• 제목/요약/키워드: Impedance Analyzer

검색결과 229건 처리시간 0.028초

고온 PEFCs를 위한 탄화수소계열 고분자와 이온성 액체를 함유하는 복합막에 관한 연구 (A study on composite membranes based on hydrocarbon polymers and ionic liquids for high temperature PEFCs)

  • 백지숙;박진수;김경현;문기영;김혜경;최영우;박구곤;양태현;김창수;설용건
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 추계학술대회 논문집
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    • pp.147-148
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    • 2009
  • The water-like ionic liquids have been widely used to enable the proton conduction in ionic liquid based membranes at high temperature and anhydrous PEFCs. In this study, we synthesized various kinds of composite membranes based on hydrocarbon polymers having good thermal and mechanical stabilities at high temperatures and ionic liquids. The composite membrane consisting of hydrocarbon polymer and ionic liquid was characterized by thermogravimetric analyzer (TGA) and impedance spectroscopy. Consequently the non-aqueous composite membranes of a variety of hydrocarbon polymer and ionic liquids have good conductivity and thermal stability at high temperature conditions.

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일개 대학생의 건강증진 생활양식과 신체조성간의 관계 연구 (The Correlational Study of Health Promotion Lifestyle and Body Composition in a University Students)

  • 박연숙;이혜경
    • 한국학교보건학회지
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    • 제19권1호
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    • pp.67-78
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    • 2006
  • Purporse : The purpose of this study was to examine the relationship between a health promoting lifestyle and body composition in university students. The study subjects were 194 university students who attended K-university located in Chungnam. Methods : The data was collected between March 2 and May 31, 2004. The instrument used for this study was the modified Health Promoting Lifestyle Profile(HPLP) developed by Walker, Sechrist, & Pender(1987). The body composition was measured by In Body 3.0, a Bioelectrical Impedance Analyzer. The data was analyzed using the SPSS/WIN 10.0 program by t-test, ANOVA and pearson correlation coefficients. Results : The results of this study are as follows: 1) The scores of the Health Promoting Lifestyle(HPL) ranged from 79 to 170, with a mean score of 110(±15.8). The mean scores of sub-categorical HPL were self-actualization 31.8(±4.9), health responsibility 17.0(±4.0), exercise 8.3(±3.2), nutrition 15.4(±3.7), interpersonal relationships 20.3(±3.5) and stress management 17.2(±3.4). 2) The HPL according to the subjects' general characteristics had significant correlation to exercise amount(F=8.09, p<.01), drinking amount(F=6.56, p<.01), perceived health status(F=19.2, p<.01) and perceived health knowledge (F=15.9, p<.01). 3) The total HPL did not significantly correlate with any categories in body composition. The exercise area of sub-categorical HPL had significant positive correlation to height (r=.199, p<.01), weight(r=.181, p<.05) and soft lean mass(r=.257, p<.01), and negative correlation to percent body fat(r=-.255, p<.01) in body composition. Conclusion : The results suggest that the exercise area of sub-categorical HPL was an important variable for an exercise program's development such as nursing intervention for the health promotion of university students.

Fabrication of PZT Film by a Single-Step Spin Coating Process

  • Oh, Seung-Min;Kang, Min-Gyu;Do, Young-Ho;Kang, Chong-Yun;Nahm, Sahn;Yoon, Seok-Jin
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2011년도 제40회 동계학술대회 초록집
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    • pp.193-193
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    • 2011
  • To obtain ceramic films, the sol-gel coating technique has been broadly used with heat treatment, but crack formation tend to occur during heat treatment in thick sol-gel films. We prepared PZT thin films by sol-gel method with single-step spin coating process. The PZT solution have been synthesized using lead acetate ($Pb(CH_3COO)_2$), zirconium acetylacetonate ($Zr(OC_3H_7^n)_4$), and titanium diisopropoxide bis(acetylacetonate) 75wt% in isopropanol ($Ti(OC_3H_7^i)_2(OC_3H_7^n)_2$) as starting materials and n-propanol was selected as a solvent. The poly(vynilpyrrolidone) (PVP) was added with 0, 0.25, 0.5, 0.75, and 1 molar ratios to control viscosity of solution. We investigated influence of the viscosity on thickness, microstructure, and electrical properties of final PZT films. Thermo-gravimetric analysis and differential scanning calorimeter (TGA/DSC) was carried out from room temperature to $800^{\circ}C$ in order to measure pyrolysis temperature. Structural characteristics were analyzed by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Ferroelectric and dielectric properties were measured by RT66A (Radiant) and impedance analyzer (Agilent), respectively. The thicknesses of PZT films depended on incorporation of an excess amount of PVP. Finally, we obtained PZT films of good quality without crack formation via single-step spin coating.

