• 제목/요약/키워드: Liquid Segregation

검색결과 79건 처리시간 0.029초

YBa_{2}Cu_{3}O_{7-\delta} 고온초전도체 단결정에서의 Y_{2}BaCuO_{5} 편석과 Multi-Seeding의 가능성, 대각선 흔적의 형성 원인 (Y2BaCuO4 Segregarion , a Possibility of Multi-Seeding and the Origin of Diagonal Line in YBa2Cu3O7-$\delta$ Superconductor Single Crystal)

  • 성현태
    • 한국초전도ㆍ저온공학회논문지
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    • 제1권1호
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    • pp.1-6
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    • 1999
  • The microstructures of top seed mult processde $\textrm{YBa}_2\textrm{Cu}_3\textrm{O}_7$.$\delta$ single crystal were studied. Although shape of the seed was not faceted. the growth shape of Y123 single crystal was faceted. It was observed that Y211 phases were trapped in specific spaces of the faceted region. From the microstructural investigation. it was suggested that the segregation of Y211 is due to the difference of growth rates in crystal direction. When a single crystal was grown by the single seed with stepped multi surfaces. a microstrue was grown from multi-seed. The microstructure show the possibility of multi-seed growth. Corn kernel like structure without Y211 phase was observed and seemed to be formed by the diffusion reaction between Y211 phase in crystal and liquid wetted on the crystal. the diagonal line on Y123 crystal was observed that it was formed by the corn kernel like structure.

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용탕압출법에 의한 Al-Cu 합금 선재의 제조에 관한 연구 (A Study on Fabrication of Al-Cu alloy bar by Melt-extrusion Process)

  • 주대헌;이병수;김명호
    • 한국주조공학회지
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    • 제24권6호
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    • pp.331-339
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    • 2004
  • Melt-extrusion process, a metallic melt poured and solidified up to semisolid state in the container can be directly extruded through the die exit to form a product of bar shape without other intermediate processes. In this study, the fabrication characteristics of the process were evaluated with various process parameters, such as preheating temperature of extrusion dies, extrusion temperature and extrusion ratio. AI-Cu alloys were successfully extruded after squeezing out of liquid during melt-extrusion with smaller force compared to the solid extrusion. Soundly AI-Cu alloy bar was fabricated at the preheating temperature of $500{\sim}520^{\circ}C$. The range of extrusion temperature for soundly melt-extruded AI-Cu alloy bar was increased with increasing extrusion ratio. Mechanical properties of melt-extruded AI-Cu alloy bars were found change with Cu content of the melt-extruded bars due to the occurrence of segregation. The various extrusion temperature yielded equiaxed structure with a grains size about 200 ${\mu}m$.

동작 전류에 의한 Magnetic fluid Linear Pump의 동특성 해석 (Analysis of the Driving Characteristics in the Magnetic Fluid Linear Pump by Operating Current)

  • 서강;박관수
    • 대한전기학회논문지:전기기기및에너지변환시스템부문B
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    • 제53권4호
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    • pp.237-246
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    • 2004
  • The advantages of the Magnetic Fluid Linear Pump(MFLP) is that this device could Pump the non-conductive. non-magnetic liquid such as Insulin or blood because of the segregation structure of the magnetic fluid and pumping liquid. In this device. the sequential currents are needed to Produce pumping forces so that Pumping Forces and Pumping speed mainly depend on the current Patterns. The excessive forces at Pumping moment could cause the medical shock, and weak forces at intermediate moment could cause the back flow or the pumping liquid. So the ripples of the pumping forces need to be reduced for the medical application. In this research, the driving characteristics in the MFLP by operating current is analysed. The change of magnetic fluid surface according to the driving currents could be obtained be magneto-hydrodynamic analysis so that Pumping fortes could be computed by integration of the surface moving to the pumping direction at each moment. The actual MFLP with 13mm diameter was made and tested for experiments. The effects of driving current and frequency on the pumping forces and pumping speed were analyzed and compared with experimental measurements.

