• 제목/요약/키워드: Instrumental analyses

검색결과 145건 처리시간 0.019초

품종이 다른 나물콩으로 재배한 콩나물의 품질 특성 (Quality Characteristics of Bean Sprouts with Different Namulkong Cultivars)

  • 손희경;김용호;이경애
    • 한국식품조리과학회지
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    • 제30권3호
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    • pp.340-350
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    • 2014
  • 껍질 색이 다른 5품종의 나물콩으로 5일간 재배한 콩나물의 이화학적 특성과 관능적 특성을 검토하였다. 본 실험에 사용한 나물콩인 녹채콩, 다원콩, 서남콩, 오리알태, 풍산나물콩의 썹질 색은 각각 연한 녹색, 검은색, 노란색, 진한 녹색, 노란색이었다. 5일 재배 후 수확한 콩나물의 재배수율은 540.00%~658.32% 이었다. 생콩나물과 삶은 콩나물의 머리 부분은 줄기 부분에 비해 견고성 견고성이 높았으며 가열에 의해 머리와 줄기 부분의 견고성이 낮아졌다. 생콩나물과 삶은 콩나물의 리폭시게나제 활성은 머리 부분이 줄기 부분에 비해 높았으며 3분간 가열 후 머리와 줄기의 리폭시게나제 활성이 감소되었다. 콩나물의 클로로필 a와 b의 함량은 머리 부분이 줄기에 비해 높았으며 3분간 가열에 의해 콩나물의 클로로필 함량은 나물콩 품종에 따라 감소 또는 다소 증가하는 경향을 보였다. 전반적인 기호도는 생콩나물의 경우 다원콩 콩나물, 서남콩 콩나물, 풍산나물콩 콩나물이 녹채콩 콩나물과 오리알태 콩나물에 비해 높았으며 삶은 콩나물과 콩나물 무침은 서남콩 콩나물과 풍산나물콩 콩나물이 가장 높았다.

인도네시아 저등급 석탄의 스팀 가스화 반응성 비교 평가 (Comparative Evaluation of Steam Gasification Reactivity of Indonesian Low Rank Coals)

  • 김수현;;유지호;이시훈;임영준;임정환;김상도;전동혁;최호경
    • 한국수소및신에너지학회논문집
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    • 제27권6호
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    • pp.693-701
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    • 2016
  • Steam gasification of low rank coals is possible at relatively low temperature and low pressure, and thus shows higher efficiency compared to high rank coals. In this study, the gasification reactivity of four different Indonesian low rank coals (Samhwa, Eco, Roto, Kideco-L) was evaluated in $T=700-800^{\circ}C$. The low rank coals containing $53.8{\pm}3.4$ wt% volatile matter in proximate analysis and $71.6{\pm}1.2$ wt% carbon in ultimate analysis showed comparable gasification reactivity. In addition, $K_2CO_3$ catalyst rapidly accelerated the reaction rate at $700^{\circ}C$, and all of the coals were converted over 90% within 1 hour. The XRD analysis showed no significant difference in carbonization between the coals, and the FT-IR spectrum showed similar functional groups except for differences due to moisture and minerals. TGA results in pyrolysis ($N_2$) and $CO_2$ gasification atmosphere showed very similar behavior up to $800^{\circ}C$ regardless of the coal species, which is consistent with the steam gasification results. This confirms that the indirect evaluation of the reactivity can be made by the above instrumental analyses.

뇌졸중 환자의 균형과 기능 수행 및 보행 검사를 위한 평가도구의 비교: BBS, TUG, TUG, Fugl-Meyer, MAS-G, C·MGS, and MBI (Correlation Between Balance, Walking Test and Functional Performance in Stroke Patients: BBS, TUG, Fugl-Meyer, MAS-G, C·MGS, and MBI)