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Dietary Intake Differences among Korean Male Smokers, Ex-smokers and Non-smokers

  • Kim, Jean-Chinock -Rim;Kim, Seonwoo;Lee, Soon-Young
    • Journal of Community Nutrition
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    • 제1권2호
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    • pp.125-132
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    • 1999
  • This study investigated the differences in dietary intake, age, body mass index(BMI), marital status and education of 1,585 Korean healthy males among current smokers, ex-smokers and non-smokers. Dietary intake was determined by a food frequency questionnaire at the Samsung Medical Center in Seoul, Korea. A bioelectric impedance analyzer measured height, body weight and BMI. This study identified 50% of the study group as current smokers and 30% as ex-smokers and 20% as non-smokers. The mean body mass index was 23.7kg/㎡ and did not differ significantly among the three groups. THe current smokers were younger(44.9 years old) and contained a lower percentage(58.5%) of college graduate than that of ex-smokers or non-smokers. The percentage of non-consumers of meat, eggs, beans and bean products was higher in non-smokers than that of ex-smokers or current smokers. Smoking was to a significant degree positively related to the amount of coffee and alcoholic beverages consumed and negatively related to the amount of milk and milk products and fruits consumed. The intake of eggs, milk and milk products, fruit, coffee, sweets, fats and oils were significantly different among the three groups. after adjusting for age, education level, marital status, and alcohol consumption. There was a strong positive relationship between smoking intensity and the intake of coffee and alcoholic beverages(p<0.0005), and an inverse relationship between smoking intensity and fruit, milk and milk product intake(p<0.005). The current smokers were characterized by a higher intake of total energy and cholesterol, and a lower intake of dietary fibers, ${\beta}$-carotine and folate than those of non-smokers or ex-smokers. The nutrient intake of ex-smokers was moderate and highest in ${\beta}$-carotine and folate, which suggested that ex-smokers were trying to change their life style.

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저합금강의 부식속도에 미치는 시편 면적의 영향 (Effect of Specimen Area on the Corrosion Rate of Low Alloy Steel)

  • 김민준;장영욱;유윤하;김종집;김정구
    • 전기화학회지
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    • 제13권2호
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    • pp.96-102
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    • 2010
  • 본 연구에서는 균일부식이 발생하는 저합금강의 노출면적에 따른 부식속도의 변화를 관찰하고 이에 대한 원인을 규명하고자 하였다. 다양한 표면적을 지닌 동일한 저합금강 시편의 부식속도를 전기 화학적 임피던스 분광법, 직선분극저항 측정법, 동전위 분극 시험법을 이용하여 산출하였다. 또한 전자주사현미경, X선 광전자 분광법 및 X선 전자탐침 미량분석을 이용하여 표면분석을 실시하였다. 전기화학적 시험 결과 모든 시험법에서 시편의 크기가 증가할수록 부식속도가 높게 산출되었으며, 표면분석을 통해 망간과 황으로 구성된 화합물이 존재하는 영역에서 우선적으로 부식이 발생하며, 이 화합물과 철 또는 구리 산화물이 소양극-대음극의 미세 갈바닉 셀을 구성함을 확인하였다. 이러한 효과는 시편 크기에 비례하여 증가하였으며, 국부적인 부식이 우선적으로 발생한 후, 부식생성물이 표면을 덮게 되어 점차 균일부식의 형태로 전환하게 된다.

