• 열처리공학회지
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• 제17권1호
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• pp.29-35
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• 2004

The effect of low tempering in a temperature range of $150{\sim}400^{\circ}C$ on corrosion resistance in 420J2 stainless steel austenitized at $1000^{\circ}C$ was investigated by the application of salt spray test, electrochemical pitting test in 3.5% NaCl solution and DL-EPR test for intergranular corrosion in 0.5M $H_2SO_4$+0.01M KSCN solution. In salt spray test, good corrosion resistance was obtained in a tempering temperature range of $150{\sim}250^{\circ}C$. Pitting potential was increased to the tempering temperature of $250^{\circ}C$, but decreased with the increase of temperature up to $400^{\circ}C$ And it was thought that the degradation of pitting corrosion resistance showed at the tempering temperature of around $400^{\circ}C$ was due to the precipitation of $Cr_7C_3$ of $M_7C_3$ type. The degree of sensitization showed increasing tendency with the increase of tempering temperature, and also Cr depletion phenomena were observed in the vicinity of grain boundary.

• Corrosion Science and Technology
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• 제17권6호
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• pp.279-286
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• 2018

Austenitic stainless steels used in nuclear power plants mainly use pipes made of seamless pipes, which depend on imports. The manufacturing process and high cost are some of the problems associated with seamless pipes. Therefore, in this study, the corrosion characteristics of the seamless pipe and the SAW pipe were assessed to determine the safety and reliability of the SAW pipe in a bid to replace the seamless pipe. Microstructure was analyzed using an optical microscope and the degree of hardness was measured using a Rockwell B scale. Intergranular corrosion resistance was evaluated by ASTM A262 Practice A, C, and E methods. The degree of sensitization was determined using a DL-EPR test. Anodic polarization test was performed in deaerated 1% NaCl solution at $30^{\circ}C$ and the U-bend method was used to evaluate the SCC resistance in 0.01 M $Na_2S_4O_6$ at $340^{\circ}C$ and 40% NaOH solution at $290^{\circ}C$. Weld metal of the SAW pipe specimen showed relatively high degree of sensitization and intergranular corrosion rate. However, annealing to SAW pipes improved the corrosion properties in comparison to that of the seamless pipe.

• 한국원자력학회:학술대회논문집
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• 한국원자력학회 1998년도 추계학술발표회요약집
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• pp.241-241
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• 1998

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 1998년도 춘계학술발표회 초록집
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• pp.110-111
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• 1998

• 한국기계가공학회지
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• 제5권3호
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• pp.86-91
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• 2006

The compressive residual stress, which is inducing by shot peening process, has the effect of increasing the intrinsic fatigue strength of surface and therefore would be beneficial in reducing the probability of fatigue damage. However, it was not known that the effect of shot peening in corrosion environment. In this study, the influence of shot peening and corrosion condition for corrosion property were investigated on immersed in 3.5% NaCl, 10% HNO3 + 3% HF, 6% $FeCl_3$. The immersion test was performed with two kind of specimen. The immersion periods was performed 150days. Corrosion potential, weight loss were investigated from experimental results. From test results, the effect of shot peening on the corrosion characteristics was evaluated.

• 한국재료학회지
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• 제34권7호
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• pp.330-340
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• 2024

Al-Mg-Si alloys are light weight and have excellent corrosion resistance, and are attracting attention as a liner material for high-pressure hydrogen containers in hydrogen fuel cell vehicles. Because it has excellent plastic hardening properties, it is also applied to car body panel materials, but it is moderate in strength, so research to improve the strength by adding Si-rich or Cu is in progress. So far, the authors have conducted research on the intergranular fracture of alloys with excessive Si addition from the macroscopic mechanical point of view, such as specimen shape. To evaluate their impact tensile properties, the split-Hopkinson bar impact test was performed using thin plate specimens of coarse and fine grain alloys of Al-Mg-X (X = Cr,Si) alloy. The effect of the shape of the specimen on the characteristics was studied through finite element method (FEM) analysis. As a result, it was found that the intergranular fracture of the alloy with excessive Si depended on the specimen width (W)/grain size (d), which can be expressed by the specimen size and grain size. As W/d decreases, the intergranular fracture transforms into a transgranular fracture. As the strain rate increases, the fracture elongation decreases, and the fracture surface of the intergranular fracture becomes more brittle. It was confirmed that intergranular fracture occurred in the high strain rate region even in materials with small grain sizes.

