• KSBB Journal
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• 제31권2호
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• pp.100-104
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• 2016

Dolsan leaf mustard has various biological functions, including those in the immune system and cancer prevention. It contains high amounts of nutritional and medicinal compounds, which are important for maintaining optimum health. The objective of this study was to determine the total phenolics contents and antioxidant activity in Dolsan leaf mustard pickle (DLMP) during storage. DLMP methanol extracts had the highest total polyphenol and flavonoid contents of $35.56{\pm}0.01GAEmg/g$ and $4.54{\pm}0.03QEmg/g$, respectively. The DPPH and ABTS radical scavenging activities in the DLMP methanol extracts showed the highest activities of 79.4 and 85.36%, respectively. The ferric reducing antioxidant power (FRAP) assay showed 2.24-3.82 mM $FeSO_4$ eq. (p<0.05) in DLMP extracts. Overall, storage at day 14 showed the highest antioxidant activity.

• KSBB Journal
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• 제31권1호
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• pp.20-26
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• 2016

This study aims to examine the optimum blanching conditions as a pretreatment condition to improve the storage stability of Dolsan leaf mustard pickle. The effects of the blan- ching temperature and time were investigated at a temperature range of $80-100^{\circ}C$. Sampling was done for 1 month after a 5 days interval. The L value of the Dolsan leaf mustard was found to be the highest at $80^{\circ}C$. The cutting force increased as the blanching temperature increased. The tensile strength decreased at $95^{\circ}C$ and $100^{\circ}C$. In addition, the sensory evaluation scores were the best at $80^{\circ}C$. The storage stability was assessed at various blanching temperatures to increase the sinigrin content during storage. Liquid chromatography with photodiode array and tandem mass spectrometry (LC-PDA/MS/MS) analysis was conducted to identify and quantify the sinigrin content in the Dolsan leaf mustard. Sinigrin as an internal standard was co-injected into each sample solution. The sample was monitored by recording the ultraviolet absorbance at 228 nm and by electrospray ionization (ESI) positive ion mode in the m/z 50-1,500 range. Blanching the sample at $80^{\circ}C$ showed the highest sinigrin concentration during storage among various temperatures and the maximum concentration was 350 ppm at 15 days storage. Study on utilization of vegetable from food processing of leaf mustard and preservation conservation results suggest that blanching at $80^{\circ}C$ is expected to improve the palatability of the pickle.

• KSBB Journal
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• 제31권3호
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• pp.165-170
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• 2016

This study was carried out for investigate that physiological activity, quantification and qualitative were sinigrin of Dolsan leaf mustard pickle (DLMP) during storage. sinigrin contains high amounts of nutritional and medicinal compounds, which are important for maintaining optimum health. ACE inhibitory activity was ranged between 43.2 and 79.4%. DLMP methanol extracts demonstrated highest ACE inhibitory activity at 79.4% on day 14, whereas DLMP ethanol extracts demonstrated highest Angiotensin I-converting Enzyme (ACE) inhibitory activity of 43.2% at day 0. The ${\alpha}-glucosidase$ inhibitory activity of positive control 0.02% (v/v) acarbose was 78%. The DLMP methanol extracts had the highest ${\alpha}-glucosidase$ inhibitory activity at 64.0% on day 14, whereas DLMP ethanol extracts had the lowest ${\alpha}-glucosidase$ inhibitory activity of 42.8% at day 28. Sinigrin was high in DLMP methanol extracts at $49.55{\mu}g/ml$ on day 14 of storage. Sinigrin standard was eluted at 2.73 min and MS analysis was m/z 283.03 along with fragment ions at m/z 204 and 149.06. These data show that sinigrin formed desulfo-glucosinolates $[M-SO_3-2H_2O+K+2H]^+$. Sinigrin concentration increased until day 14 and then decreased after that. DLMP methanol extracts had consistently higher sinigrin concentration than DLMP acetonitrile extracts during 28 days of storage.

