• 제목/요약/키워드: Inhomogeneous

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ECAP 가공에 의해 제조된 초미세립 OFHC Cu 봉재의 미세조직 및 기계적 특성의 균질성 (Homogeneity of Microstructure and Mechanical Properties of Ultrafine Grained OFHC Cu Bars Processed by ECAP)

  • 지정훈;박이주;김형원;황시우;이종수;박경태
    • 대한금속재료학회지
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    • 제49권6호
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    • pp.474-487
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    • 2011
  • Bars of OFHC Cu with the diameter of 45 mm were processed by equal channel angular pressing up to 16 passes via route $B_c$, and homogeneity of their microstructures and mechanical properties was examined at every four passes which develop the equiaxed ultrafine grains. In general, overall hardness, yield strength and tensile strength increased by 3, 7, and 2 times respectively compared with those of unECAPed sample. Cross-sectional hardness exhibited a concentric distribution. Hardness was the highest at the center of bar and it decreased gradually from center to surface. After 16 passes, overall hardness decreased due to recovery and partial recrystallization. Regardless of the number of passage, yield strength and tensile strength were quite uniform at all positions, but elongation showed some degree of scattering. At 4 passes, coarse and ultrafine grains coexisted at all positions. After 4 passes, uniform equiaxed ultrafine grains were obtained at the center, while uniform elongated ultrafine grains were manifested at the upper half position. At the lower half position, grains were equiaxed but its size were inhomogeneous. It was found that inhomogeneity of grain morphology and grain size distribution at different positions are to be attributed to scattering in elongation but they did not affect strength. The present results reveal the high potential of practical application of equal channel angular pressing on fabrication of large-sized ultrafine grained bars with quite homogeneous mechanical properties.

자동차 부품용 내열 알루미늄 합금의 고온 피로 변형 거동 (High Temperature Fatigue Deformation Behavior of Automotive Heat Resistant Aluminum Alloys)

  • 박종수;성시영;한범석;정창렬;이기안
    • 대한금속재료학회지
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    • 제48권1호
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    • pp.28-38
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    • 2010
  • High temperature high cycle and low cycle fatigue deformation behavior of automotive heat resistant aluminum alloys (A356 and A319 based) were investigated in this study. The microstructures of both alloys were composed of primary Al-Si dendrite and eutectic Si phase. However, the size and distribution for eutectic Si phase varied: a coarse and inhomogeneous distributed was observed in alloy B (A319 based). A brittle intermethallic phase of ${\alpha}-Fe\;Al_{12}(Fe,Mn)_3Si_2$ was detected only in B alloy. Alloy B exhibited high fatigue life only under a high stress amplitued condition in the high cycle fatigue results, whereas alloy A showed high fatigue life when stress was lowered. With regard to the low-cycle fatigue result ($250^{\circ}C$) showing higher fatigue life as ductility increased, alloy A demonstrated higher fatigue life under all of the strain amplitude conditions. Fractographic observations showed that large porosities and pores near the outside surface could be the main factor in the formation of fatigue cracks. In alloy B. micro-cracks were formed in both the brittle intermetallic and coarse Si phasese. These micro-cracks then coalesced together and provided a path for fatigue crack propagation. From the observation of the differences in microstructure and fractography of these two automotive alloys, the authors attempt to explain the high-temperature fatigue deformation behavior of heat resistant aluminum alloys.

