• 제목/요약/키워드: Investigation on the Spot

검색결과 188건 처리시간 0.028초

TLC 상 유도체화 반응을 이용한 아민 계 화합물의 Screening 방법 (Screening method for amines by derivatization reaction on TLC)

  • 최성운;이혜인;성낙도
    • 분석과학
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    • 제26권4호
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    • pp.228-234
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    • 2013
  • 국내에서 불법 유통 되거나 남용되고 있는 methamphetamine은 아민을 함유한 불법약물로서 그에 대한 신속하고 용이한 동정 및 정량적인 분석 방법은 불법약물 검사의 중요한 이슈가 되어왔다. 새로운 screening방법을 모색하기 위해 methamphetamine과 구조적으로 유사한 3종의 유기 화합물을 silica gel ($SiO_2$) TLC상에서 N-(9-Fluorenylmethoxycarbonyloxy)succinimide (FMOC-NHS)와 반응을 시켰다. TLC상 반응 생성물을 일반 유기합성 경로로 합성한 대조물질과 비교 확인한 다음, 이 방법의 검출한계(Limit of detection)를 조사하였다. 실험결과 유도체화 시약으로 사용한 FMOC-NHS는 TLC상에서 1차 및 2차 아민과 반응하여 UV-active한 화합물을 생성시키는 것을 확인하였다. 2D TLC 실험에서는 0.045-0.01 mg/mL ($2{\mu}L$ per spot), 그리고 1D co-spot TLC 실험에서 0.002-0.007 mg/mL ($2{\mu}L$ per spot)의 검출한계는 유도체화 시약의 농도에 대한 의존성을 나타내었다.

Geotechnical field investigation on giresun hazelnut licenced warehause and spot exchange

  • Angin, Zekai
    • Geomechanics and Engineering
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    • 제10권4호
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    • pp.547-563
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    • 2016
  • This paper describes a geotechnical field investigation in Giresun hazelnut licenced warehause and spot exchange during twelve months to determine the soil profile and static project applicability. It is also aimed to determine the superstructure loads and evaluate the relevance of foundation filling materials of the main, laboratory, package and admin buildings. The main building has $88.50{\times}63.20(5593.2)m^2$ site area. It has a big raft foundation. Eleven geotechnical reports were prepared between 2 December 2014 and 25 May 2015. Maximum settlements and safe bearing capacities were calculated to decide to be able to proceed to the next step. Also, the detail observations and evaluations were presented from October 2014 to December 2014. It has been seen that the foundation is designed as a single foundation one. But, in the light of observations, it has been evaluated that the foundation project for package building is not adequate, and after these excavations it must be revised as a raft foundation. The thickness of foundation and structural details should be defined/drawn after analyzing the details by using a special software. Construction joints should be designed between different buildings interfaces to avoid damages and cracks with in different settlements. The environmental drainage must be projected and applied to avoid the probable damage of surface waters on foundations.

진해만해역의 수질환경특성에 관한 연구 (A Study on the Characteristics of Water Quality in the Jinhae Bay)

  • 반영남;국승기
    • 한국항해항만학회:학술대회논문집
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    • 한국항해항만학회 2004년도 춘계학술대회 논문집
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    • pp.255-261
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    • 2004
  • 본 논문에서는 진해만에서 수질환경에 대한 현장관측조사를 통하여 진해만 수질현황에 대한 해수유동 시뮬레이션을 실시하여 대상해역의 유통특성을 파악하고, 계산된 유통data를 이용하여 해양오염시뮬레이션을 행하였으며 해수유동시뮬레이션 결과를 해양조사원에서 실시한 조석 및 조류관측 자료를 이용하여 시뮬레이션 결과를 검증하였으며, 유통결과를 해양오염 시뮬레이션의 유통 입력 자료로 이용하였다. 해수유통 Data 및 해양관측 Data를 이용하여 수질확산시뮬레이션을 행하여 실측데이터와 비교분석하여 COD농도 분포를 계산하여서 진해만의 수질특성을 파악하고자 하였다.

