• 제목/요약/키워드: L1 Phase

검색결과 2,522건 처리시간 0.027초

Formation of Ti-B-N-C Ceramic Composite Materials via a Gas-Solid Phase Reaction

  • Yoon, Su-Jong
    • 한국재료학회지
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    • 제16권1호
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    • pp.50-57
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    • 2006
  • Phase mixtures of Titanium boride, nitride, and carbide powder were produced by the reduction of a mixture of titanium and boron oxides with carbon via a gas-solid phase reaction. Boron oxides produce a vapour phase or decompose to a metal sub-oxide gaseous species when reduced at elevated temperature. The mechanism of BO sub-oxide gas formation from $B_2O_3$ and its subsequent reduction to titanium diboride for the production of uniform size hexagonal platelets is explained. These gaseous phases are critical for the formation of boride, nitride and carbide ceramics. For the production of ceramic phase composite microstructures, the nitrogen partial pressure was the most critical factor. Some calculated equilibrium phase fields has been verified experimentally. The theoretical approach therefore identifies conditions for the formation of phase mixtures. The thermodynamic and kinetic factors that govern the phase constituents are also discussed.

B2-규칙 NiAl계에 $L2_1$$Ni_2AlTi$상의 석출거동에 관한 연구 (A Study on the Precipitation Behavior of $L2_1$-type $Ni_2AlTi$ Phase in B2-Ordered NiAl System)

  • 한창석
    • 열처리공학회지
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    • 제20권4호
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    • pp.187-194
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    • 2007
  • A transmission electron microscope (TEM) investigation has been performed on the precipitation of $L2_1$-type $Ni_2AlTi$ phase in B2-ordered NiAl system. The hardness after solution treatment is high in NiAl-Ti alloys suggesting the large contribution of solid solution strengthening in this alloy system. However, the amount of age hardening is not large as compared to the large microstructural variations during aging. At the beginning of aging, the $L2_1$-type $Ni_2AlTi$ precipitates keep a lattice coherency with the NiAl matrix. By longer periods of aging $Ni_2AlTi$ precipitates lose their coherency and change their morphology to the globular ones surrounded by misfit dislocations. Misfit dislocations, which are observed on {100} planes of H-precipitates have the Burgers vector of a <100> with a pure edge type. The lattice misfits of NiAl-$Ni_2AlTi$ system is estimated from the spacings of misfit dislocations to be 1.1% at 1273 K. The lattice misfits decrease with increasing aging temperature in this system.

무반사 코팅된 DFB 레이저 다이오드에서 발진 모드와 격자 위상 (Oscillation Mode and Grating Phase in DFB Laser Diode with an Anti-reflection Coated Mirror)

  • 권기영;기장근
    • 문화기술의 융합
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    • 제8권5호
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    • pp.483-488
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    • 2022
  • 본 연구에서는 1.55um의 파장을 갖는 DFB 레이저 다이오드에서 이득 격자와 굴절률 격자가 동시에 존재할 때, 오른쪽 거울면에 무반사 코팅을 하여 ρr=0 이 되도록 하였다. δL<0인 경우일 때, 발진 모드에 대하여, 발진 주파수와 발진 이득의 특성을 해석했다. 좌측 거울면 상에서 격자의 위상이 π에서부터 π/2씩 연속적으로 감소할 때마다, 각 발진 모드의 (αL, δL) 그래프 선들이 좌측으로 δL 값이 약 0.6 정도씩 낮아지고 있음을 볼 수 있다. 문턱이득이 가장 낮은 발진 모드의 경우는 κL=10인 경우이고, 이때 모드 선별성은 다른 κL 값의 경우와 비교할 때 상대적으로 낮다. 모드 선별성이 우수한 경우는 κL=0.1 에서부터 κL=6 정도까지이고, 모드 선별성이 우수할수록 주파수 안정성이 우수하다. 두 개의 벽개면을 갖는 경우와 비교하면, 무반사 코팅을 한 DFB 레이저 다이오드는, 발진 모드의 문턱 이득은 약 2배 정도로 높아지지만 모드 선별성 측면은 2배 정도 더 우수해 진다.

황체기단축현상을 가진 한국여성의 호르몬양(II);혈청 Prolactin의 변동 (The Hormonal Levels of the Short Luteal Phase in Korean Women(II);Change of Serum Prolactin)

