• Title/Summary/Keyword: Liquation

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The Influence of Chemical Compositions of Weld Metal and Welding Conditions on Hot Cracking by Hot Cracking Test (Inconel 690 오버레이용접부의 고온균열 발생에 미치는 용접금속의 화학조성 및 용접조건의 영향)

  • 양병일;지병하;김정태;박광식;최해수;박화순
    • Journal of Welding and Joining
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    • v.20 no.3
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    • pp.74-83
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    • 2002
  • In order to investigate the hot cracking phenomena of the Inconel 690 overlay welds, the hot cracking test(modified Varestraint test) was performed by varying augmented strain and welding speed in GTAW. A total of five kinds of specimens was used in the hot cracking test. The specimens used were two kinds of one layer specimens that were composed of just Inconel 690 deposited metal and three kinds of double layer specimens that were composed with as upper part of Inconel 690 weld metal and lower part of SA508 cl.3 or STS 309L. The main results are as fo11ows: In the welds composed of just Inconel 690, as the augmented strain was more increased and the welding speed was more decreased, the extent of cracking was more increased. And these cracks were mainly solidification cracks, and liquation cracks were also observed partially in HAZ. And hot cracking susceptibily of Inconel 690 welds by using filler metals containing Nb were higher than that of the welds with Nb free. The hot cracking susceptibility of Inconel 690 weld metal was increased with dilution of SA 508 cl.3 and STS 309L, and the influence of SA 508 cl.3 was higher than that of 575 309L. The results of calculation of $TSC\Delta$ and $TLC\Delta$ in Inconel 690 weld metal changed by dilution with base metal or neighboring welds were agreed well with the results of hot cracking test in this study. Therefore, it was expected that the hot cracking was considerably decreased or prevented by using proper welding conditions such as lower heat input, filler metals, base metal and neighboring welds.

A Study on Microstructures and Cryogenic Mechanical Properties of Electron Beam Welds between Cast and Forged Inconel 718 Superalloys for Liquid Rocket Combustion Head (액체로켓 연소기용 Inconel 718 주조 및 단조 합금의 전자빔 용접부 미세조직 및 극저온 특성)

  • Hong, Hyun-Uk;Bae, Sang-Hyun;Kwon, Soon-Il;Lee, Je-Hyun;Do, Jeong-Hyeon;Choi, Baig-Gyu;Kim, In-Soo;Jo, Chang-Yong
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.50-57
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    • 2013
  • Characterization of microstructures and cryogenic mechanical properties of electro beam (EB) welds between cast and forged Inconel 718 superalloys has been investigated. Optimal EBW condition was found in the beam current range of 36~39 mA with the constant travel speed of 12 mm/s and arc voltage of 120 kV for 10 mm-thick specimens. Electron beam current lower than 25 mA caused to occur the liquation microfissuring in cast-side heat affected zone (HAZ) of EB welds. The HAZ liquation microfissure was found on the liquated grain boundaries with resolidified ${\gamma}/Laves$ and ${\gamma}/NbC$ eutectic constituents. EBW produced welds showing a fine dendritic structure with relatively discrete Laves phase due to fast cooling rate. After post weld aging treatment, blocky Laves phase and formation of ${\gamma}^{\prime}+{\gamma}^{{\prime}{\prime}}$ strengtheners were observed. Presence of primary strengthener and coarse Laves particles in PWHT weld may cause to reduce micro-plastic zone ahead of a crack, leading to a significant decrease in Charpy impact toughness at $-196^{\circ}C$. Fracture initiation and propagation induced by Charpy impact testing were discussed in terms of the dislocation structures ahead of crack arisen from the fractured Laves phase.

