• 제목/요약/키워드: In-situ characterization

검색결과 252건 처리시간 0.031초

침전법과 착체중합법을 이용한 Ga2O3 분말의 합성 및 결정구조 분석 (Synthesis and Crystal Structure Characterization of Ga2O3 Powder by Precipitation and Polymerized Complex Methods)

  • 정종열;김상훈;강은태;한규성;김진호;황광택;조우석
    • 한국세라믹학회지
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    • 제51권3호
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    • pp.156-161
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    • 2014
  • Gallium oxide ($Ga_2O_3$) powders were synthesized using a precipitation method and a polymerized complex method. TG-DSC, SEM, and XRD were performed to investigate the phase and morphology of the $Ga_2O_3$. In situ high-temperature XRD analysis revealed the crystal structure of $Ga_2O_3$ at different temperatures. The $Ga_2O_3$ obtained using the precipitation method and polymerized complex method were generally spherical-shaped particles and their average particle size was approximately 80 nm and $1{\mu}m$, respectively. The crystal structure of the $Ga_2O_3$ prepared by the precipitation method was changed from rhombohedral to monoclinic at $700^{\circ}C$, while monoclinic $Ga_2O_3$ was obtained directly from the precursor by the polymerized complex method.

Growth and characterization of periodically polarity-inverted ZnO structures grown on Cr-compound buffer layers

  • Park, J.S.;Goto, T.;Hong, S.K.;Chang, J.H.;Yoon, E.;Yao, T.
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2010년도 제39회 하계학술대회 초록집
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    • pp.259-259
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    • 2010
  • Periodically polarity inverted (PPI) ZnO structures on (0001) Al2O3 substrates are demonstrated by plasmas assisted molecular beam epitaxy. The patterning and re-growth methods are used to realize the PPI ZnO by employing the polarity controlling method. For the in-situ polarity controlling of ZnO films, Cr-compound buffer layers are used.[1, 2] The region with the CrN intermediate layer and the region with the Cr2O3 and Al2O3 substrate were used to grow the Zn- and O-polar ZnO films, respectively. The growth behaviors with anisotropic properties of PPI ZnO heterostructures are investigated. The periodical polarity inversion is evaluated by contrast images of piezo-response microscopy. Structural and optical interface properties of PPI ZnO are investigated by the transmission electron microcopy (TEM) and micro photoluminescence ($\mu$-PL). The inversion domain boundaries (IDBs) between the Zn and the O-polar ZnO regions were clearly observed by TEM. Moreover, the investigation of spatially resolved local photoluminescence characteristics of PPI ZnO revealed stronger excitonic emission at the interfacial region with the IDBs compared to the Zn-polar or the O-polar ZnO region. The possible mechanisms will be discussed with the consideration of the atomic configuration, carrier life time, and geometrical effects. The successful realization of PPI structures with nanometer scale period indicates the possibility for the application to the photonic band-gap structures or waveguide fabrication. The details of application and results will be discussed.

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TPM-BiP 청색 형광 재료의 전계발광특성 (Characterization of Blue Organic Light Emitting Diodes using TPM-BiP)

  • 장지근;신상배;안종명;장호정;이학민;공명선;김민영;김준우
    • 반도체디스플레이기술학회지
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    • 제6권2호
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    • pp.11-14
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    • 2007
  • For the fabrication of blue color organic light emitting diodes(OLED) with a high performance, 2-TNATA [4,4',4"-tris (2-naphthylphenyl-phenylamino)-triphenylamine] as hole injection material and NPB [N,N'-bis (1-naphthyl) -N,N'-diphenyl-1,1'-biphenyl-4,4'-diamine] as hole transport material were deposited on the ITO (indium tin oxide)/glass substrate by the vacuum thermal evaporation. After then, blue color emission layer was deposited using TPM-BiP[(4'-Benzoylferphenyl-4-yl)phenyl-methanone-Diethyl(biphenyl-4-ymethyl)phosphonate] and GDI602 as a light emitting organic material. Finally, the two kinds of OLEDs with the structure of $ITO/2-TNATA/NPB/TPM-BiP/Alq_3/LiF/Al and ITO/2-TNATA/NPB/GDI602/Alq_3/LiF/Al$ were prepared by in-situ deposition. The maximum current density and luminance were found to be about $588\;mA/cm^2\;and\;5239\;cd/m^2$ at 12V for the OLED sample with the structure of $ITO/2-TNATA/NPB/TPM-BiP/Alq_3/LiF/Al$. Color coordinate of blue OLED was x=0.18, y=0.18 (at llV) and the maximum current efficiency was 2.82 cd/A (at 6V) with the peak emission wavelength of 440 nm.

