• Title/Summary/Keyword: Interlaboratory comparison

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Interlaboratory Comparison of Critical Current Measurements on Ag-sheathed Bi-2223 tapes (Bi-2223선재의 임계전류 측정기술 비교)

  • Lee, Kyu-Won;Han, Gi-Youl
    • Progress in Superconductivity
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    • v.3 no.1
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    • pp.99-103
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    • 2001
  • We have conducted two runs of interlaboratory comparison on Ag-sheathed Bi-2223 tapes to evaluate the level of measurement techniques for the critical current measurement. Two classes of specimens were prepared for parallel and serial routings and sent to four participating laboratories. The critical currents of specimens were measured at 77 K in zero magnetic field. In the first comparison, we used twenty different Bi-2223 tapes as specimens for comparison and participating laboratories measured the specimens using their own instruments and procedures. As a result, the scattering of data on the first comparison showed -3.0% to +l2.2% for the parallel routing and -0.7% to +l5.1% for the serial routing. Major sources of these variations were attributed to different measurement techniques. Thus, the second comparison of measurement was done on the same specimens under specified measurement conditions, particularly in terms of cooling procedure and sweep rate of the test current. The variations for the second comparison were decreased -3.1% to +3.2% far the parallel routing and -1.8% to +7.7% fur the serial routing.

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Preparation of wastewater-based reference materials for heavy metal analysis and interlaboratory study (중금속분석용 폐수표준물질 제조 및 실험실간 비교평가)

  • Kim, Young-Hee;Song, Ki-Bong;Shin, Sun-Kyoung;Lee, Jung-Sub;Jeong, Gi-Taeg;Hong, Eun-Jin;Park, Jin-Ju;Yu, Suk-Min
    • Analytical Science and Technology
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    • v.23 no.3
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    • pp.295-303
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    • 2010
  • In this study, the wastewater-based reference material (RM) was prepared and certified for 7 trace metal elements with evaluation of uncertainties. The RM was distributed to 25 laboratories for the interlaboratory comparison testing. The certified values and expanded uncertainties were derived using ISO guideline 35 and the standard uncertainties for homogenieties were 0.43~2.67% of certified values. The analytical results from the interlaboratory comparison testing showed normal distributions and the robust means from the interlaboratory comparison testing were higher than the certified values of the RM for all analytes.

Interlaboratory Study for Proficiency Testing on the Water Toxicity Determinations by Acute Toxicity Test with Daphnia magna (국내 생태독성 분석기관에 대한 숙련도시험 결과 평가)

  • Kim, Jongmin;Shin, Kisik;Yu, Soonju;Kim, Myeong Ock;Choe, Sung Hun
    • Journal of Korean Society on Water Environment
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    • v.30 no.6
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    • pp.632-637
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    • 2014
  • Proficiency testing by interlaboratory comparisons is used to determine the performance of individual laboratories. In order to verify the quality of acute toxicity testing with Daphnia magna, National Institute of Environmental Research in South Korea is regularly organizing interlaboratory comparisons to estimate the analytical accuracy of different laboratories. Total 58 laboratories located in South Korea took part in interlaboratory proficiency testing scheme with three proficiency testing samples. TU(Toxic Unit) values of each laboratory were determined and robust z-score was calculated in order to evaluate the proficiency levels. Based on the robust z-score classification, 74% of the participant laboratories showed a satisfactory performance (43 laboratories). The main reason of 'unsatisfactory' performance seemed to be considered that the unsuitable management of test organism incubation system and the lack of experience on the identification of the test organism condition by effect of toxicity.

Interlaboratory Measurement Comparison of the Characteristics of Multi-mode and Single-mode Optical Fibers (다중모드 및 단일모드 광섬유의 특성의 순회측정)

  • 안종평;전영윤;이동호;박희갑;김용환;강민호
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.10 no.6
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    • pp.296-307
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    • 1985
  • The reults of the interlaboratory measurement comparison of the multimode and single mode fiber papameters are reported. 7 multi-mode fiber spools and 4 single mode spools are used and 5 independent domestic organizations (ETRI & 4 optical fiber manufacturing companies) are participated in the comparison study. Our results are compared with those of the comparison studies conducted in the foreign countries.