• Corrosion Science and Technology
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• 제7권3호
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• pp.187-191
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• 2008

Transgranular stress corrosion cracking of nickel base alloys was reported by Copson and Dean in 1965. Study to establish this cracking mechanism needs to be carried out. Laboratory stress corrosion tests were performed for mill annealed(MA) or thermally treated(TT) steam generator tubing materials in a high temperature water containing lead. An electrochemical interaction of lead with the alloying elements of SG tubings was also investigated. Alloy 690 TT showed a transgranular stress corrosion cracking in a 40% NaOH solution with 5000 ppm of lead, while intergranular stress corrosion racking was observed in a 10% NaOH solution with 100 ppm lead. Lead seems to enhance the disruption of passive film and anodic dissolution of alloy 600 and alloy 690. Crack tip blunting at grain boundary carbides plays a role for the transgranular stress corrosion cracking.

• 대한기계학회논문집
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• 제13권2호
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• pp.236-242
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• 1989

본 연구에서는 주로 보일러의 과열기 및 재열기등의 관재료로 널리 사용되고 있는 304 스테인레스강에 대하여 실제 고온부식현상을 재현한 부식환경하인 630.deg. C, 690.deg. C 및 750.deg. C 3가지 온도범위에서 크리프시험을 실시하고 고온부식이 크리프파단 특성에 미치는 영향을 부식조건이 없는 고온대기중의 실험결과와 비교 검토하였다.

• Corrosion Science and Technology
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• 제13권3호
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• pp.87-94
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• 2014

Recently, the application of bending products has been increased since the industries such as automobile, aerospace, ships, and plants greatly need the usage of pipes. For facility fabrication, bending process is one of key technologies for pipings. Induction heat bending process is composed of bending deformation by repeated local heat and cooling. Because of local heating and compressive strain, detrimental phases may be precipitated and microstructural change can be induced. This work focused on the effect of induction heat bending process on the properties of ASME SA312 TP316 stainless steel. Evaluation was done on the base metal and the bended areas before and after heat treatment. Microstructure analysis, intergranular corrosion test including Huey test, double loop electropotentiokinetic reactivation test, oxalic acid etch test, and anodic polarization test were performed. On the base of microstructural analysis, grain boundaries in bended extrados area were zagged by bending process, but there were no precipitates in grain and grain boundary and the intergranular corrosion rate was similar to that of base metal. However, pitting potentials of bended area were lower than that of the base metal and zagged boundaries was one of the pitting initiation sites. By re-annealing treatment, grain boundary was recovered and pitting potential was similar to that of the base metal.

• 한국공작기계학회:학술대회논문집
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• 한국공작기계학회 1997년도 춘계학술대회 논문집
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• pp.143-149
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• 1997

the horizontal corrosion fatigue tester has been developed for investigating environmental strength. Using this tester, we investigated about corrosion fatigue caracteristic for A106 GrB steel weldments in 3.5% synthetic seawater and room temperature. Considered parameter is only frequency of 1,3 and 5Hz. and Corrosion fatigue crack length was measured by DC potential difference method. From the results, we could find that the horizontal corrosion fatiued tester could be well applied to estimation of fatigue strength. and In case of 5Hz, corrosion fatigue crack growth path of A106 GrB steel weldment was transgranular, and of 1 and 3Hz showed that transgranular and intergranular was mixed. Also, Corrosion fatigue crack growth caracteristic values estimated in each frequency were C=9.33 x 10-9 and m=2.93 in 1Hz, C=9.77x10-10 and m=3.47 in 3Hz, C=1.02x10-10 and m=4.05 in 1Hz