• 제목/요약/키워드: LC material

검색결과 544건 처리시간 0.025초

속새(Equisetum hyemale) 추출물의 항산화 물질의 HPLC 분획과 LC-MS를 이용한 지표성분 분석 (HPLC Fractionation of Antioxidant Substances of E. hyemale Extract and Analysis of Indicator Components Using LC-MS)

  • 송진화;이거룡
    • 한국자연치유학회지
    • /
    • 제10권2호
    • /
    • pp.108-113
    • /
    • 2021
  • 배경: 속새 줄기와 뿌리의 추출물에서 항산화 물질의 작용에 관한 결과를 이미 보고하였으나 항산화 성분은 분석되지 않았다. 목적: 속새 줄기와 뿌리 부분의 성분을 추출한 물질들이 항산화 물질의 분자 구조를 확인하는 것이었다. 방법: 성분분석은 열수와 에틸알코올로 추출하여 HPLC와 LC-MS로 분석하였다. 결과: 속새 줄기와 뿌리 추출물의 HPLC 크로마토그램은 파장 205 nm에서 4개의 중요한 peak가 나타났다. 280 nm에 있는 peak 1번은 전형적인 단순 페놀릭형이고, 모두 280 nm와 370 nm 근처에 있는 peak 2~4는 전형적인 플라보노이드 배당체의 형태임을 알 수 있었다. HPLC 분석에 의한 추출물의 항산화도는 740 nm에서 peak의 합은 100% 에탄올 추출물이 3,669 mAU로 제일 높았고, 70% 에탄올 추출물은 3,096 mAU, 열수추출물은 2,868 mAU로 제일 낮았다. 항산화성 추출 물질을 LC-MS 분석한 결과는 peak 3에서는 분자량이 772 da인 kaempferol-3-sophoroside-7-glucoside, peak 4에서는 분자량이 788과 772인 물질 kaempferol-3- sophoroside- 8-glucoside가 확인되었다. 결론: 속새의 항산화 추출물에 항산화 성분이 존재하는 것이 확인되어 속새가 기능성 화장품의 원료로서 가능성이 높아 졌다고 본다.

광나무 열매 발효 추출물의 항염 및 항산화 활성 (Anti-inflammatory and Anti-oxidative Activities for Extract of Fermented Ligustrum japonicum Fruits)

  • 김정은;김소희;김미애;고미선;신찬성;이남호
    • 대한화장품학회지
    • /
    • 제49권2호
    • /
    • pp.117-125
    • /
    • 2023
  • 본 연구에서는 광나무(Ligustrum japonicum) 열매 발효 추출물의 항염 및 항산화 효능을 비발효 추출물과 비교 분석하였다. 광나무 열매의 발효는 제주 자리돔(Chromis notata) 내장에서 분리한 Latilactobacillus curvatus (L. curvatus) 및 Weisella minor (W. minor) 균주를 이용하였으며, 각각의 발효 추출물(LJF-LC 및 LJF-WM)의 수율은 40.5 ~ 46.0%로 비발효 추출물(LJF)의 29.5% 보다 높게 나타났다. Lipopolysaccaride(LPS)로 자극된 RAW 264.7 대식세포를 이용한 nitric oxide (NO) 생성 억제 활성 실험 결과, 발효 추출물인 LJF-WM이 세포 독성 없이 농도 의존적으로 NO의 생성을 저해시키는 효과가 우수함을 확인하였다. 또한 DPPH 및 ABTS+ 라디칼 소거 활성 실험 결과, 발효 추출물의 라디칼 소거 활성이 비발효 추출물과 유사하게 나타났으며, 발효 추출물 LJF-WM은 과산화수소(H2O2)로 유도된 세포 손상에 대한 세포보호 효과를 보였다. 광나무 열매의 주성분인 salidroside의 함량을 HPLC를 이용하여 분석한 결과, 발효 추출물 LJF-LC에서 15.6 mg/g, LJF-WM에서 13.9 mg/g으로 확인되어 비발효 추출물(12.0 mg/g) 보다 함유량이 높게 분석되었다. 이상의 연구 결과를 바탕으로 광나무 열매 발효 추출물은 항염 및 항산화 효과를 갖는 천연 화장품 소재로써 활용 가능할 것이라 사료된다.