플루오라이트 구조 강유전체 박막의 분극 반전 동역학 리뷰 (A Brief Review on Polarization Switching Kinetics in Fluorite-structured Ferroelectrics)

  • 김세현;박근형;이은빈;유근택;이동현;양건;박주용;박민혁
    • 한국표면공학회지
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    • 제53권6호
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    • pp.330-342
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    • 2020
  • Since the original report on ferroelectricity in Si-doped HfO2 in 2011, fluorite-structured ferroelectrics have attracted increasing interest due to their scalability, established deposition techniques including atomic layer deposition, and compatibility with the complementary-metal-oxide-semiconductor technology. Especially, the emerging fluorite-structured ferroelectrics are considered promising for the next-generation semiconductor devices such as storage class memories, memory-logic hybrid devices, and neuromorphic computing devices. For achieving the practical semiconductor devices, understanding polarization switching kinetics in fluorite-structured ferroelectrics is an urgent task. To understand the polarization switching kinetics and domain dynamics in this emerging ferroelectric materials, various classical models such as Kolmogorov-Avrami-Ishibashi model, nucleation limited switching model, inhomogeneous field mechanism model, and Du-Chen model have been applied to the fluorite-structured ferroelectrics. However, the polarization switching kinetics of fluorite-structured ferroelectrics are reported to be strongly affected by various nonideal factors such as nanoscale polymorphism, strong effect of defects such as oxygen vacancies and residual impurities, and polycrystallinity with a weak texture. Moreover, some important parameters for polarization switching kinetics and domain dynamics including activation field, domain wall velocity, and switching time distribution have been reported quantitatively different from conventional ferroelectrics such as perovskite-structured ferroelectrics. In this focused review, therefore, the polarization switching kinetics of fluorite-structured ferroelectrics are comprehensively reviewed based on the available literature.

수직하중을 받는 Barrette 말뚝의 고유진동수 특성 (Natural Frequency Characteristics of Vertically Loaded Barrettes)

  • 이준규;고준영;최용혁;박구병;김재영
    • 대한토목학회논문집
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    • 제41권1호
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    • pp.39-48
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    • 2021
  • 본 논문에서는 정적 수직하중을 받는 barrette 말뚝의 고유진동수를 산정할 수 있는 해석모델을 제안하였다. 비균질 지반에 설치된 직사각형 마찰말뚝의 자유진동을 지배하는 미분방정식을 유도하였다. 이 지배방정식을 Runge-Kutta 법을 이용하여 수치적분하였고, 미분방정식의 고유치인 고유진동수는 Regula-Falsi 법을 이용하여 산정하였다. 말뚝의 고유진동수는 유한요소해석의 결과와 잘 일치하였다. 말뚝의 고유진동수를 증가시키는 말뚝변수는 단면형상비, 마찰저항비, 지반강성비이고, 감소시키는 말뚝변수는 마찰형상비, 세장비, 압축계수이다.

트윈롤 주조법으로 제조된 마그네슘합금 판재의 균질화 열처리에 따른 미세조직 및 집합조직 발달 (Investigating the Effect of Homogenization Heat Treatment on the Microstructure and Texture of Magnesium Alloy Sheet Manufactured via Twin Roll Casting)

  • 이희재;박노진
    • 열처리공학회지
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    • 제34권3호
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    • pp.122-129
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    • 2021
  • This study focuses on the microstructural development of 99% magnesium alloy sheet manufactured using twin roll casting (TRC) process. Herein, a plate with a thickness of 5 mm was manufactured using the TRC process, homogenization heat treatment was performed at 400℃ for 2-32 h, and finally, the change in microstructure was evaluated via optical microscopy and textural analysis. The results suggest that the plate manufactured using the TRC process was not destroyed and was successfully rolled into a plate. Microscopic observation suggested that the dendritic cast structure was arranged along the rolling direction. And the central layer of the rolled plate, where was present in a liquid state at the beginning of rolling, solidified later during the TRC process to form central segregation. The initial cast structure and inhomogeneous structure of the plate were recrystallized by homogenization heat treatment for only 2 h, and it was confirmed that the segregated part of the central layer became homogeneous and recrystallization occurred. Grain growth occurred as the heat treatment time increased, and secondary recrystallization occurred, wherein only some grains were grown. The textural analysis, which was conducted via X-ray diffraction, confirmed that the relatively weak basal plane texture developed using the TRC process was formed into a random texture after heat treatment.

