• 제목/요약/키워드: In-situ characterization

검색결과 252건 처리시간 0.029초

전기폭발법에서 SMPS를 이용한 Cu 나노분말의 실시간 입자특성평가 (In-situ Particle Characterization of Cu Nanopowder using Scanning Mobility Particle Sizer in Pulsed Wire Evaporation Method)

  • 이창우;맹덕영;박중학;유지훈;이재훈;이창규;김흥회
    • 한국분말재료학회지
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    • 제10권4호
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    • pp.275-280
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    • 2003
  • Synthesis and characteristics of Cu nanopowder were considered by in-situ characterization method using SMPS in pulsed wire evaporation process. With increasing pressure in chamber, particle size and degree of agglomeration increased by increase of collision frequency. Also, it was found from the XRD analyses and BET measurements that crystallite size and particle size decreased with elevating applied voltage. However, SMPS measurements and TEM observation revealed the increase of particle size and degree of agglomeration with increase of applied voltage. These results suggested that particle growth and agglomeration depend on overheating factor in chamber at the early stage and thermal coagulation in filtering system during powder formation until collection.

Remedation of petroleum impacted filled land using of various in situ technology

  • 안훈기;김재형;고경연;서형기;임은진
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2004년도 임시총회 및 추계학술발표회
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    • pp.286-289
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    • 2004
  • On site, In situ soil remediation technologies are very important among the remediation technologies and in general efficiency of these technologies are turned to site characterization and environmental condition. specially using of only one technology has so many limitation factors. for example, existing state of tailing and channeling and so on. actually, filled land have high concentration cation exchange capacity because of existence in abundance soil organic matter. Therefore we used various on site in Situ technologies by phase for overcome the limitation factors. Target site is petroleum (diesel) impacted filled land and using technologies are SVE(Soil Vapor Extraction), BV(Bioventing), Bioremediation, Soil flushing, Chemical oxidation.

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표면파 지반 탐사를 위한 새로운 신호 처리기법의 개발 (Development of Data Analysis Method for Surface Wave Test)

  • 박형춘;김동수;조성은
    • 한국지구물리탐사학회:학술대회논문집
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    • 한국지구물리탐사학회 2007년도 공동학술대회 논문집
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    • pp.237-240
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    • 2007
  • The evaluation of shear modulus (or shear wave velocity) profile of site is very important in the various fields of geotechnical engineering. To obtain shear wave velocity profile, various in-situ seismic methods using surface waves have been developed. These surface wave based in-situ seismic methods have their own strength and weakness. In this study, new seismic site characterization method using the harmonic wavelet analysis of wave (HWAW) was proposed to overcome some of weaknesses in the existing surface wave based seismic site characterization methods. HWAW method which is based on time-frequency analysis using harmonic wavelet transform have been developed to determine phase and group velocities of waves. In order to estimate the applicability of HWAW method, field tests were performed. Through field applications and comparison with other test results, the applicability of the proposed method were verified.

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In-situ 중합법에 의한 Polyimide/Carbon Nanotube 복합재료의 제조 및 특성 (Preparation and Characterization of Polyimide/Carbon Nanotube Composites by in-situ Polymerization)

  • Seo, Min-Kang;Park, Soo-Jin
    • 한국섬유공학회:학술대회논문집
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    • 한국섬유공학회 2003년도 가을 학술발표회 논문집
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    • pp.223-224
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    • 2003
  • Polyimides (PI) are widely used in applications ranging from microelectronics to aerospace. Due to their insulating nature, significant accumulation of electrostatic charge may result on their surface, causing local heating and premature degradation to electronic components or space structures. Over the past decade, several publications have been made in fabrication and charaterization of CNT nanocomposites [1,2]. (omitted)

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Application of In Situ Measurement for Site Remediation and Final Status Survey of Decommissioning KRR Site

