• Bulletin of the Korean Chemical Society
• /
• 제32권3호
• /
• pp.915-920
• /
• 2011

Four esters of succinic and maleic acid were synthesized, separated by thin-layer chromatography (TLC), and identified using matrix-assisted laser desorption/ionization-mass spectrometry (MALDI-MS). A comparison of matrix materials showed that 2,6-dihydroxybenzoic acid (2,6-DHB) yielded a greater ionization efficiency than 2,5-DHB prior to TLC separation. The location of each ester sample on the TLC plate was estimated by comparing the developed plate with a duplicate plate that had been visualized by immersion in a $KMnO_4$ solution. Generally, mass spectra obtained from the $KMnO_4$-visualized plate were relatively poor. Reproducible mass spectra with high peak abundance were difficult to obtain using the 2,6-DHB matrix from crude synthetic esters extracted from the TLC plates. Significant improvements in both reproducibility and sensitivity were realized by using pencil lead as the MALDI matrix. The current methodology will be beneficial to organic chemists since it can provide a guideline for simple and rapid characterization of small organic compounds.

• Communications for Statistical Applications and Methods
• /
• 제23권4호
• /
• pp.321-334
• /
• 2016

In this paper, we propose power t distribution based on t distribution. We also study the properties of and inferences for power t model in order to solve the problem of real data showing both skewness and heavy tails. The comparison of skew t and power t distributions is based on density plots, skewness and kurtosis. Note that, at the given degree of freedom, the kurtosis's range of the power t model surpasses that of the skew t model at all times. We draw inferences for two parameters of the power t distribution and four parameters of the location-scale extension of power t distribution via maximum likelihood. The Fisher information matrix derived is nonsingular on the whole parametric space; in addition we obtain the profile log-likelihood functions on two parameters. The response plots for different sample sizes provide strong evidence for the estimators' existence and unicity. An application of the power t distribution suggests that the model can be very useful for real data.

• 설비공학논문집
• /
• 제26권2호
• /
• pp.91-96
• /
• 2014

An acoustical model for detecting the leak location in a buried gas pipeline has been developed. This model is divided into an experimental model for sound diagnosis, and a theoretical model for sound prediction, which is based on the transfer matrix method, representing the sound pressure and the volume velocity as state variables. The power spectrum is measured by attaching only one microphone to the closed end pipe. It has been shown that the response magnitude of acoustic pressure signals calculated by the acoustical model depends upon the thickness and diameter of a pinhole. The validity for the acoustical model has been verified through a comparison between the measured and calculated results.

• 대한조선학회논문집
• /
• 제57권3호
• /
• pp.140-151
• /
• 2020

It is important to identify the location of ship hull blocks with exact block identification number when scheduling the shipbuilding process. The wrong information on the location and identification number of some hull block can cause low productivity by spending time to find where the exact hull block is. In order to solve this problem, it is necessary to equip the system to track the location of the blocks and to identify the identification numbers of the blocks automatically. There were a lot of researches of location tracking system for the hull blocks on the stockyard. However there has been no research to identify the hull blocks on the stockyard. This study compares the performance of 5 Convolutional Neural Network (CNN) models with multi-view image set on the classification of the hull blocks to identify the blocks on the stockyard. The CNN models are open algorithms of ImageNet Large-Scale Visual Recognition Competition (ILSVRC). Four scaled hull block models are used to acquire the images of ship hull blocks. Learning and transfer learning of the CNN models with original training data and augmented data of the original training data were done. 20 tests and predictions in consideration of five CNN models and four cases of training conditions are performed. In order to compare the classification performance of the CNN models, accuracy and average F1-Score from confusion matrix are adopted as the performance measures. As a result of the comparison, Resnet-152v2 model shows the highest accuracy and average F1-Score with full block prediction image set and with cropped block prediction image set.

• 한국구조물진단유지관리공학회 논문집
• /
• 제6권3호
• /
• pp.167-175
• /
• 2002

In this paper, an analytical model is proposed for analyzing the hysteretic behavior of RC beam with relocated plastic hinge region under load reversals. The plastic hinge is modeled not to be concentrated on a point but to be distributed on a finite size in beam. This is based on the assumption that the plastic hinge is formed over a certain region, in which the curvature varies. Tangential matrix is reformed using stiffness coefficients including variales such as the length and location of plastic hinge region. In order to construct the hysteretic rule of hinge, modified Takeda rule is also proposed on the base of regression analysis for the previous test results. Previous specimens are analyzed using the proposed model and the result is compared with test result. On the result of the comparison, it was shown that the hysteretic behavior of beams with different location of plastic hinge region could be prediced using the proposed analytical process.

• 디지털융복합연구
• /
• 제13권5호
• /
• pp.205-211
• /
• 2015

최근 이동통신망과 휴대단말기가 급격하게 발전하게 되면서 모바일 오피스 서비스가 점점 각광을 받고 있다. 그러나, 사용자가 모바일 오피스환경에서 업무를 수행할 때 원격에 있는 자료를 업/다운로드 할 경우 제3자로부터 악의적인 공격을 받을 수 있다. 본 논문에서는 모바일 오피스 환경에서 사용되는 개인정보 및 기업정보(통화내역, 수신메시지, 전화번호부, 일정, 위치정보, 금융거래정보, 서류 등)를 담고 있는 스마트폰의 도난 분실로 인한 정보유출 예방 기법을 제안한다. 제안 기법에서는 개인정보 및 기업 정보의 상태정보를 삼각퍼지수를 이용하여 쌍대비교 행렬로 구현한다. 특히, 제안 기법은 쌍대비교 행렬로 구한 값을 개인정보 및 기업 정보와 쌍으로 구성하여 스마트폰 분실시 제3자가 개인정보 및 기업 정보를 확인할 수 없도록 하여 외부로 유출하는 것을 예방한다.

