• Restorative Dentistry and Endodontics
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• v.19 no.1
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• pp.64-72
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• 1994

Zinc Phosphate Cement hand been used for about more than 100 years in luting of cast gold inlay. But many scientists had been trying to develop the new form of luting agent because the ZPC hand shown the lack of adhesiveness on the tooth structure and the toxicity to the pulp tissue. Recently many researches about the surface treatment of the cast body are being done to increase the adhesion of cement to it. The conventional Class I gold inlays were fabricated in the 20 permanent molars. After the internal surface of the cast body was sandblasted with $Al_2O_3$ particles and was tin-plated, the inlays were cemented with adhesive cement [G I cement and resin cement(Super-Bond & $Panavia_{EX}$)] and the evaluation on the adhesion pattern, adhesive strength and the fracture pattern of the adhesive cast gold inlay was compared to that of the cast gold inlay cemented conventionally with ZPC. The results were as follows : 1. The surface roughness of the cast body was increased significantly after sandblasting with the $Al_2O_3$ particles and the tin oxide layer, which was consisted of round particles, came into being. 2. The bond strength was in the order of Super-Bond, ZPC, Fuji I, $Panavia_{EX}$ group. The group cemented with Super-Bond showed statistically greater strength than the other groups(p<0.05). 3. The group cemented with ZPC was fallen apart by principal adhesion failure and that with Fuji I was by complete adhesion failure. But the group with Super-Bond showed pricncipal cohesive failure pattern and in the group with $Panavia_{EX}$, complete cohesive fracture pattern was shown and small protion of tooth structure was fractured out with cast body and the fractured surface showed the figure just as the enamel prism. 4. Various gaps were shown at the pulpal side regardless of little gap at the side walls of the cavity in all groups. Only the Super-Bond was attached to the tooth structure and the other cements were detached from both the tooth and the cast body.

• Restorative Dentistry and Endodontics
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• v.24 no.3
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• pp.465-472
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• 1999

The aim of this study was to determine the shear bond properties of four dentin bonding systems to internal cervical dentin, and to investigate the effect of the pretreatment for removing smear layer and position of dentin on shear bond strength of dentin bonding agents. The materials tested in this study were consisted of four commercially available dentin bonding systems[Allbond 2(AB), Clearfil Linerbond 2(CL), Optibond FL(OP), Scotchbond Multi-purpose(SB)], a restorative light-cured composite resin[Z100]J and a chelating agent[RC-prep(RC)]. Fifty-six freshly extracted human molars were used in this study. Dentin specimens were prepared by first cutting the root of the tooth 1mm below the cementoenamel junction with a diamond bur in a high speed handpiece under air-water coolant, and then removing occlusal part at pulp horn level by means of a second parallel section, The root canal areas were exposed by means of cutting the dent in specimens perpendicular to the root axis. Dentin specimens were randomly assigned to two groups(pretreated group, not-pretreated group) based on the pretreatment method of dentin surface. In pretreated group, RC was applied to dentin surface for 1minute and then rinsed with NaOCl. In not-pretreated group, dentin surface was rinsed with saline Each groups were subdevided into four groups according to dentin bonding systems. Four dentin bonding systems and a restorative resin were applied according to the directions of manufacturer. The dentin-resin specimens were embedded in a cold cure acrylic resin, and were cut with a low speed diamond saw to the dimension of $1{\times}1mm$. The cut specimens were divided into three groups according to the position of internal cervical dentin. The shear bond properties of dentin-resin specimens were measured with Universal testing machine (Zwick, 020, Germany) with the cross head speed of 0.5mm/min. From this experiment. the following results were obtained : 1. In case of shear bond strength, there was no significant difference among dentin bonding systems in not-pretreated groups, whereas in pretreated groups, the shear bond strengths of AB and of SB were statistically significantly higher than those of CL and of OP. 2. The shear bond strengths of AB and of SB in pretreated groups were significantly higher than those in not-pretreated groups. 3. The shear bond strengths of radicular layer of OP were higher than those of occlusal layer of OP in not-pretreated groups, and of AB in pretreated groups. The shear bond strengths of radicular layer of AB and of CL in not-pretreated groups were higher than those in pretreated group.