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The Operational Comparison of SPOT GCP Acquisition and Accuracy Evaluation

  • Kim, Kam-Lae;Kim, Uk-Nam;Chun, Ho-Woun;Lee, Ho-Nam
    • Korean Journal of Geomatics
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    • 제1권1호
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    • pp.1-5
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    • 2001
  • This paper presents an investigation into the operational comparison of SPOT triangulation to build GCP library by analytical plotter and DPW (digital photogrammetric workstation). GCP database derived from current SPOT images can be used to other image sensors of satellite, if any reasons, such as lack of topographic maps or GCPs. But, general formulation of a photogrammetric process for GCP measurement has to take care of the scene interpretation problem. There are two classical methods depending on whether an analytical plotter or DPW is being used. Regardless of the method used, the measurement of GCPs is the weakest point in the automation of photogrammetric orientation procedures. To make an operational comparison, five models of SPOT panchromatic images (level 1A) and negative films (level 1AP) were used. Ten images and film products were used for the five GRS areas. Photogrammetric measurements were carried out in a manual mode on P2 analytical plotter and LH Systems DPW770. We presented an approach for exterior orientation of SPOT images, which was based on the use of approximately eighty national geodetic control points as GCPs which located on the summit of the mountain. Using sixteen well-spaced geodetic control points per model, all segments consistently showed RMS error just below the pixel at the check points in analytical instrument. In the case of DPW, half of the ground controls could not found or distinguished exactly when we displayed the image on the computer monitor. Experiment results showed that the RMS errors with DPW test was fluctuated case by case. And the magnitudes of the errors were reached more than three pixels due to the lack of image interpretation capability. It showed that the geodetic control points is not suitable as the ground control points in DPW for modeling the SPOT image.

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골프클럽 안정타점영역의 크기와 중심에 관한 연구 (Investigation on the Size and Center of Sweet Spot of Golf Club)

  • 이정윤;마정범;오재응
    • 대한기계학회논문집
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    • 제16권5호
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    • pp.992-998
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    • 1992
  • 본 연구에서는 그립부의 비틀림 모멘트를 최소화하는 안정타점영역을 정의하 였으며 전달매트릭스법에 의한 수치해석과 실험적 모드해석법을 실제의 골프클럽에 적 용하여 모드 파라메타를 구한 다음 그 파라메타변경에 따른 안정타점영역 변화를 예측 함으로써 안정타점영역을 확장시키는 방법에 대해 연구하였다.

Fatigue Strength Assessment of Spot-Welded Lap Joint Using Strain Energy Density Factor

  • Sohn, Ilseon;Bae, Dongho
    • Journal of Mechanical Science and Technology
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    • 제15권1호
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    • pp.44-51
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    • 2001
  • One of the recent issues in design of the spot-welded structure such as the automobile body is to develop an economical prediction method of the fatigue design criterion without additional fatigue test. In this paper, as one of basic investigation for developing such methods, fracture mechanical approach was investigated. First, the Model I, Mode II and Mode III, stress intensity factors were analyzed. Second, strain energy density factor (S) synthetically including them was calculated. And finally, in order to decide the systematic fatigue design criterion by using this strain energy density factor, fatigue data of the ΔP-N(sub)f obtained on the various in-plane bending type spot-welded lap joints were systematically re-arranged in the ΔS-N(sub)f relation. And its utility and reliability were verified by the theory of Weibull probability distribution function. The reliability of the proposed fatigue life prediction value at 10(sup)7 cycles by the strain energy density factor was estimated by 85%. Therefore, it is possible to decide the fatigue design criterion of spot-welded lap joint instead of the ΔP-N(sub)f relation.

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감나무 둥근무늬낙엽병의 발생과 병원균(Mycosphaerella nawae)의 전염원 동태 (Ecology of Disease Outbreak of Circular Leaf Spot of Persimmon and Inoculum Dynamics of Mycosphaerella nawae)