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Molecular characterization and expression pattern of a novel Keratin-associated protein 11.1 gene in the Liaoning cashmere goat (Capra hircus)

  • Jin, Mei;Cao, Qian;Wang, Ruilong;Piao, Jun;Zhao, Fengqin;Piao, Jing'ai
    • Asian-Australasian Journal of Animal Sciences
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    • 제30권3호
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    • pp.328-337
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    • 2017
  • Objective: An experiment was conducted to determine the relationship between the KAP11.1 and the regulation wool fineness. Methods: In previous work, we constructed a skin cDNA library and isolated a full-length cDNA clone termed KAP11.1. On this basis, we conducted a series of bioinformatics analysis. Tissue distribution of KAP11.1 mRNA was performed using semi-quantitative reverse transcription polymerase chain reaction (RT-PCR) analysis. The expression of KAP11.1 mRNA in primary and secondary hair follicles was performed using real-time PCR (real-time polymerase chain reaction) analysis. The expression location of KAP11.1 mRNA in primary and secondary hair follicles was performed using in situ hybridization. Results: Bioinformatics analysis showed that KAP11.1 gene encodes a putative 158 amino acid protein that exhibited a high content of cysteine, serine, threonine, and valine and has a pubertal mammary gland) structural domain. Secondary structure prediction revealed a high proportion of random coils (76.73%). Semi-quantitative RT-PCR showed that KAP11.1 gene was expressed in heart, skin, and liver, but not expressed in spleen, lung and kidney. Real time PCR results showed that the expression of KAP11.1 has a higher expression in catagen than in anagen in the primary hair follicles. However, in the secondary hair follicles, KAP11.1 has a significantly higher expression in anagen than in catagen. Moreover, KAP11.1 gene has a strong expression in inner root sheath, hair matrix, and a lower expression in hair bulb. Conclusion: We conclude that KAP11.1 gene may play an important role in regulating the fiber diameter.