전자빔 용접된 고장력 알루미늄 합금 용접부의 고온균열 발생 및 특성에 관한 연구

  • 김성욱;김경민;윤의박;이창희
    • Laser Solutions
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    • v.4 no.1
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    • pp.39-48
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    • 2001
  • This study was performed to evaluate basic characteristics of electron beam weldability for high strength aluminum alloys. The aluminum alloys used were A5083 and A6N01, and A7N01. The principal welding process parameters, such as accelerating voltage, beam current, welding speed and chamber pressure were investigated. The dimension and microstructure of welds were evaluated with OLM, and SEM (EDAX). In addition, weldability variation(cracking) due to process parameters was also evaluated. The degree of cracking in the EB fusion zone appears to be affected mainly by aspect ratio, such that as aspect ratio increases the cracking tendency also increases. The alloying element itself may also affect the hot cracking resistance, but its role is considered to be indirect effect such that the relatively higher vaporization pressure elements of Zn and Mg give deeper weld penetration and thus results in greater cracking tendency.

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Weldability of Al Alloys, Part II :HAZ Cgaracteristics (알루미늄 합금의 용접특성 - part II)

  • 이창희;장래웅
    • Journal of Welding and Joining
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    • v.11 no.1
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    • pp.2-8
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    • 1993
  • A literature review was conducted to gather informations available on the welding metallurgy of aluminum alloys, emphasized on characteristics in the heat affected zone(HAZ). Nominal metallurgical reactions that occur in aluminum alloys provide a basis for understanding aluminum welding metallurgy. However, welding reactions differ to some extent because of the relatively short times involved, and the non-isothermal heating excursed. For non-heat treatable alloys, welding primarily affects these alloys by annealing (recrystallization and growth) and to a less extent, changes in low temperature precipitates. In the case of heat treatable alloys, the resulting HAZ properties depend upon alloy composition, starting temper, heat input and post weld heat treatments.

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A Study on Relationship between Hot Ductility Behavior and Hot Cracking Susceptibility in PTA Weld of Ni-based Superalloy (니켈기 초내열합금 PTA용접부의 고온균열감수성과 고온연성거동에 관한 연구)

  • Lee, Chung-Rae;Kim, Sung-Wook;Choi, Woo-Hyuk;Eom, Sang-Ho;Lee, Chang-Hee;Kim, Jae-Chul;Choi, Chul
    • Proceedings of the KWS Conference
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    • 2003.05a
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    • pp.40-42
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    • 2003
  • In general, nickel-base superalloy has been extensively used as land-based gas turbine blades and vanes. Plasma transferred arc welding(PTAW) has been considered as a repair welding process of nickel-base superalloy. This research evaluated the relationship between hot ductility behavior and hot cracking susceptibility in nickel-base superalloys. Ductility recovery rate of nickel base superalloys was found to be poor due to incipient melting and constitutional liquation. This seems to increase the hot cracking susceptibility.

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Microstructural and Fatigue Characteristecs of AA6005A Weldments for Railroad Vehicles (철도차량용 6005A 알루미늄 합금 압출재의 미세조직 및 용접부 피로 특성)

  • 이정국;서창우;오창록;신동혁;이동헌;김용석
    • Transactions of Materials Processing
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    • v.9 no.1
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    • pp.10-16
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    • 2000
  • This research investigates microstructures and fatigue properties of the weldments of 6005A aluminum alloy developed for railroad vehicles. The samples were extruded into a truss structure and welded together using the gas metal arc welding process. The extruded sample showed a wide variation in grain size, possibly due to the frictional heating as well as the inghomogeneous metal flow in the extrusion die. The mechanical properties of the samples were affected by the mirocstructures. The fatigue strength of the welded structure was found to decrease significantly from that of the base metal. It was found that the fatigue characteristics of the welded structure were determined by the microstructure of the parent metal as well as weld defects such as porosities and the liquation cracks.

