• Title/Summary/Keyword: Limit of experimental method

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Dispersion Characteristics of Hydrogen Gas by the Effect of Leakage Hole Size in Enclosure Space (누출공 크기에 따른 밀폐공간 내 수소 가스의 확산 특성)

  • Choi, Jinwook;Li, Longnan;Park, Chul-Woo;Lee, Seong Hyuk;Kim, Daejoong
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.5
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    • pp.26-35
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    • 2016
  • As a potential clean energy resource, the production and consumption of hydrogen gas are expected to gradually increase, so that hydrogen related studies are also increasing. The thermal and chemical properties of hydrogen result in its high flammability; in particular, there is a high risk if leaks occur within an enclosed space. In this study, we applied the computational fluid dynamics method to conduct a numerical study on the leakage behavior of hydrogen gas and compared these numerical study results with an experimental study. The leakage hole diameter was selected as an important parameter and the hydrogen gas dispersion behavior in an enclosed space was investigated through various analytical methods. Moreover, the flammable regions were investigated as a function of the leakage time and leakage hole size. We found that the growth rate of the flammable region increases rapidly with increasing leakage hole size. We also investigated the relation between the mass flow rate and the critical time when the hydrogen gas reaches the ceiling. The analysis of the monitoring points showed that the hydrogen gas dispersion behavior is isotropic and independent of the geometry. We found that the concentration of gas in an enclosed space is affected by both the leakage flow rate and amount of gas accumulated in the enclosure.

Effect of Hooked-end Steel Fiber Volume Fraction and Aspect Ratio on Flexural and Compressive Properties of Concrete (후크형 강섬유 혼입율 및 형상비에 따른 콘크리트의 휨 및 압축 특성)

  • Kim, Dong-Hui;Jang, Seok-Joon;Kim, Sun-Woo;Park, Wan-Shin;Yun, Hyun-Do
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.25 no.3
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    • pp.40-47
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    • 2021
  • This study investigates the influence of hooked-end steel fiber volume fraction and aspect ratio on the mechanical properties, such as compressive and flexural performance, of concrete with specified compressive strength of 30MPa. Three types of hooked-end steel fibers with aspect ratios of 64, 67 and 80 were selected. The flexural tests of steel fiber reinforced concrete (SFRC) prismatic specimens were conducted according to EN 14651. The compressive performance of SFRC with different volume fractions (0.25, 0.50 and 0.75%) were evaluated through standard compressive strength test method (KS F 2405). Experimental results indicated that the flexural strength, flexural toughness, fracture energy of concrete were improved as steel fiber volume fraction increases but there is no unique relationship between steel fiber volume fraction and compressive performance. The flexural and compressive properties of concrete incorporating hooked-end steel fiber with aspect ratio of 64 and 80 are a little better than those of SFRC with aspect ratio of 67. For each SFRC mixture used in the study, the residual flexural tensile strength ratio defined in Model Code 2010 was more than the limit value to be able to substitute rebar or welded mesh in structural members with the fiber reinforcement.

A Study on Experimental Prediction of Landslide in Korea Granite Weathered Soil using Scaled-down Model Test (축소모형 실험을 통한 국내 화강암 풍화토의 산사태 예측 실험 연구)

  • Son, In-Hwan;Oh, Yong-Thak;Lee, Su-Gon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.6
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    • pp.439-447
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    • 2019
  • In this study, experiments were conducted to establish appropriate measures for slopes with high risk of collapse and to obtain results for minimizing slope collapse damage by detecting the micro-displacement of soil in advance by installing a laser sensor and a vibration sensor in the landslide reduction model experiment. Also, the behavior characteristics of the soil layer due to rainfall and moisture ratio changes such as pore water pressure and moisture were analyzed through a landslide reduction model experiment. The artificial slope was created using granite weathering soil, and the resulting water ratio(water pressure, water) changes were measured at different rainfall conditions of 200mm/hr and 400mm/hr. Laser sensors and vibration sensors were applied to analyze the surface displacement, and the displacement time were compared with each other by video analysis. Experiments have shown that higher rainfall intensity takes shorter time to reach the limit, and increase in the pore water pressure takes shorter time as well. Although the landslide model test does not fully reflect the site conditions, measurements of the time of detection of displacement generation using vibration sensors show that the timing of collapse is faster than the method using laser sensors. If ground displacement measurements using sensors are continuously carried out in preparation for landslides, it is considered highly likely to be utilized as basic data for predicting slope collapse, reducing damage, and activating the measurement industry.