• 한국지진공학회논문집
• /
• 제2권3호
• /
• pp.27-35
• /
• 1998

Steel structures with added viscoelastic dampers are analysed to investigat their behavior under earthquake excitation. The direct integration method, which produces exact solution for the non-proportional or non-classical damping system, is used throughout the analysis. The results from modal strain energy method are also provided for comparison. Then a new analytical a, pp.oach, based on the rigid floor diaphragm assumption and matrix condensation technique, is introduced, and the results are compared with those obtained from direct integration method and modal strain energy method. The well known phenomenon, that the effectiveness of the viscoelastic dampers depends greatly on the location of the dampers, is once again confirmed in the analysis. It is also found that the modal strain energy method generaly underestimates the responses obtained from the direct integration method, especially when the dampers are placed in only a part of the building. The proposed method turns out to be very efficient with considerable saving in computation this and reasonably accurate considering the reduced degrees of freedom.

• Archives of Plastic Surgery
• /
• 제33권5호
• /
• pp.592-600
• /
• 2006

Purpose: Numerous materials, both autologous and nonautologous, have been used for augmentation of sunken areas, but they have their own limitations. The purpose of this study is to determine the histologic response and volume change of the xenogenic collagen-based scaffold($Terudermis^{(R)}$) to the transfer into a subcutaneous soft tissue location in vivo rabbit model. Methods: Eighteen New Zealand white rabbits were used. Three $1.2{\times}1.2cm$ sized subcutaneous pockets were created on the dorsal surface of each ear. $1{\times}1cm$ sized collagen matrix($Terudermis^{(R)}$) and autologous dermal graft were implanted into each pocket. Full thickness of ear was harvested in 3 days, 1, 2, 4 weeks, 3, 6 months after implantation. Results: Histological analysis of implants demonstrated progressive neovascularization, fibroblast infilteration, neocollagen bundle synthesis and organization, and few foreign body reaction. The thickness of the collagen matrix in 3 days after the operation was 87.69% of the thickness of the collagen matrix in wet state. Then it decreased to 30.17% in 6 months after the operation. The rate of decrease was similar at all points at the same time compared with autologous dermal graft. Conclusion: Our experimental study suggests that $Terudermis^{(R)}$ could be a safe material as an implant for permanent augmentation in subcutaneous tissue. However the choice of graft for augmentation should be remained to the clinical situations.

• 한국지반공학회:학술대회논문집
• /
• 한국지반공학회 2009년도 세계 도시지반공학 심포지엄
• /
• pp.976-984
• /
• 2009

This study proposes a simple method that uses a simple mass-spring model to predict the natural frequency of a soil-pile-structure system in sandy soil. This model includes a pair of matrixes, i.e., a mass matrix and a stiffness matrix. The mass matrix is comprised of the masses of the pile and superstructure, and the stiffness matrix is comprised of the stiffness of the pile and the spring coefficients between the pile and soil. The key issue in the evaluation of the natural frequency of a soil-pile system is the determination of the spring coefficient between the pile and soil. To determine the reasonable spring coefficient, subgrade reaction modulus, nonlinear p-y curves and elastic modulus of the soil were utilized. The location of the spring was also varied with consideration of the infinite depth of the pile. The natural frequencies calculated by using the mass-spring model were compared with those obtained from 1-g shaking table model pile tests. The comparison showed that the calculated natural frequencies match well with the results of the 1-g shaking table tests within the range of computational error when the three springs, whose coefficients were calculated using Reese's(1974) subgrade reaction modulus and Yang's (2009) dynamic p-y backbone curves, were located above the infinite depth of the pile.

• 한국정보과학회논문지:소프트웨어및응용
• /
• 제34권7호
• /
• pp.595-602
• /
• 2007

본 논문에서는 미지의 아미노산 서열이 신호 펩티다제 I에 의해 절단되는 분비성 단백질인지를 판별하고, 분비성 단백질일 경우에는 절단 위치를 예측하는 방법을 제안한다. 아미노산의 소수성을 이용한 전처리를 수행하여 분비성 단백질의 선도서열인 신호서열의 존재와 절단 위치를 추정한다. 전처리를 통해서 신호서열 아닌 서열을 초기에 제외함으로써 신호서열 예측의 정확도를 높인다. 지지벡터기계를 신호서열의 예측에 효과적으로 적용하기 위해서, 생물학적 정보와 관련된 아미노산 서열간의 거리를 제안한다. 아미노산의 세포내 위치를 예측할 수 있는 소수성 척도와 아미노산의 진화적인 관계를 나타낼 수 있는 치환행렬을 이용하여 아미노산 서열간의 거리를 정의한다. Swiss-Prot release 50 단백질 자료에 대하여 교차타당성 기법을 사용하여 실험한 결과 제안한 방법은 신호서열중에 98.9%를 신호서열로 판별하였고, 88%의 절단위치 예측정확도를 보였다. 기존의 방법과의 비교실험을 통해서 제안한 방법이 신호서열의 예측에 더욱 효과적임을 확인하였다.