  • 권진혁;박창석
    • 식물병연구
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    • 제10권4호
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    • pp.209-216
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    • 2004
  • The circular leaf spot of persimmon is occurred almost every place where persimmon is cultivated, especially the disease outbreak severely in southern part of Korea. The disease reveals unusually long incubation period after pathogen invade into leaf tissue and no practical control measure is available once the symptom has appeared. Most of the farmers just follow the suggested spray schedules calculated on the basis of weather condition of ordinary years. Therefore the damages due to circular leaf spot greatly differ year after year. In this article, we tried to describe and summarized the investigation on the circular leaf spot pathogen, Mycosphaerella nawae, related to disease outbreak such as overwintering of pathogen, inoculum formation and spread, incubation period after infection, and secondary inoculum. With the summary of these results, we suggest the disease cycle of circular leaf spot of persimmon. The pathogen overwinters in diseased leaves as mycelial form or pseudoperithecial premodium. The pseudoperitheria become matured in spring as the temperature raise and forms asci and ascospores. The maturation of pseudoperithecia are closely related to the temperatures during March and early April. The ascospores completely mature in early May and the ascospores released when the pseudoperithecia absorbed enough moisture after rainfall. The release of ascospores are diverse greatly with the variation of maturity of pseudoperithecia. Generally the spore start to release from middle of May to early of July. Duration of ascospore release is depend on the weather condition of particular year, especially amount and number of precipitation. The ascospores produced from pseudoperithecia is known to the only inoculum for circular leaf spot disease. But according to the results obtained from our investigations, the conidia formed on the lesions which incited by natural infection. This conidia are infectious to persimmon leaves and formed identical symptom as natural infection. The time of producing secondary inoculum of circular leaf spot of persimmon is considered too late to develop new disease. Generally the importance of secondary inoculum is low but the conidia produced in early September are competent to develop new disease and new infection also significantly affect to harvest of persimmon. The importance of circular leaf spot disease is recognized well to farmers. The approaches to control of the disease should be initiated on the basis of the knowledges of inoculum dynamics and ecology of disease development. The forecasting system for circular leaf spot is need to be developed.

점용접된 판 구조물의 면적비와 거리비에 따른 진동특성 연구 (A Study on Vibration Characteristics of Plate Structures Spot-Welded with respect to Area Ratio and Distance Ratio)

  • 한동섭;안성찬;안찬우;한근조
    • 한국항해항만학회지
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    • 제26권1호
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    • pp.43-49
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    • 2002
  • 본 연구에서는 비감쇠 자유진동을 하는 점용접된 사각평판의 고유진동수를 수치해석을 통하여 살펴보고, 실험을 통하여 결과를 검증하였다 설계변수로는 점용접에 미치는 여러 설계변수 중에서 점용접이 차지하는 면적을 사각평판의 면적으로 나눈 면적비와 점용접점 사이의 거리를 평판의 한 변의 길이로 나눈 거리비로 무차원화하여 사용하였으며, 목적함수로는 점용접으로 인한 두께효과를 진동수에 대한 처짐의 비로써 나타낸 등가두께로써 무차원화하여 정의하였다. 수치해석에는 범용유한요소해석 프로그램인 ANSYS 5.6을 사용하였고, 실험에는 B&K Data analyzer를 통하여 주파수분석을 수행하였다. 연구의 결과 다음과 같은 결론을 얻었다. 1. 점용접의 면적비가 단지 4.52%인데 비해 점 용접으로 인한 두께효과는 55%로써 매우 크게 나타났다. 2. 거리비에 따른 두께효과는 거리비가 0.4일 때 가장 크게 나타났다.

안드로이드 기반의 위치정보를 이용한 수강생 인증 시스템 (Authentication System of Students using the Position Information of Android-based)

  • 박성현;편도길;육정수;정회경
    • 한국정보통신학회:학술대회논문집
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    • 한국정보통신학회 2013년도 춘계학술대회
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    • pp.632-634
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    • 2013
  • 현재 스마트시대에서 대학이나 교육기관의 수업 중 현장답사와 견학시스템 및 강의 일지 작성을 필요로 하는 과목이 증가하고 있다. 이러한 시점에서 교수들이 일일이 확인하고 일지를 작성, 데이터화 하는 과정의 편리성을 확보 하려고 한다. 이에, 본 논문에서는 안드로이드 위치정보 및 다양한 모듈로 현장답사 및 견학시스템의 자료화 및 인증화 하는 시스템을 도입하여, 보다 편리한 학습 환경 및 일지작성을 단순화 하는 작업시스템을 설계 및 구현하였다.

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소손된 배선용 차단기 동작상태에 의한 전기화재 규명의 신뢰성에 관한 연구 (A Study on Authoritativeness of Electric Fire by Activating of Fire Damaged MCCB)

  • 이종화;문용수;공하성
    • 대한안전경영과학회지
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    • 제11권2호
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    • pp.87-94
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    • 2009
  • In the fire there are fusion signs and damage by fire, and insulation aging and carbonization of the electric wiring in the ignition spot because of special characteristic of the appliance in the electricity fire. Because of the physical factor applied in the damage of fire, the decision of ignition spot by eye investigation is insufficient. In this paper, the cause of electricity fire is researched. The focus is on the operation state of operated MCCB(Molded Case Circuit Breaker) at the time of electricity fire. Through grasping the operation principle of MCCB and the experiment, the state of MCCB after fire suppression is discriminated. The distinction possibility on the exist of electricity fire is proposed.