  • 안승헌;박창식;이현주
    • 한국전문물리치료학회지
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    • 제14권3호
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    • pp.64-71
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    • 2007
  • The purposes of this study were to determine correlations between the Berg Balance Test (BBS), Timed -UP & Go Test, Fugl Meyer-L/E, Balance, Sensory (FM-L/E, B, S), Motor Assessment Scale-Gait (MAS-G), Comfortable maximal Gait Speed (C MGS), and the Modified Barthel Index (MBI). The subjects were 40 stroke patients of the Korea National Rehabilitation Center in Seoul. Main outcome measures were Balance control (BBS, FM-B), Gait (TUG, C MGS, MAS-G), ADL (MBI) and Motor Function of Lower Extremities (FM-L/E, S). The data were analyzed using Pearson product correlation. FM scales between other clinical and instrumental indexes and multiple stepwise regression analyses were performed to identify prognostic factors for Balance, Gait and ADL Motor Function of Lower Extremity inclinations. The results of this study were as follows: The BBS, FM-L/E, balance, sensory and MBI showed positive correlation relations, but TUG and C MGS showed negative correlations. The sensory factor of the FM-scale showed the strongest variance in predicting BBS. However the FM-balance showed the strongest variance in predicting TUG, MAS-G and C MGS. The use of both quantitative and qualitative scales was shown to be a good measuring instrument for the classification of the general clinical performance of the patients.

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Streptomyces sp. YBE-316이 생산하는 항암성 항생물질의 정제 및 특성 (Purification and Characterization of the Antitumor Antibiotic from Streptomyces sp. YBE-316)

  • 박재홍;함병권;배동훈;유주현
    • 한국미생물·생명공학회지
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    • 제23권3호
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    • pp.329-336
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    • 1995
  • For the development of new antitumor antibiotics produced by microorganisms, Streptomyces sp. YBE-316 was isolated from soil. The productivity of the antitumor antibiotic from Streptomyces sp. YBE-316 gradually increased after 60 hours, and was maximum after 100 hours after inoculation in growth medium (2.0% sucrose, 1.0% soybean meal, 0.1% K$_{2}$HPO$_{4}$, pH 7.0) at 30$\circ$C, 150 rpm, 5 NL/min by 30 l jar fermentor. This antitumor antibiotic was present only in mycelium, and stable in pH 5.0-10.0 for 20 minutes at 100$\circ$C. Antitumor and antibiotic activities were maintained at neutral pH, and heat stability was low. This antitumor antibiotic was soluble in methanol and ethanol, and insoluble in water, ethyl acetate, chloroform, and n-hexane. This antitumor antibiotic was sequentially purified by acetone extraction from mycelium, butanol extraction, and silica gel column chromatography. Antitumor activity was low against most tested cell lines, but antibiotic activity was high and low against yeasts and bacteria, respectivelv. The visualization test showed that this antitumor antibiotic had higher hydroxyl, ketone, amino, carboxyl groups, and sugar(s) in its structure. Instrumental analyses showed that this antitumor antibiotic was a pentaene in polyene class antibiotics. In pentaene class antibiotics, this was considered as an eurocidin or capacidin type antibiotics. The molecular weight of this antitumor antibiotic was higher than 683.0 daltons, and this antitumor antibiotic might be glycosylated by other sugar(s), instead of mycosamine or perosamine, an amino sugar.

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PECVD법에 의해 증착된 Ti-B-C코팅막 내의 보론함량과 증착온도에 따른 미세구조 및 기계적 물성의 변화 (The Effect of Boron Content and Deposition Temperature on the Microstructure and Mechanical Property of Ti-B-C Coating Prepared by Plasma-enhanced Chemical Vapor Deposition)

  • 옥정태;송풍근;김광호
    • 한국표면공학회지
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    • 제38권3호
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    • pp.106-111
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    • 2005
  • Ternary Ti-B-C coatings were synthesized on WC-Co and Si wafers substrates by a PECVD technique using a gaseous mixture of $TiCl_4,\;BCl_3,\;CH_4,\;Ar,\;and\; H_2$. The effects of deposition variables such as substrate temperature, gas ratio, $R_x=[BCl_3/(CH_4+BCl_3)]$ on the microstructure and mechanical properties of Ti-B-C coatings were investigated. From our instrumental analyses, the synthesized Ti-B-C coatings was confirmed to be composites consisting of nanocrystallites TiC, quasi-amorphous TiB2, and amorphous carbon at low boron content, on the contrary, nanocrystallites $TiB_2$, quasi-amorphous TiC, and amorphous carbon at relatively high boron content. The microhardness of the Ti-B-C coatings increased from $\~23 GPa$ of TiC to $\~38 GPa$ of $Ti_{0.33}B_{0.55}C_{0.11}$ coatings with increasing the boron content. The $Ti_{0.33}B_{0.55}C_{0.11}$ coatings showed lower average friction coefficient of 0.45, in addition, it showed relatively better wear behavior compared to other binary coatings of $TiB_2$ and TiC. The microstruture and microhardness value of Ti-B-C coatings were largely depend on the deposition temperature.