Genomic DNA Chip: Genome-wide profiling in Cancer

  • 이종호
    • 한국생물정보학회:학술대회논문집
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    • 한국생물정보시스템생물학회 2001년도 제2회 생물정보 워크샵 (DNA Chip Bioinformatics)
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    • pp.61-86
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    • 2001
  • All cancers are caused by abnormalities in DNA sequence. Throughout life, the DNA in human cells is exposed to mutagens and suffers mistakes in replication, resulting in progressive, subtle changes in the DNA sequence in each cell. Since the development of conventional and molecular cytogenetic methods to the analysis of chromosomal aberrations in cancers, more than 1,800 recurring chromosomal breakpoints have been identified. These breakpoints and regions of nonrandom copy number changes typically point to the location of genes involved in cancer initiation and progression. With the introduction of molecular cytogenetic methodologies based on fluorescence in situ hybridization (FISH), namely, comparative genomic hybridization (CGH) and multicolor FISH (m-FISH) in carcinomas become susceptible to analysis. Conventional CGH has been widely applied for the detection of genomic imbalances in tumor cells, and used normal metaphase chromosomes as targets for the mapping of copy number changes. However, this limits the mapping of such imbalances to the resolution limit of metaphase chromosomes (usually 10 to 20 Mb). Efforts to increase this resolution have led to the "new"concept of genomic DNA chip (1 to 2 Mb), whereby the chromosomal target is replaced with cloned DNA immobilized on such as glass slides. The resulting resolution then depends on the size of the immobilized DNA fragments. We have completed the first draft of its Korean Genome Project. The project proceeded by end sequencing inserts from a library of 96,768 bacterial artificial chromosomes (BACs) containing genomic DNA fragments from Korean ethnicity. The sequenced BAC ends were then compared to the Human Genome Project′s publicly available sequence database and aligned according to known cancer gene sequences. These BAC clones were biotinylated by nick translation, hybridized to cytogenetic preparations of metaphase cells, and detected with fluorescein-conjugated avidin. Only locations of unique or low-copy Portions of the clone are identified, because high-copy interspersed repetitive sequences in the probe were suppressed by the addition of unlabelled Cotl DNA. Banding patterns were produced using DAPI. By this means, every BAC fragment has been matched to its appropriate chromosomal location. We have placed 86 (156 BAC clones) cytogenetically defined landmarks to help with the characterization of known cancer genes. Microarray techniques would be applied in CGH by replacement of metaphase chromosome to arrayed BAC confirming in oncogene and tumor suppressor gene: and an array BAC clones from the collection is used to perform a genome-wide scan for segmental aneuploidy by array-CGH. Therefore, the genomic DNA chip (arrayed BAC) will be undoubtedly provide accurate diagnosis of deletions, duplication, insertions and rearrangements of genomic material related to various human phenotypes, including neoplasias. And our tumor markers based on genetic abnormalities of cancer would be identified and contribute to the screening of the stage of cancers and/or hereditary diseases

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풍촌층 고품위 석회석 광상 탐사를 위한 암석 물성 특성 (Characterization of Physical Properties for Mineral Exploration of High-grade Limestone in Pungchon Formation)

  • 신승욱;박삼규;조성준
    • 지구물리와물리탐사
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    • 제20권3호
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    • pp.137-145
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    • 2017
  • 다양한 화학산업에서 사용되는 고품위 석회석은 국내 태백산 분지 일대 상부 풍촌층에 분포하고 있다. 물리탐사는 광범위한 지표면 아래의 지질구조를 조사하는데 가장 효율적인 방법이다. 고품위 석회석 조사와 관련된 물리탐사 연구사례가 거의 선행되지 않았으므로 석회석 조사에 적절한 탐사전략이 아직 마련되지 않았다. 따라서 이 연구에서 암상별 물성연구를 바탕으로 최적의 고품위 석회석 탐사방법을 제안하고, 탐사결과 해석에서 필요한 데이터베이스를 축적하는데 초점을 두었다. 연구를 위한 암석시료는 정선 일대 하부 화절층, 풍촌층, 암맥류를 대상으로 현장 시추 코어에서 채취했고, 실내 물성 측정과 암석 기재를 수행했다. 풍촌층 암석의 대자율은 하부 화절층과 암맥보다 확연히 낮으므로 이러한 암상 경계는 자력 탐사로 구분할 수 있을 것으로 보인다. 또한, 중부 풍촌층 암석의 전기적 물성, 특히 충전성은 상부/하부 풍촌층과 비교하면 차이가 나므로 상부 풍촌층의 고품위 석회석은 유도분극 탐사로 찾을 수 있을 것으로 판단했다.