• Structural Engineering and Mechanics
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• v.65 no.5
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• pp.601-609
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• 2018

Steel bolts are used in the construction industry for a large variety of applications that range from fixing permanent installations to temporary fixtures. In the past much research has been focused on developing destructive testing techniques to estimate their pull-out load carrying capacity with very little attention to develop non-destructive techniques. In this regards the presented research work details the combined use of ultrasonic pulse velocity and Schmidt hammer tests to identify anchor bolts with faculty installation and to estimate their pull-out strength by relating it to the Schmidt hammer rebound value. From experimentation, it was observed that the load capacity of bolt depends on its embedment length, diameter, bond quality/concrete strength and alignment. Ultrasonic pulse velocity test is used to judge the quality of bond of embedded anchor bolt by relating the increase in ultrasonic pulse transit time to the presence of internal pours and cracks in the vicinity of steel bolt and the surrounding concrete. This information combined with the Schmidt hammer rebound number, R, can be used to accurately identify defective bolts which resulted in lower pull-out strength. 12 mm diameter bolts with embedment length of 70 mm and 50 mm were investigated using constant strength concrete. Pull-out load capacity versus the Schmidt hammer rebound number for each embedment length is presented.

• Journal of the Korean Wood Science and Technology
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• v.24 no.1
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• pp.17-26
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• 1996

This research was accomplished to evaluate possibility of using paper sludge for the raw materials of wood based panel products. The experimental panels were manufactured by four mixed ratios, the proportion of paper sludge to wood particle: 20:80, 30:70, 40:60, 50:50% (oven dry weight basis) and by three composition types, sludge-particle mixed board, three layered sludge-particle board and three layered particle board. They were tested mechanical (bending strength and internal bond) and physical properties (water absorption, thickness swelling and linear expansion). From the results they were shown that bending strength of mixed and three layered sludge-particle board were decreased with increasing of composition ratios of sludge. And the mechanical and physical properties of the boards of three layered composition types have superior to those of mixed composition type. Although composition ratios of sludge increased, the internal bond strength and dimensional stability of sludge-particle board not decreased quantitatively. We concluded that the mechanical and physical properties of three layered sludge-particle board were similar w those of three layered particle-board (control) made by our laboratory design. Therefore, it was recognized that paper sludge can be used as potential raw material in particle-board manufacturing industry.

• Journal of the Korean Wood Science and Technology
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• v.23 no.2
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• pp.70-76
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• 1995

Research was conducted at the Wood Materials and Engineering Laboratory, Washington State University, Pullman, WA to evaluate the effects of the sequence of wax addition, wax level, and wax type on mechanical properties and water resistance performance of isocyanate-bonded particleboard. Mechanical properties and water resistance performance were not influenced significantly by the sequence of wax addition. Internal bond and wet modulus of rupture in bending strength were decreased significantly by increasing the wax emulsion level, but dry modulus of rupture and modulus of elasticity in bending strength were not decreased significantly by increasing the wax emulsion level. Dry internal bond, dry and wet moduli of rupture, and modulus of elasticity were not decreased by increasing the solid wax level except for wet internal bond. The addition of 1.0 and 1.5% wax level did not produce any significant additional water resistance effect when compared to the addition of 0.5% wax level. Internal bond values of boards with solid wax addition showed significantly better results than boards with just a wax emulsion added. Modulus of rupture, modulus of elasticity, and water resistance performance did not show significant difference between solid wax and wax emulsion.

• Restorative Dentistry and Endodontics
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• v.26 no.1
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• pp.41-50
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• 2001

The purpose of this study was to examine the influences of camphoroquinone on the properties of five experimental composites. The contents of camphoroquinone were varied as 0.2%, 0.3%, 0.4%, 0.5%, and 0.6%, with silanized filler 75% and tertiary amine 0.2%. Five kinds of experimental composites were prepared, and diametral tensile strength, shear bond strength, depth of cure and yellowish discoloration were tested as a measurement. Specimen numbers of 10 were applied to all test items and experimental groups. Specimens for testing the diametral tensile strengths with internal diameter of 6mm in diameter and 3mm in height were filled with 5 experimental composites which were crushed with 1mm/min cross-head speed on Instron universal testing machine (Model No. 4467). Shear bond strength was measured on specimens attached to bovine teeth enamel etched with 37% phosphoric acid. Depth of cure was measured by the measurement of height of specimens which were removed the un-polymerized portion with acetone. Yellowness measurements were made by chromometer(Minolta Co. Japan) using L$^*$a$^*$b$^*$ values. ANOVA and Multiple range tests were used analyzed data with confidence level at 95%. The mean value of the shear bond strengths ranged from 31.03MPa to 39.49MPa. Following results were obtained ; 1. Diametral tensile strength was highest in experimental group 3, then was not affected by the contents of camphoroquinone ($r^2$=0.0422). 2. Composite resins containing 0.4% camphoroquinone showed the highest shear bond strength, but there was no statistical significance (p=0.3718). 3. Camphoroquinone reduces the depth of cure in the composite resins (p=0.0004, $r^2$=0.9483). 4. Camphoroquinone made the composites yellowish ($r^2$=0.9815). These results mean that increased content of camphoroquinone reduces the depth of cure, and that camphoroquinone make composites yellowish.