전자기 연속 주조법을 이용한 의료용 타이타늄 합금 제작에 관한 연구 (Fabrication of Titanium alloy by Electromagnetic Continuous Casting (EMCC) Method for Medical Applications)

  • 최수지;이현재;백수현;현승균;정현도;문병문
    • 한국주조공학회지
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    • 제38권1호
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    • pp.9-15
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    • 2018
  • Electromagnetic continuous casting (EMCC) was used to fabricate Ti-6Al-4V alloys with properties suitable for medical applications. Ti-6Al-4V alloy ingots fabricated by EMCC were subjected to heat treatment, such as residual stress removing (RRS), furnace cooling after solution treatment (ST-FC) and water-cooling after solution treatment (ST-WC), in order to obtain characteristics suitable for the standard. After component analysis, the microstructure and mechanical properties (tensile strength and elongation) were evaluated by ICP, gas analysis, OM, SEM, a Rockwell hardness tester and universal testing machine. The Ti-6Al-4V alloy ingot fabricated by EMCC was fabricated without segregation, and the lamellar structure was observed in the RRS and ST-FC specimens. The ST-WC specimen showed only martensite structure. As a result of evaluating the mechanical properties based on the microstructure results, we found that the water-cooled heat treatment condition after the solution treatment was most suitable for the Ti-6Al-4V ELI standard.

Nd-Fe-B계 소결자석의 이방화율 향상을 위한 연구 (A Study for Magnetic Orientation Enhancement in Nd-Fe-B Sintered Magnets)

  • 김동환;임광윤;김효준;조재완;서응석;김승호;김상면
    • 한국자기학회지
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    • 제11권1호
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    • pp.8-13
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    • 2001
  • Axial pressing process를 이용하여 31RE-68TM-1B(RE : 희토류원소, TM: 3d천이금속) 조성을 갖는 소결자석을 제조함에 있어서 Casting process와 Lubricant 변화에 따른 잔류자속밀도 변화를 조사하였다. 출발합금 제조방법으로서 Strip casting process는 $\alpha$-Fe 편석없이 미세하고, 균일한 microstructure를 얻기에 용이한 잇점이 있었으며, Jet mill 이후 균일한 입도의 분말을 얻을 수 있었다. 또한, Jet mill 전후에 적절한 분말 혹은 무수알콜과 같은 Lubricant를 첨가함으로써 잔류자속밀도를 향상시킬 수 있었다. 본 실험에서는 Strip casting 및 분말 Lubrican인 Zn-st(Zinc stearate)에 첨가에 의한 분말입도분포 개선효과와 무수알콜에 의한 배향율 향상효과를 접목하여 잔류자속밀도, 보자력 및 최대자기에너지적이 각각 13.1 kG, 13.5 kOe 및 39.5 MGOe인 경자기특성이 얻어졌다.

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V2O5 도핑된 NiCuZn 페라이트로 제조된 칩인덕터에서의 Ag/cu 석출 (Ag and Cu Precipitation in Multi-Layer Chip Inductors Prepared with V2O5 Doped NiCuZn Ferrites)

  • 제해준;김병국
    • 한국재료학회지
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    • 제13권8호
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    • pp.503-508
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    • 2003
  • The purpose of this study is to investigate the effect of $V_2$$O_{5}$ addition on the Ag and Cu precipitation in the NiCuZn ferrite layers of 7.7${\times}$4.5${\times}$1.0 mm sized multi-layer chip inductors prepared by the screen printing method using 0∼0.5 wt% $V_2$$O_{5}$ -doped ferrite pastes. With increasing the $V_2$$O_{5}$ content and sintering temperature, Ag and Cu oxide coprecipitated more and more at the polished surface of ferrite layers during re-annealing at $840^{\circ}C$. It was thought that during the sintering process, V dissolved in the NiCuZn ferrite lattice and the Ag-Cu liquid phase of low melting point was formed in the ferrite layers due to the Cu segregation from the ferrite lattice and Ag diffusion from the internal electrode. During re-annealing at $840^{\circ}C$, the Ag-Cu liquid phase came out the polished surface of ferrite layers, and was decomposed into the isolated Ag particles and the Cu oxide phase during the cooling process.