Li3PO4 Coated Li[Ni0.75Co0.1Mn0.15]O2 Cathode for All-Solid-State Batteries Based on Sulfide Electrolyte

  • Lee, Joo Young;Park, Yong Joon
    • Journal of Electrochemical Science and Technology
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    • 제13권3호
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    • pp.407-415
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    • 2022
  • Surface coating of cathodes is an essential process for all-solid-state batteries (ASSBs) based on sulfide electrolytes as it efficiently suppresses interfacial reactions between oxide cathodes and sulfide electrolytes. Based on computational calculations, Li3PO4 has been suggested as a promising coating material because of its higher stability with sulfides and its optimal ionic conductivity. However, it has hardly been applied to the coating of ASSBs due to the absence of a suitable coating process, including the selection of source material that is compatible with ASSBs. In this study, polyphosphoric acid (PPA) and (NH4)2HPO4 were used as source materials for preparing a Li3PO4 coating for ASSBs, and the properties of the coating layer and coated cathodes were compared. The Li3PO4 layer fabricated using the (NH4)2HPO4 source was rough and inhomogeneous, which is not suitable for the protection of the cathodes. Moreover, the water-based coating solution with the (NH4)2HPO4 source can deteriorate the electrochemical performance of high-Ni cathodes that are vulnerable to water. In contrast, when an alcohol-based solvent was used, the PPA source enabled the formation of a thin and homogeneous coating layer on the cathode surface. As a consequence, the ASSBs containing the Li3PO4-coated cathode prepared by the PPA source exhibited significantly enhanced discharge and rate capabilities compared to ASSBs containing a pristine cathode or Li3PO4-coated cathode prepared by the (NH4)2HPO4 source.

On the wave dispersion and vibration characteristics of FG plates resting on elastic Kerr foundations via HSDT

  • Bennai, Riadh;Fourn, Hocine;Nebab, Mokhtar;Atmane, Redhwane Ait;Mellal, Fatma;Atmane, Hassen Ait;Benadouda, Mourad;Touns, Abdelouahed
    • Advances in concrete construction
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    • 제14권3호
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    • pp.169-183
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    • 2022
  • In this article, vibrational behavior and wave propagation characteristics in (FG) functionally graded plates resting on Kerr foundation with three parameters is studied using a 2D dimensional (HSDT) higher shear deformation theory. The new 2D higher shear deformation theory has only four variables in field's displacement, which means has few numbers of unknowns compared with others theories. The shape function used in this theory satisfies the nullity conditions of the shear stresses on the two surfaces of the FG plate without using shear correction factors. The FG plates are considered to rest on the Kerr layer, which is interconnected with a Pasternak-Kerr shear layer. The FG plate is materially inhomogeneous. The material properties are supposed to vary smoothly according to the thickness of the plate by a Voigt's power mixing law of the volume fraction. The equations of motion due to the dynamics of the plate resting on a three-parameter foundation are derived using the principle of minimization of energies; which are then solved analytically by the Navier technique to find the vibratory characteristics of a simply supported plate, and the wave propagation results are derived by using the dispersion relations. Perceivable numerical results are fulfilled to evaluate the vibratory and the wave propagation characteristics in functionally graded plates and some parameters such wave number, thickness ratio, power index and foundation parameters are discussed in detail.

