• Journal of the Microelectronics and Packaging Society
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• v.26 no.4
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• pp.95-100
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• 2019

Nanoindentation has been widely used for evaluating mechanical properties of nano-devices, from MEMS to packaging modules. Residual stress is also estimated from indentation tests, especially the Knoop indenter which is used for the determination of residual stress directionality. According to previous researches, the ratio of the two stress conversion factors of Knoop indentation is a constant at approximately 0.34. However, the ratio is supported by insufficient quantitative analyses, and only a few experimental results with indentation depth variation. Hence, a barrier for in-field application exists. In this research, the ratio of two conversion factors with variation in indentation depth using finite elements method has been attempted at. The magnitudes of each conversion factors were computed at uniaxial stress state from the modelled theoretical Knoop indenter and specimen. A model to estimate two stress conversion factor of the long and short axis of Knoop indenter at various indentation depths is proposed and analyzed.

• Corrosion Science and Technology
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• v.20 no.6
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• pp.484-490
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• 2021

Instrumented indentation testing has been widely used for residual stress measurement. The Knoop indentation is mainly selected for determining anisotropic mechanical properties and non-equibiaxial residual stress. However, the measurement of equibiaxial stress state and compressive residual stress on a specimen surface using Knoop indentation is neither fully comprehended nor unavailable. In this study, we investigated stress conversion factors for measuring Knoop indentation on equibiaxial stress state through indentation depth using finite element analysis. Knoop indentation was conducted for specimens to determine tensile and compressive equibiaxial residual stress. Both were found to be increased proportionally according to indentation depth. The stress field beneath the indenter during each indentation test was also analyzed. Compressive residual stress suppressed the in-plane expansion of stress field during indentation. In contrast, stress fields beneath the indenter developed diagonally downward for tensile residual stress. Furthermore, differences between trends of stress fields at long and short axes of Knoop indenter were observed due to difference in indenting angles and the projected area of plastic zone that was exposed to residual stress.

• Korean Journal of Materials Research
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• v.10 no.5
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• pp.335-342
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• 2000

The microhardness of rhenium sheets was determined as a function of indentation load and temperature. The temperature dependence of the microhardness between room temperatures and $1000 ^{\circ}C$was studied using a hot microhardness tester equipped with a Vickers indenter. The load dependence of the microhardness was investigated using oth a Vickers and a Knoop indenter. The indentation size effect (ISE) was well explained using the normalized Meyers law. The hardness of the annealed rhenium sheet approached that of the as-rolled sheets at large indentation loads because of work-hardening under the indenter during indentation. The hardness at zero load(obtained from extrapolation of the load dependence of the hardness) suggested that the hardness is controlled by two different mech-anisms having different thermal activation. At low temperature the activation energy for the mechanism controlling the hardness was approximately 0.02 eV , Whereas at higher temperatures that was approximately 0.15eV. The tranisi-tion temperature between the two different controlling mechanisms was about $250^{\circ}C$.

• The korean journal of orthodontics
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• v.29 no.5 s.76
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• pp.589-597
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• 1999

The purpose of this study was to evaluate the effects of fluoride releasing orthodontic sealants, light-cured (Group L1&L2) and self-cured (Group S1&S2) $FluoroBond^{\circledR}$, on enamel microhardness under artificial carious solution in vitro.112 extracted human premolar teeth were collected for experiments and divided into seven groups. A Tukon microhardness tester equipped with a Knoop diamond indenter was employed to determine microhardness. Tukon 23 program converted the number of microhardness into KHN (Knoop hardness number). The results were as follows: 1. The microhardness of enamel depth of all groups were the least at the depth of $50{\mu}m$ and that of all groups except L2 group, the greatest at the depth of $200{\mu}m$, were the greatest at the depth of $300{\mu}m$. And as the enamel depth of all groups except L2 and S2 group increased, the microhardness value also increased. 2. There was a little preventive effect in enamel decalcification both light-and self-cured orthodontic sealant groups, but had no statistical significance between the groups(p>0.05). 3. Light-cured orthodontic sealant groups had a progressive inhibiting effect in enamel decalcification at the depth of $100{\mu}m,150{\mu}m,\;and\;200{\mu}m$ (p<0.05). 4. Self-cured orthodontic sealant groups had a progressive inhibiting effect in enamel decalcification at the depth of $150{\mu}m$ (p<0.05). 5. There was no difference of the anti-enamel demineralization effect between light- and self-cured orthodontic sealant groups (p>0.05).