• 제목/요약/키워드: Interlaboratory comparison

검색결과 17건 처리시간 0.021초

Bi-2223선재의 임계전류 측정기술 비교 (Interlaboratory Comparison of Critical Current Measurements on Ag-sheathed Bi-2223 tapes)

  • Lee, Kyu-Won;Han, Gi-Youl
    • Progress in Superconductivity
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    • 제3권1호
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    • pp.99-103
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    • 2001
  • We have conducted two runs of interlaboratory comparison on Ag-sheathed Bi-2223 tapes to evaluate the level of measurement techniques for the critical current measurement. Two classes of specimens were prepared for parallel and serial routings and sent to four participating laboratories. The critical currents of specimens were measured at 77 K in zero magnetic field. In the first comparison, we used twenty different Bi-2223 tapes as specimens for comparison and participating laboratories measured the specimens using their own instruments and procedures. As a result, the scattering of data on the first comparison showed -3.0% to +l2.2% for the parallel routing and -0.7% to +l5.1% for the serial routing. Major sources of these variations were attributed to different measurement techniques. Thus, the second comparison of measurement was done on the same specimens under specified measurement conditions, particularly in terms of cooling procedure and sweep rate of the test current. The variations for the second comparison were decreased -3.1% to +3.2% far the parallel routing and -1.8% to +7.7% fur the serial routing.

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중금속분석용 폐수표준물질 제조 및 실험실간 비교평가 (Preparation of wastewater-based reference materials for heavy metal analysis and interlaboratory study)

  • 김영희;송기봉;신선경;이정섭;정기택;홍은진;박진주;유석민
    • 분석과학
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    • 제23권3호
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    • pp.295-303
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    • 2010
  • 폐수 시료를 이용한 중금속분석용 수질표준물질을 제조하여, 납, 카드뮴, 크롬, 구리, 아연, 망간, 철 등 중금속 7 종에 대해 인증분석 및 불확도 등을 평가하고, 24 개 환경측정분석기관을 대상으로 실험실간 비교실험을 실시하였다. 폐수표준물질의 인증값 및 확장불확도는 KS A ISO 가이드 35(2005)에 의해 도출하였으며, 균질성에 기인한 표준불확도는 특성값의 0.43~2.67%로 나타났다. 환경측정분석기관간 비교실험에서 모든 항목의 비교실험 결과값이 정규분포를 따랐으며, 로버스트 평균값과 폐수표준물질의 인증값과 비교한 결과, 대부분의 항목에서 로버스트 평균값이 인증값보다 낮게 나타났다.

국내 생태독성 분석기관에 대한 숙련도시험 결과 평가 (Interlaboratory Study for Proficiency Testing on the Water Toxicity Determinations by Acute Toxicity Test with Daphnia magna)

  • 김종민;신기식;유순주;김명옥;최성헌
    • 한국물환경학회지
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    • 제30권6호
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    • pp.632-637
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    • 2014
  • Proficiency testing by interlaboratory comparisons is used to determine the performance of individual laboratories. In order to verify the quality of acute toxicity testing with Daphnia magna, National Institute of Environmental Research in South Korea is regularly organizing interlaboratory comparisons to estimate the analytical accuracy of different laboratories. Total 58 laboratories located in South Korea took part in interlaboratory proficiency testing scheme with three proficiency testing samples. TU(Toxic Unit) values of each laboratory were determined and robust z-score was calculated in order to evaluate the proficiency levels. Based on the robust z-score classification, 74% of the participant laboratories showed a satisfactory performance (43 laboratories). The main reason of 'unsatisfactory' performance seemed to be considered that the unsuitable management of test organism incubation system and the lack of experience on the identification of the test organism condition by effect of toxicity.

다중모드 및 단일모드 광섬유의 특성의 순회측정 (Interlaboratory Measurement Comparison of the Characteristics of Multi-mode and Single-mode Optical Fibers)

  • 안종평;전영윤;이동호;박희갑;김용환;강민호
    • 한국통신학회논문지
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    • 제10권6호
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    • pp.296-307
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    • 1985
  • 다중모드와 단일모드 광섬유의 특성을 순회측정한 결가이다. 7개의 다중모드 광섬유와 4개의 단일모드 광섬유를 사용하여 5개의 국내 기관이 참여하고 비교, 연구하였다. 그 결과를 외국의 순회측정과 비교하여 보았다.

