, Seung-Hoon;Kim, Yong-Il
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.4
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    • pp.315-321
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    • 2003
  • The integrity of the turbine rotors can be assessed by measuring the material properties at service temperature. In order to evaluate the remanent life of turbine rotor steel nondestructively, a measurement system of reversible magnetic permeability using an alternating perturbing magnetic field was constructed. We present a new non-destructive method to evaluate the remanent life of 1Cr-1Mo-0.25V steel using the value of reversible magnetic permeability. This method is based on the existence of reversible magnetic permeability in the differential magnetization around the coercive field strength. We measured the first harmonics voltage induced in a coil using a lock-in amplifier tuned to an exciting frequency. The Results of reversible magnetic Permeability and Wickers hardness on the aged samples show that the peak interval of reversible magnetic permeability (PIRMP) and Vickers hardness decreases as aging time increases. A softening curve is obtained from the correlation between Vickers hardness and the PIRMP. This curve can be used as a non-destructive method to evaluate the remanent life of turbine rotor steel.

Design of a CCM/DCM dual mode DC-DC Buck Converter with Capacitor Multiplier (커패시터 멀티플라이어를 갖는 CCM/DCM 이중모드 DC-DC 벅 컨버터의 설계)

  • Choi, Jin-Woong;Song, Han-Jung
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.9
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    • pp.21-26
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    • 2016
  • This paper presents a step-down DC-DC buck converter with a CCM/DCM dual-mode function for the internal power stage of portable electronic device. The proposed converter that is operated with a high frequency of 1 MHz consists of a power stage and a control block. The power stage has a power MOS transistor, inductor, capacitor, and feedback resistors for the control loop. The control part has a pulse width modulation (PWM) block, error amplifier, ramp generator, and oscillator. In this paper, an external capacitor for compensation has been replaced with a multiplier equivalent CMOS circuit for area reduction of integrated circuits. In addition, the circuit includes protection block, such as over voltage protection (OVP), under voltage lock out (UVLO), and thermal shutdown (TSD) block. The proposed circuit was designed and verified using a $0.18{\mu}m$ CMOS process parameter by Cadence Spectra circuit design program. The SPICE simulation results showed a peak efficiency of 94.8 %, a ripple voltage of 3.29 mV ripple, and a 1.8 V output voltage with supply voltages ranging from 2.7 to 3.3 V.

A Comparative Study on the Local Transmittance Homogeneity of the Ocular Lens (안경 렌즈의 국소적 투과율 균일도 비교 연구)

  • Park, Sang-Kook;Ri, Hyeong-Cheol;Jang, Yun-Seog;Sung, Duk-Yong;Kang, Sung-Soo
    • Journal of Korean Ophthalmic Optics Society
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    • v.20 no.4
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    • pp.471-476
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    • 2015
  • Purpose: We have analyzed the transmittance distribution of various ocular lenses using local transmittance microscope to investigate the optical homogeneity of the lens. Methods: The local transmittance of the laser which is focused on the surface of the spectacle lens was measured by using the photo-detector, lock-in amplifier and motorized-stage. 25 multi-coated lenses with non-tinted of 5 groups and 45 multicoated lenses with tinted of 9 groups were analyzed as a sample respectively. Results: Average and deviation of local transmittance for nontinted lenses were measured almost uniformly with various refractive index and coating. However, deviation of transmittance of for tinted lenses was analyzed as about 3.7 times larger than that of non-tinted lenses. Inhomogeneity of local transmittance of for tinted lenses was also analyzed as about 3.1 times larger than that of non-tinted lenses. Conclusions: We could analyze that standard deviation of transmittance and inhomogeneity of local transmittance of for tinted lenses is larger than that of non-tinted lenses using the local transmittance microscope. These analysis using local transmittance microscope can be utilized as a way to evaluate lens performance and improve optical homogeneity.

A Study on the Precise End-Point Detection in Titration by Using the Phase Angle Measurements (위상각 측정에 의한 적정의 정확한 종말점 검출법에 관한 연구)

  • Park, Byung-Bin;Shin, Ho-Sang;Lee, Han-Hyoung
    • Analytical Science and Technology
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    • v.12 no.4
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    • pp.290-298
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    • 1999
  • A study on the application of impedance phase angle for redox titration, acid-base titration, chelate titration and precipitation titration has been carried out. A constant alternating current was passed between two platinum electrodes. One of them was a polarizable micro-electrode of $0.1cm^2$ or $0.026cm^2$ surface area and the other a non-polarizable large electrode of $1cm^2$ surface area dipped in the solution to be titrated. The impedance and the phase angle of the titration cell were measured with lock-in amplifier to obtain well behaved titration curve respectively. In titration of oxalic acid vs. potassium permanganate, the end-point was obtained successfully from the phase angle titration curve. In this experiment, the concentration of 0.0005 M to 0.05 M, the current of $50{\mu}A$ and the frequency of near 50 Hz were used. In titration of phosphoric acid vs. sodium hydroxide, the first end-point was obtained successfully on the optimum experimental condition of 0.001 M concentration, $50{\mu}A$ current and 25~97 Hz frequency. However, the end-point in titration of cupric sulfate vs. disodium-EDTA couldn't be obtained clearly. The end-point was obtained with the out-of-phase impedance curve on the experimental condition of 0.01 M concentration, $100{\mu}A$ current, 5~35 Hz frequency range. In titration of sodium chloride vs. silver nitrate, the end-point was obtained successfully on the experimental condition of 0.1 M concentration, $100{\mu}A$ current and 5~47 Hz frequency range. This study showed that the impedance phase angle was applicable for the detection of the end-points in redox titration curve, acid-base titration curve, chelate titration curve and precipitation titration curve.

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