• Title/Summary/Keyword: Liquid Silicon Infiltration

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Defect Inspection and Physical-parameter Measurement for Silicon Carbide Large-aperture Optical Satellite Telescope Mirrors Made by the Liquid-silicon Infiltration Method (액상 실리콘 침투법으로 제작된 대구경 위성 망원경용 SiC 반사경의 결함 검사와 물성 계수 측정)

  • Bae, Jong In;Kim, Jeong Won;Lee, Haeng Bok;Kim, Myung-Whun
    • Korean Journal of Optics and Photonics
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    • v.33 no.5
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    • pp.218-229
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    • 2022
  • We have investigated reliable inspection methods for finding the defects generated during the manufacturing process of lightweight, large-aperture satellite telescope mirrors using silicon carbide, and we have measured the basic physical properties of the mirrors. We applied the advanced ceramic material (ACM) method, a combined method using liquid-silicon penetration sintering and chemical vapor deposition for the carbon molded body, to manufacture four SiC mirrors of different sizes and shapes. We have provided the defect standards for the reflectors systematically by classifying the defects according to the size and shape of the mirrors, and have suggested effective nondestructive methods for mirror surface inspection and internal defect detection. In addition, we have analyzed the measurements of 14 physical parameters (including density, modulus of elasticity, specific heat, and heat-transfer coefficient) that are required to design the mirrors and to predict the mechanical and thermal stability of the final products. In particular, we have studied the detailed measurement methods and results for the elastic modulus, thermal expansion coefficient, and flexural strength to improve the reliability of mechanical property tests.

Tribological Properties of C-SiC Brake Discs with Surface Modifications (세라믹 디스크의 표면 개질에 따른 마찰 마모 특성)

  • Jang, Ho;Kim, Ki-Jung;Hwang, Hee-Jeong;Kim, Seong-Jin;Park, Hong-Sik
    • Tribology and Lubricants
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    • v.24 no.4
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    • pp.163-169
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    • 2008
  • Tribological properties of ceramic brake discs were investigated using a commercial friction material. The discs were manufactured by liquid silicon infiltration (LSI) into a C-C preform. The disc surface was modified by two different methods, producing sliding surfaces with chopped carbon fibers and carbon felt. In addition, the composition of the surface was also changed. Friction characteristics of the discs were examined using a 1/5 scale dynamometer. Results showed that the type and composition of the disc surface significantly affected the level of braking effectiveness and high temperature brake performance. The discs with felt surfaces showed higher friction levels than those with chopped fiber surfaces and SiC tended to increase the friction level while C lowered the friction coefficient. The ceramic disc was more sensitive to the deceleration rate than gray iron, showing high speed sensitivity.

Thermal and mechanical properties of C/SiC composites fabricated by liquid silicon infiltration with nitric acid surface-treated carbon fibers

  • Choi, Jae Hyung;Kim, Seyoung;Kim, Soo-hyun;Han, In-sub;Seong, Young-hoon;Bang, Hyung Joon
    • Journal of Ceramic Processing Research
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    • v.20 no.1
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    • pp.48-53
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    • 2019
  • Carbon fiber reinforced SiC composites (C/SiC) have high-temperature stability and excellent thermal shock resistance, and are currently being applied in extreme environments, for example, as aerospace propulsion parts or in high-performance brake systems. However, their low thermal conductivity, compared to metallic materials, are an obstacle to energy efficiency improvements via utilization of regenerative cooling systems. In order to solve this problem, the present study investigated the bonding strength between carbon fiber and matrix material within ceramic matrix composite (CMC) materials, demonstrating the relation between the microstructure and bonding, and showing that the mechanical properties and thermal conductivity may be improved by treatment of the carbon fibers. When fiber surface was treated with a nitric acid solution, the observed segment crack areas within the subsequently generated CMC increased from 6 to 10%; moreover, it was possible to enhance the thermal conductivity from 10.5 to 14 W/m·K, via the same approach. However, fiber surface treatment tends to cause mechanical damage of the final composite material by fiber etching.

Effects of Carbon Fiber Arrangement on Properties of LSI Cf-Si-SiC Composites (탄소섬유 배열이 LSI Cf-Si-SiC 복합체의 특성에 미치는 영향)

  • Ji, Young-Hwa;Han, In-Sub;Kim, Se-Young;Seo, Doo-Won;Hong, Ki-Seog;Woo, Sang-Kuk
    • Journal of the Korean Ceramic Society
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    • v.45 no.9
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    • pp.561-566
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    • 2008
  • Carbon fiber fabric-silicon carbide composites were fabricated by liquid silicon infiltration (LSI) process. The porous two-dimensional carbon fiber fabric performs were prepared by 13 plies of 2D-plain-weave fabric in a three laminating method, [0/90], [${\pm}45$], [$0/90/{\pm}45$] lay-up, respectively. Before laminating, a thin pyrolytic carbon (PyC) layer deposited on the surface of 2D-plain weave fabric sheets as interfacial layer with $C_3H_8$ and $N_2$ gas at $900^{\circ}C$. A densification of the preforms for $C_f-Si-SiC$ matrix composite was achieved according to the LSI process at $1650^{\circ}C$ for 30 min. in vacuum atmosphere. The bending strength of the each composite were measured and the microstructural consideration was performed by a FE-SEM.

Fracture Characteristics of C/SiC Composites for Rocket Nozzle at Elevated Temperature (로켓 노즐목 소재 C/SiC 복합재 고온 파괴 특성)

  • Yoon, Dong Hyun;Lee, Jeong Won;Kim, Jae Hoon;Sihn, Ihn Cheol;Lim, Byung Joo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.40 no.11
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    • pp.927-933
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    • 2016
  • In a solid propulsion system, the rocket nozzle is exposed to high temperature combustion gas. Hence, choosing an appropriate material that could demonstrate adequate performance at high temperature is important. As advanced materials, carbon/silicon carbide composites (C/SiC) have been studied with the aim of using them for the rocket nozzle throat. However, when compared with typical structural materials, C/SiC composites are relatively weak in terms of both strength and toughness, owing to their quasi-brittle behavior and oxidation at high temperatures. Therefore, it is important to evaluate the thermal and mechanical properties of this material before using it in this application. This study presents an experimental method to investigate the fracture behavior of C/SiC composite material manufactured using liquid silicon infiltration (LSI) method at elevated temperatures. In particular, the effects of major parameters, such as temperature, loading, oxidation conditions, and fiber direction on strength and fracture characteristics were investigated. Fractography analysis of the fractured specimens was performed using an SEM.