Refined Exposure Assessment for Three Active Ingredients of Humidifier Disinfectants

  • Lee, Jong-Hyeon;Kang, Hyun-Joong;Seol, Hwi-Soo;Kim, Chan-Kook;Yoon, Seung-Ki;Gwack, Jin;Kim, Yong-Hwa;Kwon, Jung-Hwan
    • Environmental Engineering Research
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    • v.18 no.4
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    • pp.253-257
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    • 2013
  • Exposure assessment for three major active ingredients used for humidifier disinfectants, polyhexamethylene guanidine (PHMG), oligo(2-(2-ethoxy)ethoxyethyl guanidinium chloride (PGH), and 5-chloro-2-methylisothiazol-3(2H)-one/2-methylisothiazol-3(2H)-one (CMIT/MIT) mixture, was conducted in a bedroom using an air sampler for a refined risk assessment. The experimental site was selected to reflect consumer exposure conditions. Aerosols formed by a humidifier were sampled during 8 hr at 7.5 L/min. Absorbed PHMG and PGH by the sampler were quantified using a spectrophotometric method, and high performance liquid chromatography-ultraviolet detection was used for CMIT/MIT. Three exposure scenarios were assumed for adding humidifier disinfectants to the humidifier water at 1, 2, and 10 times the volume recommended by the product suppliers, and the humidifier was on at its maximum rate of producing aerosols in order to consider reasonable worst-cases. The sampled mass of PHMG and PGH ranged 200 to $2,800{\mu}g$ and 140 to $1,900{\mu}g$, respectively, under different exposure conditions, whereas the absorbed mass of CMIT/MIT was barely detected at the detection limit of 0.11/0.29 mg/L, only at 10 times the recommended level. The resulting risk quotients for PHMG and PGH ranged 1,400 to 20,000 and 1,000 to 13,000, indicating that health risks could be significant. For CMIT/MIT mixture, risk quotients were much smaller than estimated by assuming that they are conservative in the indoor environment, probably due to oxidative reactions. The refined exposure assessment presented here may provide a useful tool for assessing risks posed by active ingredients in spray-type biocidal products.

Analysis of 1,4-Dioxane and Chlorohydrins in Food Additives by Purge & Trap GC (퍼지앤트랩-기체크로마토그래피(PT-GC)를 이용한 식품첨가물 중 1,4-디옥산 및 클로로히드린류 분석)

  • 조태용;신영민;반경녀;오세동;이창희;이영자;문병우
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.32 no.7
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    • pp.965-970
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    • 2003
  • This study has been performed to develope a method for the simultaneous determination of 1,4-dioxane (DOX), epichlorohydrin (EPC), propylene chlorohydrin (PCH), ethylene chlorohydrin (ECH) and 1,3-dichloro-2-pro-panol (DCP) in polysorbates, chloline chloride, choline bitartrate, modified starch and spices by purge and trapgas chromatography. Experimental design was used to select a suitable trap by measuring the limit of detection (LOD) and to investigate the effect of temperature and salt of extraction, and the percentage of recovery in various matrix. The LOD of DOX, EPC, PCH, ECH and DCP were 1.38$\mu\textrm{g}$, 0.23$\mu\textrm{g}$, 3.30$\mu\textrm{g}$, 3.97$\mu\textrm{g}$, 20.43$\mu\textrm{g}$ respectively, by means of using Vorcarb 3000 trap with 5$0^{\circ}C$ sample sparger. Excluding EPC, the recoveries of target compounds were above 90% in all matrix. Target compounds in polysorbates (17), choline chloride (5), choline bitartrate (5), modified starch (8) and spices (25) were not detected. But 2.5 ppm of DOX was detected in Tween 80.