  • 윤용달;이준영
    • Clinical and Experimental Reproductive Medicine
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    • 제11권2호
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    • pp.5-15
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    • 1984
  • 본 연구는 황체기 단축현상(Short luteal phase, SLP) 을 가진 한국여성의 월경주기내 Prolactin 호르몬의 농도변화를 정상월경주기 (Normal luteal phase, NLP)와 비교하고져 하였다. 한편, Circadian rhythm 내 PRL 농도의 변화를 비교하고 임신기간중 PRL의 농도변화를 방사면역측정법(RIA) 으로 조사하였다. SLP여성의 PRL 농도는 후기의 여포성숙기(Late follicular phase) 및 초기황체형성기(Early IuteaI phase) 정상에 비하여 현저히 낮았다. 정상 월경주기에서는 PRL/Progesterone(mU/1/mg/ml)의 비율이 후기 여포성숙기까지 증가한 후 LH Peak day 이후 감소하는데 반하여 SLP여성의 비율은 조기 여포성숙기부터 계속적인 감소현상을 보였다. 또한 취침전 (04:00시) PRL의 농도는 SLP여성에게는 현저히 낮았다. 임신주기중 PRL의 농도는 4개월째 1,077mU/l 에서부터 9개월째 4,462mU/l까지 점진적인 증가를 하였다. 위의 결과로 보아 황체기단축현상은 PRL의 분비이상이 하나의 주요요인이 될 수 있으며, 특히 PRL/Progesterone의 농도비율이 SLP의 판정에 한 지표가 될 수 있을 것으로 사료된다.

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Baseline Refinement for Topographic Phase Estimation using External DEM

  • Lee, Chang-Won;Moon, Wooil-M.
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2002년도 Proceedings of International Symposium on Remote Sensing
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    • pp.460-464
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    • 2002
  • Multitemporal interferometric SAR has became an useful geodetic tool for monitoring Earth's surface deformation, generation of precise DEM, and land cover classification even though there still exist certain constraints such as temporal and spatial decorrelation effects, atmospheric artifacts and inaccurate orbit information. The Korea where nearly all areas are heavily vegetated, JERS-1 SAR has advantages in monitoring surface deformations and environmental changes in that it uses 4-times longer wavelength than ERS-l/2 or RADARSAT SAR system. For generating differential SAR interferogram and differential coherence image fer deformation mapping and temporal change detection, respectively, topographic phase removal process is required utilizing a reference inteferogram or external DEM simulation. Because the SAR antenna baseline parameter for JERS-1 is less accurate than those of ERS-l/2, one can not estimate topographic phases from an external DEM and the residual phase appears in differential interferogram. In this paper, we examined topographic phase retrieval method utilizing an external DEM. The baseline refinement is carried out by minimizing the differences between the measured unwrapped phase and the reference points of the DEM.

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L1/L2 이중-밴드 GPS 수신기용 RF 전단부 설계 (Design of the RF Front-end for L1/L2 Dual-Band GPS Receiver)

  • 김현덕;오태수;전재완;김성균;김병성
    • 한국전자파학회논문지
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    • 제21권10호
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    • pp.1169-1176
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    • 2010
  • 본 논문에서는 L1/L2 이중-밴드 GPS(Global Positioning System) 수신기용 RF 전단부를 설계하였다. 수신기는 Low IF 구조이며, 인덕터를 사용하지 않는 광대역 저잡음 증폭기(Low Noise Amplifier: LNA)와 이미지 제거를 위하여 다상 여과기(poly-phase filter)를 포함하는 quadrature 하향 변환 주파수 혼합기(quadrature down-conversion mixer) 및 전류 모드 논리(Current Mode Logic: CML) 주파수 분배기로 구성되어 있다. 저잡음 증폭기와 이미지 제거 주파수 혼합기는 높은 이득과 헤드룸 문제를 해결하기 위하여 전류 블리딩 기술을 이용하였으며, 광대역 입력 정합을 구현하기 위하여 공통 드레인 피드백을 이용하였다. $0.18{\mu}m$ CMOS 공정을 이용해 제작된 RF 전단부는 L1 밴드에서 38 dB 그리고 L2 밴드에서 41 dB의 이득을 보이며, IIP3는 L1 밴드에서 -29 dBm, L2 밴드에서는 -33 dBm이다. 입력 정합은 50 MHz에서 3 GHz까지 -10 dB 이하를 만족하며, 잡음 지수(Noise Figure: NF)는 L1 밴드에서는 3.81dB, L2 밴드에서는 3.71 dB를 보인다. 이미지 주파수 제거율은 36.5 dB이다. 설계된 RF 전단부의 칩 사이즈는 $1.2{\times}1.35mm^2$이다.

Formation and Intergrowth of the Superconducting Phase in the Bi2Sr2Can-1CunOx (n=2~4) System

  • Cheon, Min-Woo;Park, Yong-Pil
    • Transactions on Electrical and Electronic Materials
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    • 제5권5호
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    • pp.199-203
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    • 2004
  • Superconducting B $i_2$S $r_2$C $a_{n-l}$C $u_{n}$ $O_{x}$(n=2~4) thin films were prepared by single target DC-magnetron sputtering. And, that was compared with the B $i_2$S $r_2$C $a_{n-l}$C $u_{n}$ $O_{x}$(n=1~3) thin film fabricated by using the ion beam sputtering. Phase intergrowth among n=2-3, 3-4 and 4-5 phases was observed. The molar fraction of each phase in the mixed crystal of the deposited films was determined by x-ray diffraction analyses and investigated as a function of $O_2$ gas pressure during sputtering. We investigated the changes of the superconducting properties by molar fraction of each phase. Also, the thin film surface observation was carried out by atomic force microscope. The images show the average particle size decreases, and the distribution density of particles on the film surface was to increase with lower gas pressures. The fabrication conditions for selective growth of the single n=2, 3 and 4 phases in BiSrC $a_{n-l}$C $u_{n}$ $O_{x}$(n=2~4) thin film are discussed.e discussed.ussed.