• KSBB Journal
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• 제31권1호
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• pp.1-7
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• 2016

Changes in the concentrations of glucosinolates and related compounds in different extracts of Dolsan leaf mustard kimchi (DLMK) and Dolsan leaf mustard pickles (DLMP) were during storage investigated. Samples were kept at 0oC for 35 days and collected at 7 day intervals. The leaves and stems of DLMK and DLMP were refluxed for 24 h with 50% acetonitrile, and the extracts were analyzed by LC-PDA/MS/MS. The main glucosinolates detected in DLMK were sinigrin, gluconapoleiferin, glucobrassicanapin, and gluconapin, whereas those in DLMP were sinigrin, gluconapoleiferin, glucobrassicanapin, glucobrassicin, and glucoerucin. Sinigrin concentrations were quantified by UV absorption at 228 nm. Sinigrin concentrations in the leaves and stems of DLMK on the day of preparation were 2.14 mg/g and 2.25 mg/g, respectively, and those on day 35 after preparation were 1.25 mg/g and 1.00 mg/g, respectively. DLMP showed a similar trend: the concentrations in the leaves and stems on the day of preparation were 2.04 mg/g and 0.29 mg/g, respectively, whereas those on day 35 after preparation were 0.59 mg/g and 0.41 mg/g, respectively. Thus, sinigrin concentrations decreased during storage.

• 한국식품과학회지
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• 제44권5호
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• pp.545-552
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• 2012

3% 이하의 저염 농도에서 맛, 향미 및 저장성을 높이기 위하여 갓과 고추를 첨가한 야콘 피클의 저장 중 품질특성을 이요인 분산분석을 이용하여 품질 특성을 분석한 결과는 다음과 같다. 당도, 총산도 및 염도는 갓과 고추 첨가에 따라 시료간에 유의적인 차이가 있었고, 저장기간에 따라서도 시료간에 유의한 차이가 있었다. 갓과 고추 첨가와 저장기간에 따른 상호작용 효과도 나타났으며, 저장기간이 길어질수록 모든 시료에서 당도, 총산도 및 염도는 증가하였다. 색도에서 L값은 갓과 고추 첨가에 따른 시료간에 차이는 없었으나, 저장기간에 따라서는 유의적인 차이가 있었다. a값과 b값은 갓과 고추 첨가에 따른 시료간 차이와 저장 기간에 따른 차이에서 모두 유의적으로 나타났으며, L, a 및 b값 모두 갓과 고추 첨가와 저장기간에 따른 상호작용 효과가 나타났다. 저장기간 동안 야콘 피클의 절단력은 갓과 고추 첨가와 저장기간에 따른 시료간에 차이가 없어 연부현상은 나타나지 않은 것으로 보여진다. 관능검사에서 색, 맛과 전체적인 선호도는 갓과 고추 첨가와 저장기간에 따라서 각각 유의적인 차이가 있었다. 향미는 저장기간에 따른 차이만 나타났고, 질감은 갓과 고추 첨가와 저장기간에 따라서도 유의적인 차이가 없는 것으로 나타났다. 저염 야콘 피클은 저장 30일과 40일에 전체적인 선호도가 높았고, 갓과 고추를 첨가한 야콘 피클은 다른 시료보다 선호도가 높았다. 부재료 첨가 유무와 저장기간에 따른 상호작용 효과는 전체적인 선호도에서만 나타났다.

• 생명과학회지
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• 제25권8호
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• pp.936-941
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• 2015

본 연구에서는 돌산 갓을 이용하여 저염 피클을 개발하기 위한 기초적인 연구로 저장기간 중 이화학적 및 관능 변화에 대해 분석하였다. 돌산 갓 피클을 −2℃에서 90일 동안 저장하였다. 염도는 1.63~1.85% 범위를 유지하였다. pH는 저장 0일째 약 4.5에서 저장 90일째 4.37로 감소하였다. 산도는 저장기간 중 60일째까지 점진적으로 증가하다가 이후 약 1.10%로 급격히 증가하였다. 색도의 L값은 잎에서 30일째까지 증가하였다가 이후 감소하였고, 줄기에서는 저장기간 동안 감소하였다. 저장기간 동안 a값은 증가하였고, 반면에, b값은 감소하여 갈변 현상이 진행된 것을 알 수 있었다. 유산균 수는 0일째 DMP잎에서 1.4×10³ CFU/ml, DMP 줄기에서 5.6×10³ CFU/ml로 나타났고 이후 점차 감소하였다. 관능검사 결과는 아삭거림이 30일째 감소하였고, 질긴 정도는 증가하였다. 신맛은 증가하였고, 짠맛은 감소하였다. 90일간 저장기간 동안에도 연부현상이 발생하지 않았다. 그래서 최적의 돌산 갓 피클은 30일째 적합하다고 판단되며 돌산 갓은 저염 피클제품으로서의 이용 가능성을 제시하고, 수입 위주의 피클을 대체함과 동시에 돌간 갓을 이용한 식품의 다양화에 기여하고자 분석을 실시하였다.