Validation of enzyme immunoassay for the quantitative measurement of human IgG antibodies specific for Haemophilus influenzae Type b capsular polysaccharide (Haemophilus influenzae type b 피막 다당질 특이 인간 IgG 항체의 정량적 측정을 위한 enzyme immunoassay의 타당성 연구)

  • Kim, Kyung Hyo;Lim, Soo Young
    • Clinical and Experimental Pediatrics
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    • v.50 no.2
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    • pp.143-150
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    • 2007
  • Purpose : This study was conducted to validate enzyme immunoassay (EIA) for the quantitative measurement of human IgG antibodies specific for Haemophilus influenzae type b (Hib) capsular polysaccharide. Method : We evaluated specificity, repeatability, intermediate precision, accuracy, lower limit of quantification (LLOQ), and stability to validate standardized EIA for the quantitative measurement of human anti-polyribosylribitol phosphate (PRP) IgG antibodies. Results : The results indicated that this EIA showed specificity to HbO-HA antigen and repeatability and intermediate precision were within acceptance criteria (repeatability: $CV{\leq}15%$, intermediate precision: $CV{\leq}20%$). The EIA-derived results from this laboratory were equivalent to those obtained by the standard radioactive antigen binding assay (RABA) for quantitation of anti-PRP antibodies in the 28 sera. Spiking recovery result was within acceptance criteria ($100{\pm}20%$). The precision and accuracy of samples in LLOQ were from -14.7 to -4.7% in nominal values, which were within acceptance criteria (precision: $CV{\leq}25%$, accuracy: ${\pm}25%$). Freeze-thaw stability and short term temperature stability were within ${\pm}20%$ of acceptance criteria. Conclusions : The EIA which is performed at the Center for Vaccine Evaluation and Study Ewha Medical Research Institute, is an appropriate serologic assay which can be used for quantitation of anti-PRP IgG antibodies in human sera.

Microwave Digestion and Solid-Phase Extraction for Determination of Aluminum in Human Urine by Graphite Furnace Atomic Absorption Spectrometer (흑연로 원자흡수 분광법에 의한 사람 오줌 중 알루미늄의 정량을 위한 마이크로파 삭힘과 고체상 추출)

  • Kim, Young-Sang;Choi, Yoon-Seok
    • Analytical Science and Technology
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    • v.16 no.2
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    • pp.102-109
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    • 2003
  • Microwave digestion and solid-state extraction were studied for determination of trace aluminum{Al(III)} in human urine samples. A mixed acid of nitric acid and hydrogen peroxide was added to urine samples, organic materials were destructed in a home microwave oven and dried in a drying oven. The dried residues were dissolved in a sulfuric acid solution. The solution was eluted through a XAD-4 resin column adsorbed with 8-hydroxyquinoline(Oxine, HQ). Al(III)-8-hydroxyquinolinate complex was formed in the column and eluted with 0.5 M nitric acid solution. The Al(III) eluted was determined by graphite atomic absorption spectrophotometry. Various experimental conditions of followings were investigated for the optimization : the type of acid to dissolve the residues, the amount of HQ adsorbed on the resin, the pH of sample solutions, the type and concentration of acid to elute the complex from column and so on. The contents of Al(III) in real samples were determinated by a calibration curve method. The recovery in standard spiked samples was 94~101% and the detection limit of this procedure was 0.05 ng/mL.

