• 한국지구과학회지
• /
• 제40권6호
• /
• pp.613-623
• /
• 2019

지난 수십년 동안 인공위성을 통해 광범위하고 주기적으로 관측된 해수면온도 자료를 사용하여 일별 해수면온도 합성장이 생산되고 있으며 기후변화 감시와 해양 대기 예측 등 다양한 목적으로 활용되어 왔다. 본 연구에서는 지역적인 해역에서 최적화된 활용을 위해 한반도 주변해역에서 해수면온도 합성장 자료의 정확도 평가와 오차 특성 분석을 수행하였다. 2016년 1월부터 12월까지 이어도 해양과학기지 관측 수온 자료를 활용하여 4종의 다중 인공위성 기반 해수면온도 합성장 자료(OSTIA (Operational Sea Surface Temperature and Sea Ice Analysis), OISST (Optimum Interpolation Sea Surface Temperature), CMC (Canadian Meteorological Centre) 해수면온도 및 MURSST (Multi-scale Ultra-high Resolution Sea Surface Temperature))를 비교하여 각 해수면온도 합성장의 정확도를 평가하였다. 이어도 해양과학기지 수온 자료에 대하여 각 해수면온도 합성장은 최소 0.12℃ (OISST)와 최대 0.55℃ (MURSST)의 편차와 최소 0.77℃ (CMC 해수면온도)와 최대 0.96℃ (MURSST)의 평균 제곱근 오차를 나타냈다. 해수면온도 합성장 사이의 상호 비교 결과에서는 -0.38-0.38℃의 편차와 0.55-0.82℃의 평균 제곱근 오차의 범위를 보였으며 OSTIA와 CMC 해수면온도 자료가 가장 작은 오차 특성을 보인 반면 OISST와 MURSST 자료는 가장 큰 오차 특성을 나타내었다. 이어도 해양과학기지와 가장 가까운 지점에서 해수면온도 합성장 자료를 추출하여 시계열을 비교한 결과에서는 이어도 해양과학기지 관측 수온 뿐만 아니라 모든 해수면온도 합성장 자료에서 뚜렷한 계절 변동을 보였으나 봄철 해수면온도 합성장은 이어도 해양과학기지 관측 수온에 비해 과대추정되는 경향이 나타났다.

• Bulletin of the Korean Chemical Society
• /
• 제31권7호
• /
• pp.1993-1996
• /
• 2010

Silver nanoparticles has been prepared by the $\gamma$-irradiation and in situ reduction methods. Based on the Raman spectra, TEM images, X-ray Diffraction (XRD) patterns and UV-vis spectra, the in situ reduction method is more stable and the average size of the silver nanoparticles is also smaller than by the $\gamma$-irradiation reduction method. It is identified that the silver ions interacting with nonbonding electrons of oxygen atom in the carbonyl group of polyvinylpyrrolidone (PVP) by the in situ reduction method. It is also found advantages of the in situ reduction method including no additional reducing agents, without $\gamma$-irradiations treatment and the room temperature treatment suitability.

• Composites Research
• /
• 제36권5호
• /
• pp.321-328
• /
• 2023

본 연구에서는 다관절 로봇 암을 활용한 열 성형 공정을 통해 열가소성 복합재 부품을 개발하였다. 유한요소해석을 기반으로 로봇 암이 적용된 고속 열 성형 공정의 최적 공정 변수를 도출하였고, 이를 기반으로 실제 제작 공정을 통해 공정 변수를 구체화하였다. 제작된 부품과 유한요소해석 간의 두께 균일성, 주름 분포를 비교하였고, 이를 통해 유한요소해석의 타당성을 입증하였다. 또한, 제작된 복합재 부품의 성형성을 평가하기 위해 결정화도와 기공률을 측정하였고, 그 결과 우수한 성형성을 보인 것으로 평가하였다. 이에 따라 본 연구는 로봇 암기반의 고속 열 성형 공정을 통한 공정 확립과 이를 통한 복합재 구조의 제작 가능성을 확인하였다.

