• 한국연소학회:학술대회논문집
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• 2015.12a
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• pp.197-200
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• 2015

Understanding the slag flow behavior is important in an entrained coal gasifier for its influence of ash discharge and wall heat transfer rate. This study presents a new model to predict the transient behavior of the liquid and solid slag layers. Unlike the previous steady-state model, the solid slag layer was included in solving the governing equations in order to identify the temporal and spatial transformation between the solid-liquid slag, rather than treating the solid region as a boundary condition of the liquid layer. The performance of the new model was evaluated for changes in the slag deposition rate (${\pm}10%$) and gas temperature (${\pm}50K$) in a simple cylindrical gasifier. The results show that the characteristic times to reach a new steady-state ranged between 80 s to 180s for the changes in the two parameters. Because the characteristic times of the gasifier temperature and slag deposition rate by changes in the coal type and/or operating conditions would be almost instantaneous, the time-scale for the slag thickness at the bottom of the gasifier to stabilize was much larger.

• Journal of Advanced Marine Engineering and Technology
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• v.25 no.4
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• pp.898-903
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• 2001

The particle image velocimetry with liquid crystal tracers is used for visualizing and analysis of the bubbly flow in a vertical temperature gradient. This method allows simultaneous measurement of velocity and temperature field at a given instant of time Quantitative data of velocity were obtained by applying the MQD technique to visualized image. The paper describes the method, and presents the transient velocity patterns of bubbly flow.

• Journal of Industrial Technology
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• v.6
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• pp.19-31
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• 1986

The residence time distribution of liquid flow in a 4.0cm diameter column packed with porous $Al_2O_3$ spheres of 0.37cm diameter were measured with pulse injections of a tracer under cocurrent trickling flow conditions. The mean residence time of liquid flow and liquid hold-up calculated by the transient curve of tracer were unaffected by gas flow rates under experimental ranges of liquid flow rates from 2.4 to $4.5(kg/m^2\;sec)$ and gas flow rates from 0 to $0.13(kg/m^2\;sec)$. The axial dispersion coefficient of liquid stream and apparent diffusivity of tracer in a micropore of solid particle were estimated from the response curve of tracer. The calculated Peclet No. were increased in ranges of 68-to 82 with a increasing of liquid mass velocity, and the external effective contacting efficiency between liquid and solid which can be expressed. by $(D_i)_{app}/D_i$ varied in ranges of 0.54 to 0.68 depending on the liquid flow rates. The gas to liquid(water) volumetric mass transfer coefficient were determined from desorption experiments with oxygen at $25^{\circ}C$ and 1 atm. The measured mass transfer coefficients were increased with liquid flow rates and the effect of gas flow rates on the mass transfer coefficient was insignificant.

• Journal of Welding and Joining
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• v.21 no.2
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• pp.89-96
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• 2003

The change of microstructures in the base metal during transient liquid phase bonding process of directionally Ni base superalloy, GTD-111 was investigated. Bonds were fabricated using a series of holding times(0-7.2ks) at three different temperatures(1403, 1418 and 1453K) under a vacuum of 13.3mPa. In raw material, ${\gamma}$- ${\gamma}$' eutectic phases, platelet η phases, MC carbide and PFZ were seen in interdendritic regions or near grain boundary and size of primary ${\gamma}$' precipitates near interdendritic regions were bigger than core region. The primary ${\gamma}$' precipitates in dendrite core were dissolved early in bonding process, but ${\gamma}$' precipitates near interdendritic regions were dissolved partially and shape changed. The dissolution rate increased with increasing temperature. Phases in interdendritic regions or near pain boundary continually changed with time at the bonding temperature. In the bonding temperature of 1403K, eutectic phases had not significantly changed, but η phases had transformed from platelet shape to needle morphology and PFZ region had widened with time. The interdendritic region and near pain boundary were liquated partially at 1423k and fully at 1453k by reaction of η phases and PFZ. In the bonding temperature of 1453K, interdendritic region and near pain boundary were liquated and then new phases which mixed with η phases, PFZ and MC carbide crystallized during cooling. Crystallized η phases transformed from rod shape to platelet shape with increasing holding time.

• Transactions of the Korean hydrogen and new energy society
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• v.23 no.6
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• pp.678-687
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• 2012

Concentration fields of solid powder in a liquid fuel were quantitatively measured by a visualization technique. The measurement system consists of a camcoder and three LCD monitors. The solid powder (glass powder) were filled in a head tank which was installed over a main mixing tank ($D{\times}H$, $310{\times}370mm$). The main mixing tank was filled with JetA1 fuel oil. With a sudden opening of the upper tank by pressurized nitrogen gas with 1.9 bar, the solid powder were poured into the JetA1 oil. An impeller type agitator was being rotated in the mixing with 700 rpm for the enhancements of mixing. Uniform visualization for the mixing flow field was made by the light from the three LCD monitors, and the visualized images were captured by the camcoder. The color images captured by the camcoder The color information of the captured images was decoded into three principle colors R, G, and B to get quantitattive relations between the concentrations of the solid powder and the colors. To get better fitting for the strong non-linearity between the concentration and the color, a neural network which has strong fitting performances was used. Analyses on the transient mixing of the solid powders were quantitatively made.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.23 no.6
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• pp.734-743
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• 1999