산초나무 추출물의 피부사상균에 대한 항균활성과 그 성분 (Antifungal Activity of the Extracts of Zanthoxylum Schinifolium Sieb. et Zucc. against Dermatophytes)

  • 민경희
    • Journal of the Korean Wood Science and Technology
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    • 제26권4호
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    • pp.78-85
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    • 1998
  • 산초나무 각 부위별 알코올추출물의 피부사상균에 대한 항균활성은 근피 추출물에서 가장 높게 나타났으며, 각 용매별 분획분의 항균활성은 근피부의 petroleum ether 분획에서 가장 높게 나타났다. 항균활성성분을 분리하기 위해 항균력이 가장 높게 나타난 근피알코올추출물의 petroleum ether 분획분을 silica gel column chromatography를 실시하였으며, 항균활성성분인 CI과 CII가 분리되었다. CI과 CII의 MIC을 측정한 결과 CI의 MIC은 $40{\mu}g/m\ell$였으며, $20{\mu}g/m\ell$의 농도에서도 균액의 접종흔적이 조금 남아있었을 뿐 균사의 생장은 관찰할 수 없었다. 또한 CII의 MIC은 $800{\mu}g/m\ell$였으며, $600{\mu}g/m\ell$의 농도에서도 균액의 접종흔적이 조금 있었을 뿐 다른 농도에서처럼 균사의 생장은 관찰할 수 없었다. 기기 분석 결과 CI과 CII는 기지(旣知)의 alkaloid 화합물들이었다.

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Paleoseismological implications of liquefaction-induced structures caused by the 2017 Pohang Earthquake

  • Gihm, Yong Sik;Kim, Sung Won;Ko, Kyoungtae;Choi, Jin-Hyuck;Bae, Hankyung;Hong, Paul S.;Lee, Yuyoung;Lee, Hoil;Jin, Kwangmin;Choi, Sung-ja;Kim, Jin Cheul;Choi, Min Seok;Lee, Seung Ryeol
    • Geosciences Journal
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    • 제22권6호
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    • pp.871-880
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    • 2018
  • During and shortly after the 2017 Pohang Earthquake ($M_w$ 5.4), sand blows were observed around the epicenter for the first time since the beginning of instrumental seismic recording in South Korea. We carried out field surveys plus satellite and drone imagery analyses, resulting in observation of approximately 600 sand blows on Quaternary sediment cover in this area. Most were observed within 3 km of the epicenter, with the farthest being 15 km away. In order to investigate the ground's susceptibility to liquefaction, we conducted a trench study of a 30 m-long sand blow in a rice field 1 km from the earthquake epicenter. The physical characteristics of the liquified sediments (grain size, impermeable barriers, saturation, and low overburden pressure) closely matched the optimum ground conditions for liquefaction. Additionally, we found a series of soft sediment deformation structures (SSDSs) within the trench walls, such as load structures and water-escaped structures. The latter were vertically connected to sand blows on the surface, reflecting seismogenic liquefaction involving subsurface deformation during sand blow formation. This genetic linkage suggests that SSDS research would be useful for identifying prehistoric damage-inducing earthquakes ($M_w$ > 5.0) in South Korea because SSDSs have a lower formation threshold and higher preservational potential than geomorphic markers formed by surface ruptures. Thus, future combined studies of Quaternary surface faults and SSDSs are required to provide reliable paleoseismological information in Korea.