  • Hong, Sang Bum;Nam, Jong Soo;Choi, Yong Suk;Seo, Bum Kyoung;Moon, Jei Kwon
    • Journal of Radiation Protection and Research
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    • 제41권2호
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    • pp.173-178
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    • 2016
  • Background: In situ gamma spectrometry has been used to measure environmental radiation, assumptions are usually made about the depth distribution of the radionuclides of interest in the soil. The main limitation of in situ gamma spectrometry lies in determining the depth distribution of radionuclides. The objective of this study is to develop a method for subsurface characterization by in situ measurement. Materials and Methods: The peak to valley method based on the ratio of counting rate between the photoelectric peak and Compton region was applied to identify the depth distribution. The peak to valley method could be applied to establish the relation between the spectrally derived coefficients (Q) with relaxation mass per unit area (${\beta}$) for various depth distribution in soil. The in situ measurement results were verified by MCNP simulation and calculated correlation equation. In order to compare the depth distributions and contamination levels in decommissioning KRR site, in situ measurement and sampling results were compared. Results and Discussion: The in situ measurement results and MCNP simulation results show a good correlation for laboratory measurement. The simulation relationship between Q and source burial for the source layers have exponential relationship for a variety depth distributions. We applied the peak to valley method to contaminated decommissioning KRR site to determine a depth distribution and initial activity without sampling. The observed results has a good correlation, relative error between in situ measurement with sampling result is around 7% for depth distribution and 4% for initial activity. Conclusion: In this study, the vertical activity distribution and initial activity of $^{137}Cs$ could be identifying directly through in situ measurement. Therefore, the peak to valley method demonstrated good potential for assessment of the residual radioactivity for site remediation in decommissioning and contaminated site.

Epstein-Barr 바이러스 인사이투 보결합 시행시 양성대조표지로서의 버키트 림프종 세포주 (CCL85 EB-3)의 응용 (Application of Epstein-Barr Virus Cell Lines (CCL85 EB-3) in Performing the EBER mRNA In Situ Hybridization as a Positive Control)

  • 김성숙;한운섭;서주영;허주령
    • 대한세포병리학회지
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    • 제7권1호
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    • pp.38-43
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    • 1996
  • Epstein-Barr virus(EBV) is associated with a wide spectrum of benign and malignant disorders including leukoplakia, Hodgkln's lymphoma, central nervous system lymphoma, peripheral T cell lymphoma and nasopharyngeal undifferentiated carcinoma. There are several distinctive aspects of biology of the virus that are important in investigation of virus in clinical specimens. The abundant expression of the EBER mRNA transcripts makes possible the sensitive detection of latent expression in EBV-associated tumors. Although there has been a dramatic increased interest in the direct characterization of EBV in clinical specimens, there have been few studios about the effective and reliable positive controls in performing in situ hybridization technique for EBV, especially on paraffin-em bedded tissue. We applied Burkitts lymphoma ceil line as positive control in EBV in situ hydridization using Oncor Kit. The cell block of Burkitt lymphoma cell line(CCL85 EB-3) showed strong and specific positivity for EBER in situ in nuclei of EBV infected cells.

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Synchrotron-based Transmission X-ray Microscopy (TXM) Observations of Fully Hydrated Blood Platelets and Their Activation Process

  • Yang, Nuri;Nho, Hyun Woo;Kalegowda, Yogesh;Kim, Jin Bae;Song, Jaewoo;Shin, Hyun-Joon;Yoon, Tae Hyun
    • Bulletin of the Korean Chemical Society
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    • 제35권9호
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    • pp.2625-2629
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    • 2014
  • Platelets are anuclear discoid-shaped blood cells with key roles in human body. To understand the mechanisms of their activation process, it is required to have analytical imaging techniques capable of acquiring platelet images under fully hydrated conditions. Herein, for the first time, we demonstrate the capability of synchrotron-based transmission X-ray microscopy (TXM) to study platelets (resting and ADP activated) under hydrated and air-dried conditions. To confirm the biological imaging capability of TXM, fixed platelets were imaged and compared with whole mount electron microscopy (EM) images. TXM provided morphological information with sufficient spatial resolution with simple and quick sample preparation procedure. We also observed temporal changes during the platelet activation, which initially had a discoid shape (0 s), formed pseudopodia (30 s) and generated a network of fibrin (5 min). Our results clearly demonstrate the potential of TXM technique to study fully hydrated biological samples under in situ conditions.