• 제목/요약/키워드: Isotopic Analysis

검색결과 161건 처리시간 0.03초

조선후기 사랑방 목가구의 표현과 의미 구조 분석 (Analysis of Expressive Features and Structural Meanings in Korean Men's Furniture of the 19th century)

  • 김은정;박영순
    • 한국실내디자인학회논문집
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    • 제21권6호
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    • pp.147-157
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    • 2012
  • This paper aims to examine the fundamental relationship of what principles cause the aesthetic shapes in Korean sarangbang furniture of the $19^{th}$ century. Focusing on the Greimas' isotopic and semantic structure analysis, this research analyzed the traditional Korean men's furniture in four steps; signifier analysis, isotopic analysis, semantic structure analysis, and comprehensive interpretation. The results show that the expressive qualities of sarangbang furniture included visual symmetric aesthetics, and the hues of natural materials with dark tones. The manufacturing process emphasized the characteristics of natural materials; while diversity was respected in decorations, function as restrained form was also important with a concise image. Through these characteristics, sarangbang furniture revealed a balance, a harmony of contrastive elements, and a restrained aesthetics. Within these qualities, it was seen that aesthetic principles, such as "severance and communication," "artifice and nature," "restraint and manifestation," "toughness and softness," "filling and emptying" and "decoration and utility" were in a mutually supplementary relationship. At the basis of this aesthetic thought appears to be Confucianism, which had been the model for seonbi politics and scholarship.

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DEVELOPMENT OF LEAD SLOWING DOWN SPECTROMETER FOR ISOTOPIC FISSILE ASSAY

  • Lee, YongDeok;Park, Chang Je;Ahn, Sang Joon;Kim, Ho-Dong
    • Nuclear Engineering and Technology
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    • 제46권6호
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    • pp.837-846
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    • 2014
  • A lead slowing down spectrometer (LSDS) is under development for analysis of isotopic fissile material contents in pyro-processed material, or spent fuel. Many current commercial fissile assay technologies have a limitation in accurate and direct assay of fissile content. However, LSDS is very sensitive in distinguishing fissile fission signals from each isotope. A neutron spectrum analysis was conducted in the spectrometer and the energy resolution was investigated from 0.1eV to 100keV. The spectrum was well shaped in the slowing down energy. The resolution was enough to obtain each fissile from 0.2eV to 1keV. The detector existence in the lead will disturb the source neutron spectrum. It causes a change in resolution and peak amplitude. The intense source neutron production was designed for ~E12 n's/sec to overcome spent fuel background. The detection sensitivity of U238 and Th232 fission chamber was investigated. The first and second layer detectors increase detection efficiency. Thorium also has a threshold property to detect the fast fission neutrons from fissile fission. However, the detection of Th232 is about 76% of that of U238. A linear detection model was set up over the slowing down neutron energy to obtain each fissile material content. The isotopic fissile assay using LSDS is applicable for the optimum design of spent fuel storage to maximize burnup credit and quality assurance of the recycled nuclear material for safety and economics. LSDS technology will contribute to the transparency and credibility of pyro-process using spent fuel, as internationally demanded.

Inter-laboratory Comparison of Stable Carbon and Nitrogen Isotopic Composition Data Using Elemental Analyzer-isotope Ratio Mass Spectrometers

  • Kim, Jung-Hyun;Kang, Sujin;Bong, Yeon-Sik;Park, Kwangkyu;Kang, Tae-Woo;Park, Yong-Se;Kim, Dahae;Choi, Seunghyun;Joo, Young Ji;Choi, Bohyung;Nam, Seung-Il;Lee, Sang-Mo;Shin, Kyung-Hoon
    • 환경분석과 독성보건
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    • 제21권4호
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    • pp.229-236
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    • 2018
  • In this study, inter-laboratory comparison was done using elemental analyzer-isotope ratio mass spectrometers (EA-IRMSs) to determine carbon and nitrogen contents as well as stable carbon and nitrogen isotopic compositions (${\delta}^{13}C$ and ${\delta}^{15}N$) of five environmental samples containing lake and marine sediments, higher plant leaves, and fish muscle, and one organic analytical standard (Protein (Casein) Standard OAS). Five national laboratories participated in this comparison study, and each laboratory analyzed all five samples and the analytical standard. Results showed that variations in total organic carbon (TOC) and total nitrogen (TN) contents as well as ${\delta}^{13}C_{TOC}$ and ${\delta}^{15}N_{TN}$ values among the laboratories were large compared to the analytical uncertainties. The results highlighted the inhomogeneity of the test samples and thus, the need to select suitable standard reference materials for future inter-laboratory studies. Further inter-laboratory comparison exercises could promote good measurement practices in the acquisition of stable carbon and nitrogen isotopic composition data.