초고경도 Ti-Al-Si-N 나노복합체 코팅막의 미세구조 및 트라이볼로지 거동에 관한 연구 (A Study on Microstructure and Tribological Behavior of Superhard Ti-Al-Si-N Nanocomposite Coatings)

  • 허성보;김왕렬
    • 한국표면공학회지
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    • 제54권5호
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    • pp.230-237
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    • 2021
  • In this study, the influence of silicon contents on the microstructure, mechanical and tribological properties of Ti-Al-Si-N coatings were systematically investigated for application of cutting tools. The composition of the Ti-Al-Si-N coatings were controlled by different combinations of TiAl2 and Ti4Si composite target powers using an arc ion plating technique in a reactive gas mixture of high purity Ar and N2 during depositions. Ti-Al-Si-N films were nanocomposite consisting of nanosized (Ti,Al,Si)N crystallites embedded in an amorphous Si3N4/SiO2 matrix. The instrumental analyses revealed that the synthesized Ti-Al-Si-N film with Si content of 5.63 at.% was a nanocomposites consisting of nano-sized crystallites (5-7 nm in dia.) and a three dimensional thin layer of amorphous Si3N4 phase. The hardness of the Ti-Al-Si-N coatings also exhibited the maximum hardness value of about 47 GPa at a silicon content of ~5.63 at.% due to the microstructural change to a nanocomposite as well as the solid-solution hardening. The coating has a low friction coefficient of 0.55 at room temperature against an Inconel alloy ball. These excellent mechanical and tribological properties of the Ti-Al-Si-N coatings could help to improve the performance of machining and cutting tool applications.

청년 남녀의 사회경제적 특성 및 세대관계 특성이 결혼의향에 미치는 영향 (Socioeconomic and intergenerational characteristics associated with marital intentions among Korean men and women in young adulthood)

  • 권소영;강시은;엄세원;박지수;이재림
    • 한국가족관계학회지
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    • 제21권4호
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    • pp.3-25
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    • 2017
  • Objectives: We examined which socioeconomic and intergenerational characteristics were associated with the level of intention to marry among Korean men and women in young adulthood. Method: Data came from 351 men and 391 women who were 25-34 years old, had never been married, and had at least one living parent. We conducted multiple regression analyses by gender after controlling for age and current romantic relationship. Results: Among the socioeconomic characteristics, more years of education was linked to both men's and women's higher levels of intention to marry. For women, having a secure, full-time job was related to greater intention to marry. For men, the higher their subjective socioeconomic status, the greater their intention to marry. Among intergenerational characteristics, both men's and women's positive attitudes toward supporting elderly parents were related to a higher level of intention to marry. For men, the frequency of providing instrumental support for their parents was negatively associated with the men's intention to marry. For women, higher levels of agreement with parents' responsibility to support their adult children as well as greater affection for their parents were positively related to greater intention to marry. Conclusions: The findings suggest that young adults' socioeconomic resources and the family context are important predictors of young adults' marital intentions. The results also reveal gender differences in the factors associated with young adults' marital intentions.

모유 중 지방산 조성 및 구조 분석 (Compositions of fatty acids and structural identification in human breast milk)

  • 유지우;금영수;강남미
    • 분석과학
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    • 제35권6호
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    • pp.229-236
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    • 2022
  • 모유의 지질대사체에 대한 연구는 축산유래 유제품의 경우와 비교하여 매우 제한적으로 이루어져 있다. 본 연구는 지용성 대사체 연구의 선행연구로서, 모유중 극성 및 비극성 지질 중의 주요 지방산 조성에 대한 세부적 정량법 및 구조동정을 목적으로 수행되었다. 인지질을 포함한 극성 지질과 비극성 지질의 분리를 위하여 silica gel을 활용한 정제법을 개발하였으며, 효과적인 methyl ester 및 pyridylcarbinol ester 유도체화 방법을 적용하여 개별 분획의 세부적 지방산조성을 분석한 결과, 16 종의 필수지방산을 확인하였으며, 이와 함께 29 종의 미량 지방산이 확인되어, 구조 분석을 실시하였다. 측쇄 지방산의 경우, 15-18 개의 탄소를 보유한 iso 및 anteiso 지방산이 주요한 것으로 확인되었다.