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PM10 채취와 PM10 조성물질의 실험실간 동시측정 비교 연구 (Interlaboratory Comparison for the Sampling and Chemical Species Measurement of PM10)

  • 서영화;이병규;정용삼;정영주;문종화;이길용;심상권;홍완;최한우;김기현
    • 한국대기환경학회지
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    • 제15권4호
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    • pp.485-493
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    • 1999
  • This paper presents the results of the first interlaboratory comparison of ambient particles measurement conducted by 5 laboratories under the framework of Korean Society for Atmospheric Environment(KOSAE) on the May of 1998 in Seoul. Collection of particles less than 10$mu extrm{m}$(PM10) was carried out by two different types of PM10 sampler, and their concentration reported by three laboratories ranged from 36.2~56.05$\mu\textrm{g}$/㎥. Analyses of chemical composition of particles collected by each lab were performed by the destructive and nondestructive instrumental methods. Statistical analysis of the measurement results could not be carried out because a comprehensive QA/QC had not been applied before experiment. The importance of QA/QC as well as the performance of QA/QC for the measurement of PM10 was discussed in detail.

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제동디스크라이닝의 비교시험 연구 (A Study on Comparison Test for Brake Disc Lining)

  • 정종덕;권성태;한석윤;박기준;천홍정
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2005년도 추계학술대회 논문집
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    • pp.43-48
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    • 2005
  • In order to facilitate technical exchange among nations and/or institutes through the establishment of mutual recognition and the reliability guarantee of testing results by testing standards standardization, the interlaboratory comparison tests on brake discs and linings between KRRI and CARS were conducted. So far, two ways of comparison tests were performed for a better understanding of mutual recognition and standardization in railroad brake linings between Korea and China. In this paper, the first and second comparison testing results have been summarized, and the suggestions for the future research work are also presented to encourage extensive research on comparison study of railroad brake discs and linings between KRRI and CARS. Eventually, the final goal of the current research will be the establishment of standardization of railroad testing standards.

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동위원소희석 질량분석법에 의한 혈액 중 Cd, Pb 성분의 측정 : 국제공동분석 (Determination of Cd and Pb in Human Blood by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry : International Comparison)

  • 박창준;서정기;이상화
    • 분석과학
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    • 제9권2호
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    • pp.145-160
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    • 1996
  • 한국표준과학연구원 무기분석그룹에서는 1994년과 1995년도에 카나다 퀘백주 독성센터에서 실시한 혈액시료의 국제공동분석프로그램에 참여하였다. 이 프로그램의 목적은 생체시료에 있는 미량의 독성원소에 대해 참여하는 각국 실험실의 재현성과 정확도의 평가이다. 본 실험실에서는 3개 농도수준의 Pb과 Cd이 함유된 혈액시료를 동위원소희석 유도결합플라스마 질량분석법으로 분석하였다. 0.5mL의 혈액시료에 농축 동위원소를 첨가하고 질산 2mL와 함께 마이크로파 가압분해장치에서 분해한 후 약 10mL로 묽힌 후 ICP-MS에 주입하였다. 각국 실험실에서 보고한 Pb과 Cd의 농도를 나타내고 서로 비교하였으며 본 실험실에서 보고한 값은 모두 목표값에 매우 가까운 값을 얻었다.

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대기오염측정에 대한 정도관리의 필요성 - 1998년도 한국대기환경학회 측정분석분과회의 실험실간 비교분석사업 시행과 전개방향 (The Need for QA/QC in the Measurements of Airborne Pollutants - Conduction of and Directions towards an Interlaboratory Comparison Test in 1998 by the Measurement and Analysis Division of KOSAE)

  • 김기현;이강웅;김조천;서영화;이종해;허귀석
    • 한국대기환경학회지
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    • 제15권1호
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    • pp.63-69
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    • 1999
  • To offer a general guideline for the quantitative analysis of airborne pollutants, we designed and conducted a comprehensive QA/QC test using two different strategic approaches, namely (1) field-based comparative measurement and (2) laboratory-based comparative analysis. The former task was performed to make meaningful comparison of combined errors occurring from both sampling and analytical techniques in the measurements of such components as: (1) criteria pollutants, (2) volatile organic compounds (VOCs), and (3) particulate matters with the associated metals and ions. The latter task was also conducted to compare various types of bias arising mainly from the laboratory analytical procedures of (1) gaseous standards of VOCs and (2) of aqueous standards of metals and ions. The concentration data derived from each of these two different types of major tasks were evaluated per chemical species categorized as above. While the very details of these studies are to be reported on an individual basis according to the above classification of the project, this paper is presented to provide an overview of the whole project - its aim and direction.

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