부산 가덕도 장항 유적 출토 인골의 안정동위원소 분석을 통해 본 신석기시대의 식생활 양상 (Isotopic dietary history of Neolithic people from Janghang site at Gadeok Island, Busan)

  • 신지영;강다영;김상현;정의도
    • 분석과학
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    • 제26권6호
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    • pp.387-394
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    • 2013
  • 인골에서 추출된 콜라겐의 탄소와 질소 안정동위원소 정보는 당시 사람들의 식생활과 영양 상태, 생계 경제를 복원하는데 구체적인 가능성을 제시한다. 지금까지 우리나라의 신석기시대 유적에서는 인골이 많이 발견되지 않아 직접적인 식생활 양상 추적이 어려웠는데, 부산 가덕도 장항유적에서 출토된 인골 48개체의 확인은 매우 주목할 만한 성과이다. 본 연구에서는 인골에서 추출된 콜라겐의 탄소와 질소 안정동위원소 분석을 수행하였으며, 평균값은 각각 다음과 같다(${\delta}^{13}$C=$-14.5{\pm}1.3$‰, ${\delta}^{15}$N=$-17.4{\pm}1.7$‰, n=10). 뼈의 조직 분석 결과 보존 상태는 매우 안좋은 HI (조직학 지수) 0을 나타냈으나, 뼈 콜라겐의 경우 질 평가지수에 합격한 값만을 사용하여 생존 시 식생활을 반영한다는 것을 알 수 있었다. 당시의 고고학적인 정황을 고려할 때 장항 유적 피장자들은 해양성 식료를 주로 섭취하였고, 육상 동물 및 야생 식물의 섭취 가능성 역시 배제할 수 없는데, 본 연구에서는 식료 섭취의 직접적인 증거가 되는 인골의 안정동위원소 분석을 통해 이러한 가정을 입증하였다. 이 외에도 펴묻기와 굽혀묻기 등 장법이나 토기 등 부장품에 따른 안정동위원소값에서는 유의미한 차이를 확인할 수 없었다. 신석기시대 최대 집단 묘역인 부산 가덕도 장항 유적 출토 인골 콜라겐의 탄소와 질소 안정동위원소 분석은 우리나라 신석기 시대 생활상을 복원하는 데 매우 핵심적인 증거가 될 것이라 기대된다.

Determination of the Concentration and Isotope Ratio of Uranium in Soil and Water by Thermal Ionization Mass Spectrometry

  • Park, Jong-Ho;Park, Sujin;Song, Kyuseok
    • Mass Spectrometry Letters
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    • 제5권1호
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    • pp.12-15
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    • 2014
  • Thermal ionization mass spectrometry (TIMS) was used to determine the concentration and isotope ratio of uranium contained in samples of soil and groundwater collected from Korea. Quantification of uranium in ground water samples was performed by isotope dilution mass spectrometry. A series of chemical treatment processes, including chemical separation using extraction chromatography, was applied to the soil samples to extract the uranium. No treatments other than filtration were applied to the groundwater samples. Isotopic analyses by TIMS showed that the isotope ratios of uranium in both the soil and water samples were indistinguishable from those of naturally abundant uranium. The concentration of uranium in the groundwater samples was within the U.S. acceptable standards for drinking water. These results demonstrate the utility of TIMS for monitoring uranium in environmental samples with high analytical reliability.

Integral nuclear data validation using experimental spent nuclear fuel compositions

  • Gauld, Ian C.;Williams, Mark L.;Michel-Sendis, Franco;Martinez, Jesus S.
    • Nuclear Engineering and Technology
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    • 제49권6호
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    • pp.1226-1233
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    • 2017
  • Measurements of the isotopic contents of spent nuclear fuel provide experimental data that are a prerequisite for validating computer codes and nuclear data for many spent fuel applications. Under the auspices of the Organisation for Economic Co-operation and Development (OECD) Nuclear Energy Agency (NEA) and guidance of the Expert Group on Assay Data of Spent Nuclear Fuel of the NEA Working Party on Nuclear Criticality Safety, a new database of expanded spent fuel isotopic compositions has been compiled. The database, Spent Fuel Compositions (SFCOMPO) 2.0, includes measured data for more than 750 fuel samples acquired from 44 different reactors and representing eight different reactor technologies. Measurements for more than 90 isotopes are included. This new database provides data essential for establishing the reliability of code systems for inventory predictions, but it also has broader potential application to nuclear data evaluation. The database, together with adjoint based sensitivity and uncertainty tools for transmutation systems developed to quantify the importance of nuclear data on nuclide concentrations, are described.