국내 내륙의 설계 지반 운동 결정을 위한 지반 증폭 계수 및 지반 분류 체계 제안 (A Proposition of Site Coefficients and Site Classification System for Design Ground Motions at Inland of the Korean Peninsula)

  • 선창국;정충기;김동수
    • 한국지반공학회논문집
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    • 제21권6호
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    • pp.101-115
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    • 2005
  • 국내 내륙의 지형 및 지질 특성을 대표하는 두 지역인 경주와 홍성을 대상으로 전단파 속도$(V_s)$ 획득 목적의 현장 탄성파 시험을 포함한 다양한 지반 조사를 실시하여 지반 특성을 평가하고, 이를 토대로 등가 선형 및 비선형 기법의 부지 응답 해석을 수행하였다. 현행 국내 내진 설계의 근간인 미국 서부 지역과의 지반 특성 비교 결왔 국내 내륙 지역의 기반암 심도는 매우 얕고 강성은 다소 컸다. 지반 분류 기준인 심도 30m까지의 평균 전단파 속도$V_s30$는 대상 지역 내에서 $250\sim650m/s$의 좁은 범위의 분포를 보였고, 그에 따라 대부분의 부지가 C와 D 지반 조건으로 분류되었다. 부지 응답 해석 결과로부터 현행 국내 내진 설계를 위한 단주기 증폭 계수$(F_ㅁ)$는 지반 운동을 과소평가하고 중장주기 증폭계수$(F_v)$는 과대평가하고 있음을 확인하였다. 이에 따라 국내 내륙 지역에 대한 지반 증폭 계수를 재산정하고, 지역적 지반 특성을 고려하여 기존 지반 분류 C 및 D의 세부 분류와 지표면 부근 심도까지의 평균 $V_s$$V_s20,\;V_s15,$$V_s10$의 추가 분류 기준이 적용된 합리적 지반 분류 체계를 제안하였다. 제안된 지반 분류 체계는 현재로서는 예비적인 방안이므로 향후 보완 및 개선이 필요할 것으로 판단된다.

실내모형실험에 의한 핵석 풍화대 지반 특성 산정 (Characterization of Weathered Zone bearing Corestones through Scale Model Test)

  • 우익
    • 지질공학
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    • 제17권3호
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    • pp.435-443
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    • 2007
  • 본 연구에서는 풍화대에 분포하고 있는 핵석지반에 대한 지질공학적 조사와 실내모형실험을 통하여 핵석지반의 공학적 물성을 산정하였다. 핵석이 노출된 세 곳의 산사면에 대한 조사창 조사와 시추공 코어 관찰로 핵석의 분포도와 기하학적 모양을 분석하였다. 현장 핵석분포 및 크기에 대한 조사 자료와 모형실험용 공시체 시편의 크기를 바탕으로 산정된 축소율을 고려하여 5mm이하-평균 2mm의 분쇄-연마된 핵석시료를 실내핵석 실험용으로 사용하였다. 핵석 체적함유비를 0%, 10%, 20%로 달리하면서 토양 직접전단시험 및 석고모형실험을 실시하였고, 이를 통하여 핵석지반의 특성을 구하고자 하였다. 핵석함유 토양의 직접전단실험에서는 핵석 함유량의 증가로 인하여 전단강도가 증가하는 경향을 보여주었다. 핵석함유비가 20%일 경우는 핵석 입자의 맞물림에 의한 점착력의 증가가 마찰각의 변화보다 더욱 전단강도의 상승을 유발시키는 요소로 작용하였다. 핵석 함유비를 달리한 석고모형실험에서는 핵석이 많아질수록 모형시료의 강도 및 탄성계수가 증가하는 경향을 보여주었다. 석고모형실험에서 얻어진 핵석 함유량에 따른 모형의 물성변화률을 현장에서 측정한 풍화대의 물성과 비교하여, 현장에서 핵석함유에 따른 물성을 예측한 결과, 핵석 함유가 0%에서 10%로 증가하면 15%의 일축압축강도 증가를, 핵석 함유가 20%로 증가되면 30%의 일축압축강도 증가를 유발하는 것으로 예측이 되었다.