고융점 금속의 미소형상 정밀주조를 위한 탄소몰드의 적용성에 관한 연구 (A Study on the Applicability of Carbon Mold for Precision Casting of High Melting Point Metal)

  • 지창욱;이은주;김양도;임영목
    • 한국분말재료학회지
    • /
    • 제18권2호
    • /
    • pp.141-148
    • /
    • 2011
  • Carbon material shows relatively high strength at high temperature in vacuum atmosphere and can be easily removed as CO or $CO_2$ gas in oxidation atmosphere. Using these characteristics, we have investigated the applicability of carbon mold for precision casting of high melting point metal such as nickel. Disc shape carbon mold with cylindrical pores was prepared and Ni-base super alloy (CM247LC) was used as casting material. The effects of electroless Nickel plating on wettability and cast parameters such as temperature and pressure on castability were investigated. Furthermore, the proper condition for removal of carbon mold by evaporation in oxidation atmosphere was also examined. The SEM observation of the interface between carbon mold and casting materials (CM247LC), which was infiltrated at temperature up to $1600^{\circ}C$, revealed that there was no particular product at the interface. Carbon mold was effectively eliminated by exposure in oxygen rich atmosphere at $705^{\circ}C$ for 3 hours and oxidation of casting materials was restrained during raising and lowering the temperature by using inert gas. It means that the carbon can be applicable to precision casting as mold material.

구치부 복합레진 수복을 위한 와동 이장용 재료의 방사선투과성에 관한 연구 (A Study on the Radiopacity of Cavity Lining Materials for Posterior Composite Resin Restoration)

  • 문주훈;최의환
    • Imaging Science in Dentistry
    • /
    • 제30권4호
    • /
    • pp.243-248
    • /
    • 2000
  • Purpose: The aim of this study was to determine the relative radiopacities of cavity lining materials (Resin-modified Glass Ionomer cement, Compomer and Plowable resin) for posterior composite resin restoration. Material & Methods: Resin-modified glass ionomer cement (Fuji II LC, Vitrebond/sup TM/), Compomers (Dyract /sup (R)/ Compoglass, F2,000, Dyract/sup (R)/ flow Compoglass Flow) and Flowable resins (Tetric/sup (R)/ flow, Aeliteflo/sup TM/ Revolution/sup TM/) were used. Five specimens of 5 mm in diameter and 2 mm thick were fabricated with each material. Human molars were horizontally sectioned 2 mm thick to include both enamel and dentin. The radiopacities of enamel, dentin, cavity lining materials, aluminum step wedge were obtainded from conventional radiograph and NIH image program. Results: All the tested lining materials showed levels of radiopacity the same as or greater than that of dentin. All compomer tested (Dyract, Compoglass, F2,000, Dyract flow, Compoglass Flow) and Vitrebond/sup TM/, Tetric/sup (R)/ flow were more radiopaque than enamel. The radiopacities of Fuji II LC and Revolution/sup TM/ were between enamel and dentin and resin-modified glass ionomer cement, Compomer and Tetric/sup (R)/ flow were greater than those of Revolution/sup TM/, Aeliteflo/sup TM/ or dentin. The level of radiopacity of the tested materials was variable; those with low radiopacity should be avoided in class II restorations, where a clear determination of recurrent caries by the examining clinician could be compromised. Conclusion: Clinician should be able to distinguish these cavity lining materials radiographically from recurrent decay, voids, gaps, or other defects that lead to clinical failure. Utilization of materials ranked more radiopaque than enamel would enable clinicians to distinguish the lining material from tooth structure.

  • PDF

Comparison of Shear Bond Strength in Novel Calcium Silicate-Based Materials to Composite Resin

  • Wonkyu Shin;Hyuntae Kim;Ji-Soo Song;Teo Jeon Shin;Young-Jae Kim;Jung-Wook Kim;Ki-Taeg Jang;Hong-Keun Hyun
    • 대한소아치과학회지
    • /
    • 제50권4호
    • /
    • pp.443-451
    • /
    • 2023
  • The purpose of this study was to evaluate whether the newly introduced calcium silicate-based materials with fast-setting properties could be appropriately used as basement materials in indirect pulp treatment (IPT). This was performed by quantifying the durability of adhesion between the material and composite resin, measured by the shear bond strength (SBS). Five calcium silicate-based materials, TheraCal LC® (TLC), TheraCal PT® (TPT), TheraBase® (TB), Well-RootTM PT (WPT), and Endocem® MTA (EMTA), as well as two glass ionomer-based materials, Fuji II and Fuji II LC, were included. Specimens containing these materials were manufactured and bonded to composite resin with a universal adhesive applied in self-etch mode. The SBS values and failure modes were recorded, and the mean SBSs of the materials were compared. Both TPT and TB exhibited SBS values that were similar to TLC, while both WPT and EMTA appeared to have statistically lower SBS values. Mixed failure was commonly observed in TLC and TPT, while all WPT and EMTA samples showed cohesive failure. In comparison with TLC and TPT, more samples with cohesive failure were observed in TB, implying that this material forms a stronger bond with composite resin. Together with the ability of TB to chemically bind to dentin due to its 10-methacryloyloxydecyl dihydrogen phosphate component, TB seems to be a promising material for IPT within the limitations of this in vitro study.