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The Effect of Weld Metal Copper Content on HAZ Cracking in Austenitic Stainless Steel welded with Al-brass

  • Lee, H.W.;Lee, J.S.;Choe, W.H.
    • Proceedings of the KWS Conference
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    • 2005.06a
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    • pp.152-154
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    • 2005
  • Austenitic stainless steel has good weldability but is sensitive to hot cracking such as solidification crack and liquation crack. In this study, the specimens of dissimilar metals made between austenitic stainless steel and Al-brass were welded by GTAW process using four different filler metals. Cracks were detected in the heat-affected zone of the stainless steel when welded with CuAl, CuSn and NiCu filler metals, but no cracks were detected a Ni filler metal was used. The cracks propagated along the grain boundary in the heat affected zone near the fusion line to base metal of 316L stainless steel. The cracks were located inside the weld bead with very fine hairline crack. All cracks initiated at the fusion line and moved forward in the base metal. From energy dispersion spectroscopy (EDS), Cu peak was detected only in the crack-opening area.

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Fatigue Life of the Repair TIG Welded Hastelloy X Superalloy

  • SIHOTANG, Restu;CHOI, Sang-Kyu;PARK, Sung-Sang;BAEK, Eung-Ryul
    • Journal of Welding and Joining
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    • v.33 no.5
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    • pp.26-30
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    • 2015
  • Hastelloy X in this study was applied in jet engine F-15 air fighter as shroud to isolate the engine from outer skin. After 15 years operation at elevated temperature the mechanical properties decreased gradually due to the precipitation of continues second phases in the grain boundaries and precipitated inside the grain. The crack happened at the edge of the shroud due to the thermal and mechanical stress from jet engine. Selective TEM analysis found that the grain boundaries consist of $M_{23}C_6$ carbide, $M_6$ Ccarbide and small percentage of sigma(${\sigma}$) phase. Furthermore, it was confirmed the nano size of ${\sigma}$ and miu (${\mu}$) phase inside the grain. In this study, it was investigated the microstructure of the degraded shroud component and HAZ of repair welded shroud. In the HAZ, it was observed the dissolution of the $M_{23}C_6$ carbides and smaller precipitates, the migration of the undissolved larger $M_{23}C_6$ carbide and $M_6$ Ccarbide. It is also observed the liquation due to the simply melt of the segregated precipitates in the grain boundaries. Interestingly, the segregated second phases which simply melt in the grain boundaries more easily happened at higher heat input welding condition. High temperature tensile test was done at $300^{\circ}C$, $700^{\circ}C$ and $900^{\circ}C$. It was obtained that the toughness of welded sample is lower compare to the non-welded sample. The solution heat treatment at $1170^{\circ}C$ for 5 minutes was suggested to obtain a better mechanical properties of the shroud. The high cycle fatigue number of the repair welded shroud shows a much lower compare to the shroud. In addition, the high cycle fatigue number at room temperature after solution heat treatment was almost double compare to the before solution heat treatment under 420-500MPa stress amplitude. However, the high cycle fatigue number of repaired welded sample was shown a much lower compare to the non- welded shroud and solution treated shroud. One of the main reasons to decrease the tensile strength and the high cycle fatigue properties of the repair welded shroud is the formation of the liquid phase in HAZ.

Potential of HAZ Property Improvement through Control of Grain Boundary Character in a Wrought Ni-based Superalloy (단련용 Ni기 초내열합금의 입계구조 제어를 통한 HAZ 특성 향상 가능성 고찰)