Multiple damage detection of maglev rail joints using time-frequency spectrogram and convolutional neural network

  • Wang, Su-Mei;Jiang, Gao-Feng;Ni, Yi-Qing;Lu, Yang;Lin, Guo-Bin;Pan, Hong-Liang;Xu, Jun-Qi;Hao, Shuo
    • Smart Structures and Systems
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    • 제29권4호
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    • pp.625-640
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    • 2022
  • Maglev rail joints are vital components serving as connections between the adjacent F-type rail sections in maglev guideway. Damage to maglev rail joints such as bolt looseness may result in rough suspension gap fluctuation, failure of suspension control, and even sudden clash between the electromagnets and F-type rail. The condition monitoring of maglev rail joints is therefore highly desirable to maintain safe operation of maglev. In this connection, an online damage detection approach based on three-dimensional (3D) convolutional neural network (CNN) and time-frequency characterization is developed for simultaneous detection of multiple damage of maglev rail joints in this paper. The training and testing data used for condition evaluation of maglev rail joints consist of two months of acceleration recordings, which were acquired in-situ from different rail joints by an integrated online monitoring system during a maglev train running on a test line. Short-time Fourier transform (STFT) method is applied to transform the raw monitoring data into time-frequency spectrograms (TFS). Three CNN architectures, i.e., small-sized CNN (S-CNN), middle-sized CNN (M-CNN), and large-sized CNN (L-CNN), are configured for trial calculation and the M-CNN model with excellent prediction accuracy and high computational efficiency is finally optioned for multiple damage detection of maglev rail joints. Results show that the rail joints in three different conditions (bolt-looseness-caused rail step, misalignment-caused lateral dislocation, and normal condition) are successfully identified by the proposed approach, even when using data collected from rail joints from which no data were used in the CNN training. The capability of the proposed method is further examined by using the data collected after the loosed bolts have been replaced. In addition, by comparison with the results of CNN using frequency spectrum and traditional neural network using TFS, the proposed TFS-CNN framework is proven more accurate and robust for multiple damage detection of maglev rail joints.

대규모 노천 석탄광산의 사면 안정화를 위한 지하수 유동 체계 분석 (Field Tests and Analysis of Groundwater System for Stabilization of Slope in Large Open-Pit Coal Mine)

  • 류동우;김형목;오준호;선우춘;정용복
    • 터널과지하공간
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    • 제19권3호
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    • pp.248-260
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    • 2009
  • 직접 개발 형식의 해외자원개발과 관련하여 단순 자본 투자에서 직접 개발로 변화하고 있다. 대규모 노천 석탄광산에서의 사면 안정성과 관련하여 지하수 유동 체계 분석과 사면 보강공으로서의 수평 배수공 타당성을 인도네시아 Pasir 탄광을 대상으로 검토하였다. 본 연구에서는 지하수 체계를 특징짓기 위해 지하수 수위 분석, 현장 투수 시험, 추적자 실험 등 다양한 현장 실험 및 계측을 수행하였다. 특히, 중부 지역의 상부에 위치한 SM강과의 연계성을 분석에 중점을 두었다. Guelph 투수계수를 활용하여 투수계수를 측정하였으며, 사암이 이암이나 탄층보다 투수성이 매우 높은 것으로 나타났다. 지하수 수위 분석 결과 사암층과 협재되어 많은 균열을 포함한 얇은 탄층이 주된 지하수 유동 경로 역할을 히는 것으로 나타났다. 추적자 시험 결과 SM강이 인근 지하수계에 미치는 영향은 강 바닥의 지층구조에 따라 다른 것으로 파악되었다. 수평 배수공의 효과를 파악하기 위한 2차원 지하수 유동 해석 결과는 폭이 좁은 탄층이 협재되어 있는 지층과 사암층이 주된 지하수 유동 경로이며, 충분한 심도로 수평 배수공 시공시 사면 안정화에 효과가 있는 것으로 파악되었다. 따라서 수평 배수공의 시공 위치와 시공 심도의 결정을 위해서는 지층 구조의 파악이 선행되어야 한다.