Effects of Blood Flow Restriction Exercise on the Alacrity and Balanced Capacity of Female University Students in Their 20s for Health-Care Increase (헬스케어증진을 위한 하지혈류제한운동이 20대 여대생의 순발력과 균형에 미치는 영향)

  • Seo, Tae-Hwa;Kim, Eun-Ho;Jeong, Yeon-Woo
    • Journal of Korea Entertainment Industry Association
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    • v.14 no.4
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    • pp.333-340
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    • 2020
  • This study aims to examine the effects of squat exercise on the vitality and balanced capacity of female university students in their 20s with lower blood flow control. This study selected 40 volunteers from normal adult women in their twenties. Blood flow restriction used Blood Flow Restriction bands (BFR bands). The application method was to put on a blood flow restriction belt in the lower leg of the restricted blood flow area and put 120 mmHg of pressure to limit blood flow while the subject was standing comfortably. It was found that there were statistically significant differences in Height, Maximum concentric power and Take off speed between two groups(p<.05), There was statistically unimportant differences in foot scan between two groups(p>.05). This study found that to find out the changes in balance and alacrity, the experimental and control groups were divided into two groups. In conclusion, there were no significant differences in balance capability, but there were significant differences over time in net power.

Study on Uncertainty Factors of Head Vibration Measurements (머리 진동 측정치의 불확도 인자들에 관한 연구)

  • Cheung, Wan-Sup;Kim, Young-Tae;Ryu, Je-Dam;Hong, Dong-Pyo
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.15 no.1 s.94
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    • pp.20-28
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    • 2005
  • This paper addresses uncertainty issues encountered recently in measuring head vibration using the conventional 6-axis or 9-axis bite-bar model. Those conventional bite-bar models are shown to present insufficient information to evaluate a generalized motion of head vibration. In order to overcome such limit, a new theoretical measurement model that consists of four 3-axis linear accelerometers is suggested. It is shown to enable the measurement of three angular acceleration components and six second-order angular velocity-dependent terms. Those nine angular motion-related ones, in addition to the three linear acceleration terms at the origin, are found to make it possible to evaluate the generalized head vibration for a given position. To examine the feasibility of the proposed method, a newly designed 12-axis bite-bar was developed. Detailed experimental results obtained from the developed 12-axis bite-bar are demonstrated in this paper. They illustrate that the popular 6-axis bite-bar model yield about $4.0\%$ relative measurement uncertainty for the pitch component of head vibration, $14\%$ and $10\%$ relative measurement uncertainty for the roll and yaw components of head vibration, respectively. Furthermore, this paper proposes other uncertainty factors to be considered in the future.

Prediction of Expected Residual Useful Life of Rubble-Mound Breakwaters Using Stochastic Gamma Process (추계학적 감마 확률과정을 이용한 경사제의 기대 잔류유효수명 예측)

  • Lee, Cheol-Eung
    • Journal of Korean Society of Coastal and Ocean Engineers
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    • v.31 no.3
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    • pp.158-169
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    • 2019
  • A probabilistic model that can predict the residual useful lifetime of structure is formulated by using the gamma process which is one of the stochastic processes. The formulated stochastic model can take into account both the sampling uncertainty associated with damages measured up to now and the temporal uncertainty of cumulative damage over time. A method estimating several parameters of stochastic model is additionally proposed by introducing of the least square method and the method of moments, so that the age of a structure, the operational environment, and the evolution of damage with time can be considered. Some features related to the residual useful lifetime are firstly investigated into through the sensitivity analysis on parameters under a simple setting of single damage data measured at the current age. The stochastic model are then applied to the rubble-mound breakwater straightforwardly. The parameters of gamma process can be estimated for several experimental data on the damage processes of armor rocks of rubble-mound breakwater. The expected damage levels over time, which are numerically simulated with the estimated parameters, are in very good agreement with those from the flume testing. It has been found from various numerical calculations that the probabilities exceeding the failure limit are converged to the constraint that the model must be satisfied after lasting for a long time from now. Meanwhile, the expected residual useful lifetimes evaluated from the failure probabilities are seen to be different with respect to the behavior of damage history. As the coefficient of variation of cumulative damage is becoming large, in particular, it has been shown that the expected residual useful lifetimes have significant discrepancies from those of the deterministic regression model. This is mainly due to the effect of sampling and temporal uncertainties associated with damage, by which the first time to failure tends to be widely distributed. Therefore, the stochastic model presented in this paper for predicting the residual useful lifetime of structure can properly implement the probabilistic assessment on current damage state of structure as well as take account of the temporal uncertainty of future cumulative damage.