• 한국지반신소재학회논문집
• /
• 제11권1호
• /
• pp.47-56
• /
• 2012

PBD의 통수능력은 지반조건 빛 두께에 비례하여 영향을 크게 받는 성질이 있으며, 배수재 타입 시 시용되는 맨드럴, 타입기기 및 방식에 의한 주변지반의 교란영향으로 배수성능이 저하되는 문제점 등이 있다. 또한, 여러 기지 조건에 따라 통수능의 편차가 크게 나타나며 원지반 조건에 따라 배수재의 통수능 저하, 간극수압소산의 시간지연 등의 분석이 미흡하다. 따리서 본 연구에서는 원지반 조건을 고려한 연직배수재의 복합 통수능 시험을 실시하여 지반개량 및 통수능 평가를 하였다. ${\phi}\;38{\times}70cm$ 크기의 원통형 실린더에 배수재를 고정한 후 교반한 시료를 투기하고 원지반 조건 CL, ML, SM과 준설토 CL을 매립한 후 가입장치를 사용하여 30, 70, 120 kpa의 하중을 가해 단계별로 복합통수능 실험을 수행하였다. 시험결과, 통수능의 크기는 원지반 조건이 SM>ML>CL>CL(준설토)인 순으로, 세립분 함량이 적을수록 통수량은 크게 나타났다.

• Composites Research
• /
• 제12권3호
• /
• pp.36-44
• /
• 1999

In-situ process에 의한 $Al_2O_{3p}/Al$기 복합재료 제조시, Mg의 첨가형태와 함량, 공정온도 및 유지시간이 응용Al의 침투거동과 미세조직 및 경도에 미치는 영향을 조사하였다. Mg분말과 $Al_2O_3$입자의 혼합분말에 순 Al을 침투시켜 복합재를 제조하는 경우, 침투율에 영향을 주는 가장 유력한 변수는 Mg분말의 함량이며, Mg의 활발한 반응으로 $700^{\circ}C$의 낮은 온도에서도 침투가 가능했다. 한편 Al-Mg합금을 $Al_2O_3$입자에 침투시켜 복합재를 제조하는 경우 Mg함량과 공정온도에 관계없이 거의 동일한 침투율을 나타냈으며 침투 가능한 공정온도는 $800^{\circ}C$이었다. Mg과 $Al_2O_3$의 혼합분말로 제조한 복합재가 Al-Mg합금으로 제조한 복합재 보다 월등히 높은 경도를 나타냈으나, 과도한 계면방응에 의한 불균일한 강화상의 분산으로 경도의 산포도는 컸다.

• 대한전기학회논문지:전기물성ㆍ응용부문C
• /
• 제55권11호
• /
• pp.505-513
• /
• 2006

The present study investigated the influence of the content of $Al_2O_3+Y_2O_3$ sintering additives on the microstructure, mechanical and electrical properties of the pressureless-sintered $SiC-ZrB_2$ electroconductive ceramic composites. Phase analysis of composites by XRD revealed mostly of ${\alpha}-SiC(4H),\;ZrB_2,\;{\beta}-SiC(15R)$ and In Situ $YAG(Al_5Y_3O_{12})$. The relative density and the flexural strength showed the highest value of 86.8[%] and 203[Mpa] for $SiC-ZrB_2$ composite with an addition of 8[wt%] $Al_2O_3+Y_2O_3$ as a sintering aid at room temperature respectively. Owing to crack deflection and crack bridging of fracture toughness mechanism, the fracture toughness showed 3.7 and $3.6[MPa{\cdot}m^{1/2}]\;for\;SiC-ZrB_2$ composites with an addition of 8 and 12[wt%] $Al_2O_3+Y_2O_3$ as a sintering aid at room temperature respectively. Abnormal grain growth takes place during phase transformation from ${\beta}-SiC\;into\;{\alpha}-SiC$ was correlated with In Situ YAG phase by reaction between $Al_2O_3\;and\;Y_2O_3$ additives during sintering. The electrical resistivity showed the lowest value of $6.5{\times}10^{-3}[({\Omega}{\cdot}cm]$ for the $SiC-ZrB_2$ composite with an addition of 8[wt%] $Al_2O_3+Y_2O_3$ as a sintering aid at room temperature. The electrical resistivity of the $SiC-ZrB_2$ composites was all positive temperature coefficient(PTCR) in the temperature ranges from $25[^{\circ}C]\;to\;700[^{\circ}C]$. The resistance temperature coefficient showed the highest value of $3.53{\times}10^{-3}/[^{\circ}C]\;for\;SiC-ZrB_2$ composite with an addition of 8[wt%] $Al_2O_3+Y_2O_3$ as a sintering aid in the temperature ranges from $25[^{\circ}C]\;to\;700[^{\circ}C]$. In this paper, it is convinced that ${\beta}-SiC$ based electroconductive ceramic composites for heaters or ignitors can be manufactured by pressureless sintering.