고효율 압전 트랜스포머용 PSN-PMN-PZT 조성 설계 (Energy Efficient Alloy Design in PSN-PMN-PZT Ceramic System for Piezoelectric Transformer Application)

  • 최용길;어순철;윤만순
    • 한국재료학회지
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    • 제15권12호
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    • pp.814-817
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    • 2005
  • In order to enhance energy efficiency in high electric conversion devices such as Power transformers, which need to have high power properties, an alloy design approach in $Pb(Zr,Ti)O_3(PZT)$ base ceramic system was attempted $0.03Pb(Sb_{0.5}Nb_{0.5})O_3-0.03Pb(Mn_{1/3}Nb_{2/3})O_3-(0.94-x)PbTiO_3-xPbZrO_3$[PSN-PMN- PZT] ceramics were synthesized by conventional bulk ceramic processing technique. To improve power properties, the various Zr/Ti ratio was varied ]lear their morphotropic phase boundary (MPB) composition of PSN-PMN-PZT system and their effects on subsequent piezoelectric and dielectric properties for the transformer application at high power were systematically investigated using an impedance analyzer. Microstructure and phase information were characterized using X-ray diffractometer (XRD), a scanning electron microscope (SEM) and others. When the Zr/Ti ratio was 0.415/0.465, the value of $Q_m\;and\;k_p$ were shown to reach to the maximum, indicating that this alloy design can be a feasible composition :or high power transformer.

후면 그라운드를 이용한 휴대단말 Wi-Fi 칩 안테나 설계 (Design of Mobile Handset Chip Antenna with a Backside Ground for Wi-Fi Application)

  • 오세원;김형동
    • 한국전자파학회논문지
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    • 제23권5호
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    • pp.592-597
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    • 2012
  • 본 논문에서는 휴대단말기의 Wi-Fi 대역에서 동작하는 소형 칩 안테나를 설계하였다. 제안된 안테나의 소형화를 위해 칩 안테나 하단에 후면 그라운드를 갖도록 설계하였다. 제안된 안테나는 S자 모양 대칭형으로 유전율이 3.5인 LCP(Liquid Crystal Polymer) 위에 설계되었으며, 칩 안테나의 전체 크기는 $6.0mm{\times}2.5mm{\times}1.2mm$를 갖는다. 제작된 안테나는 VSWR=3 이하 기준 300 MHz(fractional bandwidth: 12.2 %, 2.3~2.6 GHz)의 임피던스 대역폭과 peak gain은 1.42 dBi의 특성을 나타냈다. 안테나 설계는 CST Microwave Studio 상용 프로그램을 사용하여 최적화한 후, 설계된 안테나를 제작하고, 네트워크 분석기와 무반향실을 이용하여 측정하였다.

임베디드 커패시터의 응용을 위해 CCL 기판 위에 평가된 BMN 박막의 특성 (The Properties of $Bi_2Mg_{2/3}Nb_{4/3}O_7$ Thin Films Deposited on Copper Clad Laminates For Embedded Capacitor)

  • 김혜원;안준구;안경찬;윤순길
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.45-45
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    • 2007
  • Capacitors among the embedded passive components are most widely studied because they are the major components in terms of size and number and hard to embed compared with resistors and inductors due to the more complicated structure. To fabricate a capacitor-embedded PCB for in-line process, it is essential to adopt a low temperature process (<$200^{\circ}C$). However, high dielectric materials such as ferroelectrics show a low permittivity and a high dielectric loss when they are processed at low temperatures. To solve these contradicting problems, we studied BMN materials as a candidate for dielectric capacitors. processed at PCB-compatible temperatures. The morphologies of BMN thin films were investigated by AFM and SEM equipment. The electric properties (C-F, I-V) of Pt/BMN/Cu/polymer were evaluated using an impedance analysis (HP 4194A) and semiconductor parameter analyzer (HP4156A). $Bi_2Mg_{2/3}Nb_{4/3}O_7$(BMN) thin films deposited on copper clad laminate substrates by sputtering system as a function of Ar/$O_2$ flow rate at room temperature showed smooth surface morphologies having root mean square roughness of approximately 5.0 nm. 200-nm-thick films deposited at RT exhibit a dielectric constant of 40, a capacitance density of approximately $150\;nF/cm^2$, and breakdown voltage above 6 V. The crystallinity of the BMN thin films was studied by TEM and XRD. BMN thin film capacitors are expected to be promising candidates as embedded capacitors for printed circuit board (PCB).