Candida tropicalis DS-72에 의한 Xylose로부터 Xylitol의 생산

  • 오덕근;김상용
    • 한국미생물·생명공학회지
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    • 제25권3호
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    • pp.311-316
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    • 1997
  • A high xylitol producing yeast was isolated from the sludge of xylose manufacturing factory and then identified as Candida tropicalis DS-72 according to physiological properties. The strain was able to produce xylitol in a high concentration up to 72g/l from 100g/l xylose in 32 hours. Medium optimization for xylitol production by C. tropicalis DS-72 was performed. Effect of various nitrogen sources on xylitol production was investigated. Of nitrogenous compounds, yeast extract was the most suitable organic nitrogen nutrient for the enhancement of xylitol production. However, inorganic nitrogen resulted in a low cell concentration and did not produce xylitol. Effect of inorganic salts such as KH$_{2}$PO$_{4}$, and MgSO$_{4}$, 7H$_{2}$O on xylitol production was also studied. Optimal medium was selected as xylose 100g/l, yeast extract 10g/l, KH$_{2}$PO$_{4}$, 5 g/l and MgSO$_{4}$, 7H$_{2}$O 0.2 g/l. Xylitol of 88 g/l was produced from 100 g/l xylose in 30 hours using the optimal medium in a flask. In a fermentor, a fed-batch culture with 300g/l xylose was carried out. A final xylitol concentration of 240 g/l in the culture could be obtained in 43 hours of culture time by maintaining the high level of dissolved oxygen during growth phase and limiting the dissolved oxygen in the same culture during production phase. This result corresponded to a xylitol yield of 80% and a xylitol productivity of 5.58 g/1-h.

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Enhancement of eurycomanone biosynthesis in cell culture of longjack (Eurycoma longifolia) by elicitor treatment

  • Nhan, Nguyen Huu;Loc, Nguyen Hoang
    • Journal of Plant Biotechnology
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    • 제45권4호
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    • pp.340-346
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    • 2018
  • In this study, the effect of elicitors such as yeast extract (YE), methyl jasmonate (MeJA) and salicylic acid (SA) on the accumulation of eurycomanone in Eurycoma longifolia cell cultures were investigated. Suspension cells of E. longifolia was cultured in Murashige and Skoog (MS) medium supplemented with 30 g/L sucrose, 1.25 mg/L naphthaleneacetic acid (NAA) and 1 mg/L kinetin at a shaking speed of 120 rpm. Elicitors were added in the culture at different concentrations and times to stimulate eurycomanone accumulation in the Eurycoma longifolia cells. Eurycomanone content was determined by HPLC with a C18 column, flow rate of 0.8 mL/min, run time of 17.5 min, and a detector wavelength of 254 nm. The stationary phase was silica gel and the mobile phase was acetonitrile: $H_2O$. Non-elicited cells were used as the control. The study showed the effect of different elicitor concentrations, YE at 200 mg/L, MeJA at $20{\mu}M$ and SA at $20{\mu}M$ stimulated high production of eurycomanone. In which, treatment of $20{\mu}M$ MeJA after 4 days of culture resulted in the highest accumulation of this compound (17.36 mg/g dry weight), approximately 10-fold higher than that of untreated cells (1.70 mg/g dry weight).

$Ni/\gamma -Al_2O_3$ Catalyst Prepared by Liquid Phase Oxidation for Carbon Dioxide Reforming of Methane

  • 정경수;조병율;이호인
    • Bulletin of the Korean Chemical Society
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    • 제20권1호
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    • pp.89-94
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    • 1999
  • Carbon dioxide reforming of methane on Ni/γ-Al2O3 catalyst was studied. A new 10 wt% Ni/γ-Al2O3 catalyst prepared by the liquid phase oxidation method (L10O) exhibited much higher activity as well as resistances to both sintering and coke formation during the reaction than the catalyst prepared by the conventional impregnation method (D10). The electrically strong attractive interaction between nickel and support during the liquid phase oxidation process and the resultant high nickel dispersion made the L10 have superior activity and stability to the D10. To elucidate the results, the experiments with nickel catalysts on the other supports as well as 7-AI203 were performed. The effect of sodium as a promoter was also studied.