Geographic authentication of rice (Oryza sativa L.) collected from Asian countries using multi-elements, stable isotope ratio, and chemometric analyses

  • Lee, Kyoung-Jin;Park, Sung-Kyu;Lee, Ji-Hee;Son, Na-Young;Chung, Ill-Min;Kim, Seung-Hyun
    • 한국작물학회:학술대회논문집
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    • 한국작물학회 2017년도 9th Asian Crop Science Association conference
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    • pp.263-263
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    • 2017
  • Rice (Oryza sativa L.) is the world's third largest food crop after wheat and corn. Geographic authentication of rice has recently emerged as an important issue for enhancing human health via food safety and quality assurance. Here, we aimed to discriminate rice from six Asian countries through geographic authentication using combinations of elemental/isotopic composition analysis and chemometric techniques. Principal components analysis could distinguish samples cultivated from most countries, except for those cultivated in the Philippines and Japan. Furthermore, orthogonal projection to latent structure-discriminant analysis provided clear discrimination between rice cultivated in Korea and other countries. The major common variables responsible for differentiation in these models were ${\delta}^{34}S$, Mn, and Mg. Our findings contribute to understanding the variations in elemental and isotopic compositions in rice depending on geographic origins, and offer valuable insight into the control of fraudulent labeling regarding the geographic origins of rice traded among Asian countries.

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PRELIMINARY STUDY ON THE ALPHA TRACK ANALYSIS OF SPHERICAL URANIUM METAL PARTICLES

  • Pyo Hyung-Yeol;Kim Jong-Yun;Lee Myung-Ho;Park Yong-Jun;Jee Kwang-Yong;Kim Won-Ho
    • Nuclear Engineering and Technology
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    • 제38권4호
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    • pp.353-358
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    • 2006
  • Alpha track analysis for the determination of the trace amount of alpha emitting nuclides in a very small particle was performed as an efficient and powerful technique during safeguard inspection. Metal particles with well-defined spherical shape, size and isotopic compositions as a reference material were used to correlate the number of tracks or track diameter with an isotopic composition eventually to identify the uranium enrichment in the environmental swipe samples. Slopes in the number of tracks versus the exposure time curve provide a simple insight into the uranium enrichment of an unknown particle. Low enriched uranium metal particles result in slopes still steeper than the depleted or natural uranium metal particles. In addition, a linear relationship between track diameter and particle size Is thought to be a useful first stage analytical tool as an efficient and convenient inspection guide. The significance of the simple linear model was also judged using the usual statistical tests.

Feasibility study of a novel hash algorithm-based neutron activation analysis system for arms control treaty verification

  • Xiao-Suo He;Yao-Dong Dai;Xiao-Tao He;Qing-Hua He
    • Nuclear Engineering and Technology
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    • 제56권4호
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    • pp.1330-1338
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    • 2024
  • Information on isotopic composition and geometric structure is necessary for identifying a true warhead. Nevertheless, such classified information should be protected physically or electronically. With a novel Hash encryption algorithm, this paper presents a Monte Carlo-based design of a neutron activation analysis verification module. The verification module employs a thermal neutron source, a non-uniform mask (physically encrypting information about isotopic composition and geometric structure), a gamma detector array, and a Hash encryption algorithm (for electronic encryption). In the physical field, a non-uniform mask is designed to distort the characteristic gamma rays emitted by the inspected item. Furthermore, as part of the Hash algorithm, a key is introduced to encrypt the data and improve the system resolution through electronic design. In order to quantify the difference between items, Hamming distance is used, which allows data encryption and analysis simultaneously. Simulated inspections of simple objects are used to quantify system performance. It is demonstrated that the method retains superior resolution even with 1% noise level. And the performances of anti-statistical attack and anti-brute force cracking are evaluated and found to be very excellent. The verification method lays a solid foundation for nuclear disarmament verification in the upcoming era.