• Computers and Concrete
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• v.1 no.4
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• pp.401-416
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• 2004

This paper presents investigation of a three-dimensional (3-D) nonlinear finite element model analysis to examine the behavior of reinforced concrete beams strengthened with Carbon Fiber Reinforced Polymer (CFRP) composites to enhance the flexural capacity and ductility of the beams. Three-dimensional nonlinear finite element models were developed between the internal reinforcement and concrete using a smeared relationship. In addition, bond models between the concrete surface and CFRP composite were developed using a smeared bond for general analyses and a contact bond for sensitivity analyses. The results of the FEA were compared with the experimental data on full-scale members. The results of two finite-element bonding models showed good agreement with those of the experimental tests.

• Journal of Korea Technical Association of The Pulp and Paper Industry
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• v.39 no.4
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• pp.14-20
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• 2007

The effects of blending starches with different gelatinization temperatures on the development of ply-bond strength were systematically investigated using a three component mixture design technique. Oxidized corn starches with different gelatinization temperatures were blended with natural corn starch and sprayed for plybonding. Optimum blend ratio for maximizing plybond strength improvement for the starch blends was 40% of natural starch, 27% of oxidized starch with low gelatinization temperature and 33% of oxidized starch with high gelatinization temperature. Starch granules with the lowest gelatinization temperature gelatinizes at the lowest temperature, while the natural corn starch gelatinizes at later stage of drying. The improvement of plybond strength with starch blends were verified on machine trial as well. Plybond strength improvement obtained from the machine trial was lower than that achievable with handsheets, which was attributed to the lower internal bond strength of the linerboards made from recycled fibers.

• Journal of the Korean Wood Science and Technology
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• v.35 no.2
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• pp.51-60
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• 2007

In this study, the possibility of using pyrolysis oil as wood adhesives was explored. Especially, adhesives were formulated by reacting pyrolysis oil and formaldehyde and also partially replacing phenol with pyrolysis oil in phenol-formaldehyde (PF) adhesive and soy hydrolizate/PF adhesive formulation. The pine wood was fast pyrolyized and the oils were obtained from a series of condensers in the pyrolysis system. The oils from each condenser were first reacted with formaldehyde to explore potential use of the oil itself as adhesive. The lap-shear bond strength test results indicated that the oil itself could be polymerized and form bonds between wood adherends. The oils from each condenser were then mixed together and used as partial replacement of phenol (25, 33, and 50% by weight) in phenol-formaldehyde adhesive. The bond strength of the oil containing PF adhesives was decreased as percent phenol replacement level increased. However, no significant difference was found between 25 and 33% of phenol replacement level. The oil-contained PF resins at 25, 33, and 50% phenol replacement level with different NaOH/Phenol (Pyrolysis oil) molar ratio were further formulated with soy hydrolizate to make soy hydrolizate/pyrolysis oil-phenol formaldehyde adhesive at 6:4 weight (wt) ratio and used for fiberboard manufacturing. Surface internal bond strength (IB) of the boards bonded with 33% replacement at 0.3 NaOH/Phenol (Pyrolysis oil) molar ratio performed better than other replacement levels and molar ratios. Thickness swelling after 24 hr cold water soaking and after 2 hr in boiling water was increased as % replacement of pyrolysis oil increased.

• International Journal of Reliability and Applications
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• v.8 no.1
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• pp.111-124
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• 2007

In this paper, we apply insightful statistical reliability tools to manage and seek improvements in the strengths of Oriented Strand Board (OSB). As a part of the OSB manufacturing process, the product undergoes destructive testing at various intervals to determine compliance with customers' specifications. Workers perform these tests on sampled cross sections of the OSB panel to measure the tensile strength, also called internal bond (IB), in pounds per square inches until failure. Additional stiffness strength tests include parallel and perpendicular elasticity indices (EI), which are taken from cross sectional samples of the OSB panel in the parallel and perpendicular directions with respect to the orientation of the wood strands. We explore both graphically and statistically these "pressure-to-failures" of OSB. Also, we briefly comment on reducing sources of variability in the IB and EI of OSB.