  • Hong, H.U.;Kim, I.S.;Choi, B.G.;Jeong, H.W.;Yoo, Y.S.;Jo, C.Y.
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.43-43
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    • 2009
  • 단련용 다결정 Ni기 초내열합금은 우수한 가공성, 내산화성, 고온특성 등으로 가스터빈 연소기, 디스크, 증기발생기 전열관 등 발전용 고온부품 소재에 널리 적용되고 있다. 최근 발전설비의 고효율화를 꾀하기 위해 작동 온도를 현격히 증가시키는 기술방향으로 발전하고 있고, 소재측면에서는 기존의 초내열합금 대비 고기능성을 확보할 수 있는 차세대 Ni기 초내열합금 개발이 유럽, 미국, 일본, 중국 등을 중심으로 활발히 이루어지고 있다. 이러한 소재의 고온강도 (온도수용성)를 향상시키기 위해서는 통상 규칙격자 금속간화합물인 $Ni_3(Al,Ti)-{\gamma}'$상의 분율을 증가시킬 수 있지만, ${\gamma}'$상분율이 증가할 경우 용접 및 후열처리 동안 용접열영향부 (HAZ)에서 액화균열이 발생할 가능성이 높아진다. 결정립계를 따라 발생하는 HAZ 액화균열은 입계특성에 의해 크게 영향을 받을 것으로 판단된다. 한편, 본 연구자들은 최근 입계 serration 현상을 단련용 합금에 도입시키는 특별한 열처리를 이론적 접근법을 통해 개발하였다. 형성된 파형입계는 결정학적인 관점에서 조밀 {111} 입계면을 갖도록 분해 (dissociation)되어 낮은 계면에너지를 갖게 됨을 확인하였으며, 입계형상 변화뿐만 아니라 탄화물 특성변화까지 유도하여 크리프 수명을 기존대비 약 40% 정도 향상시킴을 확인하였다. 이러한 직선형 입계 대비 'special boundary'로 간주되는 파형입계가 도입될 경우, HAZ 결정립크기 변화 및 액화거동에 미치는 영향을 고찰하고, 아울러 입계특성 제어가 용접성/용접부 품질 향상에 기여할 수 있는 가능성도 토의하고자 하였다. 본 연구에서는 재현 HAZ 열사이클 시험을 통해 미세구조를 정량적으로 비교하였다. 상대적으로 입계구조가 안정된 파형입계의 이동속도가 高계면 에너지를 갖는 직선형 입계보다 느려 HAZ 결정립 성장이 효과적으로 억제됨을 확인할 수 있었다. 입계 액화거동을 살펴보면, 두 시편 모두 $M_{23}C_6$, MC 등 입계탄화물 계면이 빠른 승온중 액화반응 (constitutional liquation)에 의해 입계가 액화되었으며, 이후 급냉에 의해 입계에 액상막이 존재한 흔적이 발견되었다. 최고온도별로 입계액화 폭/비율을 정량적으로 비교한 결과, 파형입계가 직선입계 대비 대체로 낮음을 확인할 수 있었으며, 때때로 액화되지 않고 잔존하는 입계 탄화물이 관찰되었다. 재현 HAZ 미세조직을 통해 Hot ductility 시험 결과를 유추하자면, 파형입계가 직선입계 보다 좁은 취성온도영역 (Brittle Temperature Range)을 나타낼 것으로 예상되어, 입계특성제어에 의해 Ni기 초내열합금의 용접성을 향상 가능성을 확인하였다.

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Electron Beam Weld ability of Alloy 718 Nozzle for Jet Propulsion Component (고속 추진체용 Alloy 718 노즐 단조품의 전자빔 용접성 평가)

  • Lee, C.H.;Kim, J.H.;Hong, J.K.;Yeom, J.T.;Yoon, J.W.;Park, N.K.
    • Transactions of Materials Processing
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    • v.17 no.7
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    • pp.523-527
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    • 2008
  • In this study, mechanical properties of Alloy 718 welded after forgings for jet propulsion component was investigated. Hot-forged and machined work-pieces($230mm\times70mm\times15mm$) which have different grain sizes are welded by electron beam welding technique. After welding, the components were solution heat-treated and aged. Samples were sectioned to analyze the microstructural evolution and formation of micro-crack. It was found that HAZ grain boundary liquation crack generally initiates in the coarse grains rather than the fine grains. Needle-like phases with high Nb contents were found at the outer part near the base metal. Vickers hardness and tensile tests were carried out at room temperature and at $649^{\circ}C$. The tensile properties of electron beam welding specimens exhibited around 100MPa and 10% decrease in strength and elongation, respectively.