Theoretical buckling analysis of inhomogeneous plates under various thermal gradients and boundary conditions

  • Laid Lekouara;Belgacem Mamen;Abdelhakim Bouhadra;Abderahmane Menasria;Kouider Halim Benrahou;Abdelouahed Tounsi;Mohammed A. Al-Osta
    • Structural Engineering and Mechanics
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    • 제86권4호
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    • pp.443-459
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    • 2023
  • This study investigates the theoretical thermal buckling analyses of thick porous rectangular functionally graded (FG) plates with different geometrical boundary conditions resting on a Winkler-Pasternak elastic foundation using a new higher-order shear deformation theory (HSDT). This new theory has only four unknowns and involves indeterminate integral variables in which no shear correction factor is required. The variation of material properties across the plate's thickness is considered continuous and varied following a simple power law as a function of volume fractions of the constituents. The effect of porosity with two different types of distribution is also included. The current formulation considers the Von Karman nonlinearity, and the stability equations are developed using the virtual works principle. The thermal gradients are involved and assumed to change across the FG plate's thickness according to nonlinear, linear, and uniform distributions. The accuracy of the newly proposed theory has been validated by comparing the present results with the results obtained from the previously published theories. The effects of porosity, boundary conditions, foundation parameters, power index, plate aspect ratio, and side-to-thickness ratio on the critical buckling temperature are studied and discussed in detail.

탄소성유강화플라스틱으로 만들어진 소형 인장 시험편에서 여러 종류의 심재에 따른 파손 연구 (Fracture Study due to Various Core at Compact Tension Specimen Made of Carbon Fiber Reinforced Plastic)

  • 김재원;조재웅
    • 예술인문사회 융합 멀티미디어 논문지
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    • 제8권3호
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    • pp.589-596
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    • 2018
  • 현대 사회에서 의식주 중에서 구조물이나 운송수단은 중요한 역할을 가진다. 만약 구조물이나 운송수단에 작은 크랙이라도 생기고 크랙이 진전되면 그 부품들이 파괴되어 큰 사고를 야기할 수 있다. 이러한 상황을 방지하기 위한 본 연구에서는 크랙의 진전에 따른 파손 경향을 조사하기 위하여 시험편을 이용하였다. CT 시험편의 재질로는 요즘 각광받는 복합재료인 단방향 탄소섬유 강화플라스틱을 사용하였다. 시험편 모델은 단방향성 섬유로서 적층각도를 주었고 적층각도는 [60/-60/60/-60]순으로 지정하였다. 해석 조건으로는 하단부의 홀을 고정시킨후 상단부 홀을 15mm의 강제 변위를 가하였다. 본 연구 결과로는 구조용 강, 구리, 티타늄, 알루미늄 순으로 등가응력과 전단응력이 높게 나왔다. 이러한 결과는 이종재료로 만들어진 CT 시험편의 파손을 검증하는 데 유용하게 사용될 수 있다고 사료된다.

섬유강화 플라스틱 복합재료의 압축성형에서 리브 성형품의 휨에 미치는 성형조건의 영향 (Effects of Molding Conditions on the Deflection of Rib Moldings of Fiber-reinforced Plastic Composites in Compression Molding)

  • 김진우;이정훈;이동기
    • 공학기술논문지
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    • 제10권3호
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    • pp.285-290
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    • 2017
  • Molding of body with ribs is the most difficult during flow molding process. The rib area is easy to be deformed at the rear side due to wall thickness variation. In this study, relationships between molding condition and deflection of rib-shaped part is investigated during the compression molding of fiber reinforced plastic composites, and the following results are derived. Polypropylene(PP), Polystyrene(PS), and stampable sheet(SS 40wt%) show the increment of deflection along with releasing temperature. For the correlation between incremental holding pressure load and deflection, stampable sheet exhibits lower deflection along with higher holding pressure, while PS shows significant increase of deflection with higher holding pressure, PP shows completely different characteristic, significant reduction of deflection along with higher holding pressure. Regarding to mold temperature and deflection, deflection amount of SS is the biggest, and PS shows the smallest. In addition, all three kinds shows the highest amount of deflection at 173C. Deflection is reduced when mold closing speed is increased. Amount of deflection in SS is larger and is not highly dependent on molding conditions like holding pressure and cooling parameters, compared with single component material like PP. This can be elucidated by anisotropic and inhomogeneous characteristics of glass fiber during filling process of stampable sheet composite.