이종적층 LTCC 기술을 이용한 WLAN용 대역통과 필터 설계 (Design of BPF for WLAN with Heterogeneous LTCC Materials)

  • 고정호;육종관;박한규;김준철;이영신
    • 한국전자파학회:학술대회논문집
    • /
    • 한국전자파학회 2003년도 종합학술발표회 논문집 Vol.13 No.1
    • /
    • pp.188-192
    • /
    • 2003
  • A multilayer two-stage LC bandpass filter using low-temperature cofired-ceramic (LTCC) is proposed in this paper. The proposed bandpass filter is composed of two ceramic substrates with different dielectric constant instead of single ceramic material from top to bottom layer. The bandpass filter size is $2.0 mm{\times}1.2 mm{\times}0.8 mm$. Positioning of attenuation polefrequency, importance parameter for a performance of filter, is discussed using even-odd mode analysis by tuned capacitance of coupling capacitor and those results is implemented to LTCC filter circuit. Measured filter performances show that the insertion losses are -4.5dB, -4.1dB at 2.45GHz, 2.75GHz and the return losses are -8.5dB, 8.7dB.

  • PDF

고분자 분산형 액정 표시소자의 전기광학적 특성 개선 (Improvement in the electro-optical properties of PDLCs)

  • 최기석;박우상;박세근
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
    • /
    • pp.125-128
    • /
    • 1998
  • The electro-optical properties of PDLCs ( Polymer Dispersed Liquid Crystals ) that have been interested for applications to projection display devices lately are significantly improved. For this improvement, we optimized not only the material parameters of liquid crystal and polymer but also the process conditions. Using TL series liquid crystals and polymer PN393 provided from Merck, we obtained the optimized process conditions such as cell gap, LC concentration, curing temperature and curing time. Under these conditions, we have achieved PDLC cells of threshold voltage 2.6V. contrast ratio 260 and negligible hysteresis.

  • PDF

단일갭 반투과 FFS 액정 디스플레이를 위한 최적 화소 디자인 (Optimal Pixel Design for Low Driving Single Gamma Curve and Single Gap Transflective Fringe Field Switching Display)

  • 정연학;임영진;정은;이승희
    • 한국전기전자재료학회논문지
    • /
    • 제20권12호
    • /
    • pp.1068-1071
    • /
    • 2007
  • When a dielectric layer, in-cell retarder (ICR) is formed between electrode and LC layer to get a single gap transflective fringe-field switching (FFS) display, the operating voltage ($V_{op}$) is highly increased due to the thickness of dielectric material. But, we also knew the phenomenon that the increasing rate of Vop is different whether the 1st common electrode was composed of plate type or slit type. In this paper, the common electrode in transmissive part was composed of slit type which had less steepness effect of the Vop and in reflective part was composed of plate type. The rubbing angle of reflective part can be adjusted properly to match the voltage dependent transmittance and reflectance.

Chalconyl과 Cholesteryl기를 함유한 광폴리머의 테마틱 액정의 배향 (Alignment capabilities of nematic liquid crustal using a photo-polymer containing chalconyl and cholesteryl moiety)

  • 황정연;서대식
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2000년도 하계학술대회 논문집
    • /
    • pp.835-838
    • /
    • 2000
  • A new photo-alignment material, copoly (PM4Ch-ChMA), copoly (poly (4-methacryloyloxy) chalcone-cholesterol methacrylate) was synthesized and the electro-optical (EO) characteristics for the photo-aligned vertical-aligned (VA)-LC display (LCD) were studied. Good voltage-transmittance (V-T) and response time characteristics for the photo-aligned VA-LCD with polarized UV exposure on the copolymer-1 (2%) surfaces for 1 min. were observed. EO performance for the photo-aligned VA-LCD decreased with increasing UV exposure time on a copolymer surface. Also, excellent V-T and response time characteristics for the photo-aligned VA-LCD with UV exposure on copolymer-2 and copolymer-3 surfaces for 3min. can be achieved.

  • PDF

단일랩 반투과 FFS 액정 디스플레이를 위한 최적 화소 디자인 (Optimal pixel design for low driving single gamma curve and single gap transflective fringe field switching display)

  • 정연학;임영진;정은;이승희
    • 한국전기전자재료학회:학술대회논문집
    • /
    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
    • /
    • pp.435-436
    • /
    • 2007
  • In general, Single gap transflective FFS display has an in-cell retarder (ICR) between reflective electrode and liquid crystal (LC) layer. Therefore, Operating voltage is highly increased due to this thick dielectric material. But, we also knew the phenomenon that the increasing rate of Vop is different whether the 1st common electrode was composed of plate type or slit type. In this paper, the common electrode in transmissive part was composed of slit type which had less steepness effect of the V op and in reflective part was composed of plate type. The rubbing angle of reflective part can be adjusted properly to match the voltage dependent transmittance and reflectance.

  • PDF