The local Nusselt numbers have been measured for a round turbulent jet impinging on the concave surface with and without rib. Liquid crystal/transient method was used to determine the Nusselt number distributions along the surface. The temperature on the surface was measured using liquid crystal and a digital color image processing system. The experiments were made for the jet Reynolds number (Re) 23,000, the dimensionless nozzle-to-surface distance (L/d) from 4 to 10, the dimensionless surface curvature (d/D) 0.056, and the rib type (height ($d_1$) 0.2 cm, pitch (p) from 1.2 to 3.2 cm). It was founded that only when $L/d{\geq}6$, the average Nusselt numbers on the concave surface with rib are higher than those without rib, mainly due to an increase in the turbulent intensity caused by the effect of rib attached to the wall surface. It was realized that the rib attached to the concave surface may no longer enhance the heat transfer rate or even lowers it depending on the rib type and flow conditions. In addition, the results by the steady-state method using the gold-film Intrex were in good agreement with those by the transient shroud method.

• Korean Journal of Metals and Materials
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• v.47 no.4
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• pp.242-247
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• 2009

On the Transient Liquid Phase Bonding (TLPB) phenomenon with the MBF-50 insert metal at narrow gap (under 100), it takes long time for the bonding and the homogenizing. Typically, isothermal solidification is controlled by the diffusion of depressed element of B and Si. However, the amount of B and Si in the MBF-50 filler metal is large. This is reason of the long bonding time. Also, the MBF-50 filler metal did not contained Al and Ti which are ${\gamma}^{\prime}$ phases former. This is reason of the long homogenizing time. From the bonding phenomenon with the MBF-50 insert metal, we search main factors on the bonding mechanism and select several insert-metals for using the wide-gap TLPB. New insert-metals contained Al and Ti which are ${\gamma}^{\prime}$ phases former and decrease the B then the MBF-50. When the new insert-metal was used on the TLPB, the bonding time was decreased about 1/10 times and homogenizing heat treatment was no needed. In spite of the without homogenizing, the volume fraction of ${\gamma}^{\prime}$ phases in the boned interlayer was equal to homogenizing heat treated specimen which was TLPB with the MBF-50. Finally, the new insert metal named WG1 for the wide-gap TLPB is more efficient then the MBF-50 filler metal without decreasing the bonding characteristic.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.536-537
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• 2006

In the present work, the sintering behavior of high strength Al-5.6Zn-2.5Mg-1.6Cu (in wt.%) alloy compacts prepared from elemental powders was investigated. Microstructural evaluation was accompanied by XRD and DSC methods in order to determine the temperature and chemical composition of the liquid phases formed during sintering. It was found that three transient liquid phases are formed at 420, 439 and 450 $^{\circ}C$. Microstructural study revealed the progressive formation of sintered contacts due to the presence of the liquid phases, although the green compact expands as a result of the melt penetration along the grain boundaries. While Zn melts at ${\sim}420\;^{\circ}C$, the intermetallic phases formed between Al and Mg were found to be responsible for the formation of liquid phase and the dimensional change at higher temperatures.

• Journal of the Microelectronics and Packaging Society
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• v.30 no.1
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• pp.55-62
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• 2023

In this study, Sn-3.0Ag-0.5Cu (wt.%, SAC305) solder dipping process was performed between Ni-foam skeleton with different pore per inch (PPI) to fabricate Ni-foam/SAC305 composite solder, and then applied to the transient liquid phase (TLP) bonding process to evaluate the microstructure and mechanical properties of the bonded joint. The Ni-foam/SAC305 composite solder preform consisted of Ni-foam and SAC305, and an intermetallic compound (IMC) having a (Ni,Cu)₃Sn₄ composition was formed at the Ni-foam interface. During TLP bonding process, the IMC at the Ni-foam interface was converted to (Ni,Cu)₃Sn₄+Au, and as the bonding time increased, the Ni-foam and SAC305 continuously reacted, and the bonded joint was converted into an IMC. And it was confirmed that the 130 PPI Ni-foam/SAC305 composite solder joint was converted into an IMC at the fastest rate. As a result of performing a shear test to confirm the effect of Ni-foam on mechanical properties, solder joints under all conditions exhibited excellent mechanical properties of 50 MPa or more in the early stages of the TLP bonding process, and the shear strength tends to increase as the bonding time increases.

• 한국전산유체공학회:학술대회논문집
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• 2004.03a
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• pp.178-182
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• 2004

Numerical analysis of a gaseous jet submerged in a liquid environment was carried out using the volume of fluid(VOF) method to simulate the kinematics of the gas-liquid interface. Two nozzle geometries were tested, one for Fanno tube and the other for converging diverging nozzle. Commercial code was used for the present calculation. Transient behavior of a gaseous jet since its start showed periodic nature of the jet, which was also observed in previous measurements.