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Interlaboratory Comparison for the Sampling and Chemical Species Measurement of PM10 (PM10 채취와 PM10 조성물질의 실험실간 동시측정 비교 연구)

  • Seo, Young-Hwa;Lee, Byung-Kyu;Chung, Yong-Sam;Chung, Young-Ju;Moon, Jong-Hwa;Lee, Kil-Yong;Shim, Sang-Kwon;Hong, Wan;Choi, Han-Woo;Kim, Ki-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.4
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    • pp.485-493
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    • 1999
  • This paper presents the results of the first interlaboratory comparison of ambient particles measurement conducted by 5 laboratories under the framework of Korean Society for Atmospheric Environment(KOSAE) on the May of 1998 in Seoul. Collection of particles less than 10$mu extrm{m}$(PM10) was carried out by two different types of PM10 sampler, and their concentration reported by three laboratories ranged from 36.2~56.05$\mu\textrm{g}$/㎥. Analyses of chemical composition of particles collected by each lab were performed by the destructive and nondestructive instrumental methods. Statistical analysis of the measurement results could not be carried out because a comprehensive QA/QC had not been applied before experiment. The importance of QA/QC as well as the performance of QA/QC for the measurement of PM10 was discussed in detail.

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A Study on Comparison Test for Brake Disc Lining (제동디스크라이닝의 비교시험 연구)

  • Chung Jong-Duk;Kwon Sung-Tae;Han Seok-Yoon;Park Ki-Joon;Chun Hong-Jung
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.10a
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    • pp.43-48
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    • 2005
  • In order to facilitate technical exchange among nations and/or institutes through the establishment of mutual recognition and the reliability guarantee of testing results by testing standards standardization, the interlaboratory comparison tests on brake discs and linings between KRRI and CARS were conducted. So far, two ways of comparison tests were performed for a better understanding of mutual recognition and standardization in railroad brake linings between Korea and China. In this paper, the first and second comparison testing results have been summarized, and the suggestions for the future research work are also presented to encourage extensive research on comparison study of railroad brake discs and linings between KRRI and CARS. Eventually, the final goal of the current research will be the establishment of standardization of railroad testing standards.

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Determination of Cd and Pb in Human Blood by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry : International Comparison (동위원소희석 질량분석법에 의한 혈액 중 Cd, Pb 성분의 측정 : 국제공동분석)

  • Park, C.J.;Suh, J.K.;Lee, S.H.
    • Analytical Science and Technology
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    • v.9 no.2
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    • pp.145-160
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    • 1996
  • Inorganic analytical laboratory of Korea Research Institute of Standards and Science participated in an interlaboratory comparison program operated by Quebec Toxicology Centre of Canada in 1994 and again in 1995. The objective of this program is to enable participating laboratories to assess reproducibility and accuracy of their analytical results for trace toxic elements in human biological fluids. This laboratory determined Cd and Pb concentrations in 3 levels of human blood samples by isotope dilution inductively coupled plasma mass spectrometry. 0.5mL of blood sample is added to the digestion bomb together with 2mL of nitric acid and enriched spike isotopes and then decomposed in the microwave digestion system. The decomposed sample is diluted to 10mL and nebulized into ICP-MS. The Cd and Pb values reported by all participating laboratories are presented and compared. The values reported by this laboratory are within the acceptable range of target values.

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The Need for QA/QC in the Measurements of Airborne Pollutants - Conduction of and Directions towards an Interlaboratory Comparison Test in 1998 by the Measurement and Analysis Division of KOSAE (대기오염측정에 대한 정도관리의 필요성 - 1998년도 한국대기환경학회 측정분석분과회의 실험실간 비교분석사업 시행과 전개방향)

  • 김기현;이강웅;김조천;서영화;이종해;허귀석
    • Journal of Korean Society for Atmospheric Environment
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    • v.15 no.1
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    • pp.63-69
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    • 1999
  • To offer a general guideline for the quantitative analysis of airborne pollutants, we designed and conducted a comprehensive QA/QC test using two different strategic approaches, namely (1) field-based comparative measurement and (2) laboratory-based comparative analysis. The former task was performed to make meaningful comparison of combined errors occurring from both sampling and analytical techniques in the measurements of such components as: (1) criteria pollutants, (2) volatile organic compounds (VOCs), and (3) particulate matters with the associated metals and ions. The latter task was also conducted to compare various types of bias arising mainly from the laboratory analytical procedures of (1) gaseous standards of VOCs and (2) of aqueous standards of metals and ions. The concentration data derived from each of these two different types of major tasks were evaluated per chemical species categorized as above. While the very details of these studies are to be reported on an individual basis according to the above classification of the project, this paper is presented to provide an overview of the whole project - its aim and direction.

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