• Nano
• /
• 제13권12호
• /
• pp.1850137.1-1850137.9
• /
• 2018

A series of silica surface-capped with hexamethyldisilazane (denoted as $H-SiO_2$) were prepared by liquid-phase in-situ surface-modification method. The as-obtained $H-SiO_2$ was incorporated into acrylic amino (AA) baking paint to obtain AA/$H-SiO_2$ composite extinction paints and/or coatings. $N_2$ adsorption-desorption tests were conducted to determine the specific surface area as well as pore size and pore volume of $H-SiO_2$. Moreover, the effects of $H-SiO_2$ matting agents on the physical properties of AA paint as well as the gloss and transmittance of AA-based composite extinction coatings were investigated. Results show that $H-SiO_2$ matting agents possess a large specific surface area and pore volume than previously reported silica obtained by liquid-phase method. Besides, they have better dispersibility in AA baking paint than the unmodified silica. Particularly, $H-SiO_2$ with a silica particle size of $6.7{\mu}m$ and the dosage of 4% (mass fraction) provides an extinction rate of 95.2% and a transmittance of 79.3% for the AA-based composite extinction coating, showing advantages over OK520, a conventional silica matting agent. Along with the increase in the silica particle size, $H-SiO_2$ matting agents cause a certain degree of increase in the viscosity of AA paint as well as a noticeable decrease in the gloss of the AA-based composite extinction coating, but they have insignificant effects on the hardness and adhesion to substrate of the AA-based composite coatings. This means that $H-SiO_2$ matting agents could be well applicable to preparing low-viscosity and low-gloss AA-based matte coatings.

• 한국분말야금학회:학술대회논문집
• /
• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
• /
• pp.1294-1295
• /
• 2006

Various reactions and the in-situ formation of new phases can occur during the mechanical alloying process. In the present study, Al powders were strengthened by AlN, using the in-situ processing technique during mechanical alloying. Differential thermal analysis and X-ray diffraction studies were carried out in order to examine the formation behavior of AlN. It was found that the precursors of AlN were formed in the Al powders and transformed to AlN at temperatures above $600^{\circ}C$. The hot extrusion process was utilized to consolidate the composite powders. The microstructure of the extrusions was examined by SEM and TEM. In order to investigate the mechanical properties of the extrusions, compression tests and hardness measurements were carried out. It was found that the mechanical properties and the thermal stability of the Al/AlN composites were significantly greater than those of conventional Al matrix composites.

• Steel and Composite Structures
• /
• 제6권2호
• /
• pp.123-138
• /
• 2006

This paper proposes a model for the analysis of the construction sequences of steel-concrete composite decks in which the slab is cast-in-situ for segments. The model accounts for early age shrinkage, such as thermal and endogenous shrinkage, drying shrinkage, tensile creep effects and the complex sequences of loading due to pouring of the different slab segments. The evolution of the structure is caught by suitably defining the constitutive relationships of the concrete and the steel reinforcements. The numerical solution is obtained by means of a step-by-step procedure and the finite element method. The proposed model is then applied to a composite deck in order to show its potential.

• 한국재료학회:학술대회논문집
• /
• 한국재료학회 2003년도 춘계학술발표강연 및 논문개요집
• /
• pp.137-137
• /
• 2003

Conducting PPy/PVA composite and pure PPy gas sensors were prepared by in-situ vaporstate polymerization method in a vaporization chamber under N2 condition, by exposing the pre-coated electrode with PVA/FeC13 to distilled pyrrole monomer. The various electrical sensing behaviors of both types of sensors were systematically investigated by a flow measuring system including mass flow controller (MFC) and bubbling bottle. The FT-Raman spectroscopy of vapor state polymerized PPy was identical to that of chemically polymerized PPy, confirming the same chemical structure. Both types of sensors had positive sensitivity when exposed to methanol gas. The sensitivity varied linearly with gas concentration in the range of 50ppm to 1059ppm. The detection limit of PPy/PVA sensor was believed to be as low as 10ppm. The sensitivity of PPy/PVA composite sensor was higher than that of pure PPy sensor. Both the response time and recovery time of PPy/PVA composite sensors were longer than those of pure PPy sensors. The thickness of the sensing film affected the sensitivity this way that the sensor having thinner film had higher sensitivity, indicating that the resistance of polymer film involved in the sensing behavior was bulk resistance rather than surface resistance. The reproducibility of PPy/PVA composite sensor was excellent during eight on-off cycles by switching between N2 and 3000ppm methanol gas. The sensitivity of PPy/PVA composite sensor was only maintained for two weeks, while the sensitivity of pure PPy sensor was maintained over two months.