혼합이론에 근거한 반용융 재료의 고상률 분포 예측 (Prediction of Distribution of Solid Volume Fraction in Semi-Solid Materials Based on Mixture Theory)

  • 윤종훈;김낙수;임용택
    • 소성∙가공
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    • 제8권4호
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    • pp.399-406
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    • 1999
  • It is more appropriate to treat that the semi-solid mixture as a single phase material that obeys incompressibility in the global sense and to analyze the liquid flow only locally than the approach based on compressible yield criteria. In the present study, a numerical algorithm of updating the solid volume fraction based on mixture theory has been developed. Finite element analysis of simple upsetting was carried out using the proposed algorithm to investigate the degree of macro-segregation according to friction conditions and compressive strain rates under the isothermal condition. The simulation results were compared to experimental results available in reference to test the validity of the currently proposed algorithm. Since the comparison results show a good agreement it is construed that the proposed algorithm can contribute to the development of numerical analysis of determining the solid volume fraction semi-solid processing.

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SKH51의 반응고 상태에서의 가열 및 성형에 의한 부품 제조 (Fabrication of a Part by Heating and Forming in the Semi-solid State of the SKH51 Material)

  • 이상용
    • 열처리공학회지
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    • 제27권3호
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    • pp.127-132
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    • 2014
  • The semi-solid metal forming process has been applied to realize a near-net shape fabrication of a high speed tool steel. A complicatedly shaped part out of SKH51 was successfully manufactured by introducing pertinent materials, tooling and processing conditions. A SKH51 billet with globular grains was heated at temperatures between 1300 and $1350^{\circ}C$ using high frequency induction heater to get semi-solid microstructure before high rate injection of mushy metal into a die cavity for the forming process. It was necessary to control the preheating of dies between 300 and $400^{\circ}C$ to maintain the homogeneous microstructure during the semi-solid metal forming process. Significant defects such as pores, high fraction of liquid fraction and segregation could be removed from the part by using air vents.

Thixoforming을 응용한 금속복합재료의 콤푸레서용 피스톤 제품의 성형 (Forming of Compressor Piston Part of Metal Matrix Composites by Thixoforming Process)

  • 이동건;강충길
    • 소성∙가공
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    • 제10권3호
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    • pp.223-234
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    • 2001
  • The characteristics of thixoforming process can decrease liquid segregation because of the improvement in fluidity in a globular microstructure state and utilizes flow without an air entrapment. Therefore, in order to obtain the sound parts of metal matrix composites by using thixoforming process which has co-existing solidus-liquidus phase, it is very important to design a die shape property and to obtain the fabrication conditions which affect the unifomity of the solid fraction on unfilling state and various defects throughout the fabricated parts. The die designs and fabrication conditions to obtain the good piston part are proposed for thixoforging process of metal matrix composites. When reheated metal matrix composites billets were transferred to the closed die gate, thixoforging were carried out under the various pressure(60, 80, 100MPa) with controled forging speed. The mechanical properties such as hardness and tensile strength for thixoforged parts have been investigated after T6 heat treatment.

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반용융 성헝에서의 다구찌 방법과 신경망을 이용한 자동차 알루미늄 피스톤의 최적 재가열 과정에 대한 연구 (A Study on Optimum Reheating Process of Automotive Aluminum Piston using Neural Network and the Taguchi Method in Semi-Solid forming)

  • 윤재민;김영호;박준홍;최재찬
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2000년도 추계학술대회 논문집
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    • pp.902-905
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    • 2000
  • As the manufacturing processes of automotive engine piston, gravity die-casting, squeeze casting, hot forging and powder forging process are generally used for the various specifications. As the semi-solid forming(SSF) is compared with conventional casting such as gravity die-casting and squeeze casting for the characteristics of its process, the product without inner defects such as gas porosity and segregation can be obtained and its microstructure is globular grain. In SSF process, the materials are heated up to the temperature between the solvus and liquidus line at which the materials exists in the form of liquid-solid mixture. In this time, Discussion is given about reheating process of row material and results are presented regarding accurate temperature and process variables controlling for right solid fractions.

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