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(1-x)$(Na_{0.5}K_{0.5})NbO_3-xLiNbO_3$ 무연 압전세라믹스의 첨가물질에 따른 전기적 특성 평가

  • 우덕현;류성림;윤만순;권순용
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 추계학술대회 논문집
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    • pp.260-260
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    • 2007
  • 강유전성 세라믹스 재료로써는 PZT계열의 세라믹재료가 널리 쓰이고 있다. 이는 우수한 유전 및 압전특성을 가지고 있으나, PbO을 다량 함유하고 있어 $1000^{\circ}C$이상에서 PbO가 급격하게 휘발되는 성질에 따라서 조성의 변동이 생겨 재현성이 어려우며 이를 방지하기 위하여 과잉 PbO를 첨가시키기 때문에 PbO휘발로 인한 강한 독성이 인체에 유해하다. 최근에는 Pb의 환경문제가 대두됨에 따라 이를 대체할 다른 물질의 개발이 활발하게 연구되고 있다. 대표적인 비납계 강유전 세라믹스인 $(Na_{0.5}K_{0.5})NbO_3$ ($d_{33}$ = 120 pC/N, Kp = 39%, Qm = 210, 이하 NKN라 표기) 조성은 $KNbO_3,\;NaNbO_3$ 상태도에 따라 순수한 NKN 세라믹스는 $1140^{\circ}C$에서 안정상을 가지나, 높은 온도로 인하여$Na_2O$$K_2O$가 쉽게 휘발됨에 따라 화학량 비의 변화가 생겨 이차 상을 형성하기도 한다. 따라서 본 연구에서는 $LiNbO_3$의 새로운 고용체를 추가시켜 기본 NKN조성에 압전성 및 고온에서의 상안정성을 향상시키고자 하였다. 최적 조성을 설계하기 위하여 (1-x)$(Na_{0.5}K_{0.5})NbO_3-xLiNbO_3$, x=(0,0.02,0.04,0.06,0.08)의 범위에서 조성을 변화시키면서 실험하였다. 시편 제작은 일반적인 세라믹스 소결 공정을 적용하였는데, $850^{\circ}C$에서 5시간 하소 후 $1080^{\circ}C$에서 2시간 소결하였다. 하소 및 소결 후에는 XRD분석을 통해 perovskite구조를 확인하였고, 미세구조 확인을 위해 주사전자현미경 (SEM)으로 관찰하였다. 압전특성을 평가하기 위해 압전 $d_{33}$-meter를 사용하였으며, impedance analyzer (HP 4194A)를 이용하여 전기적 특성을 측정하였다.

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Si(100)기판에 $SrBi_2Ta_2O_9$ 박막증착 시 $Bi_2O_3$ 후열처리에 따른 유전특성 (Dielectric properties of SBT($SrBi_2Ta_2O_9$) on $Bi_2O_3$/Pt/Ti/$SiO_2$/Si substrate accordiing to various substrate temperature of $Bi_2O_3$ buffer layer)

  • 윤지언;차원효;이철수;손영국
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.200-201
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    • 2007
  • The SBT($SrBi_2Ta_2O_9$) thin films with $Bi_2O_3$ buffer layer were deposited on Pt/Ti/$SiO_2$/Si substrate by R.F. magnetron sputtering method in order to improve the ferroelectric characteristics. In SBT thin films, the deficiency of bismuth during the process due to its volatility results in an obvious non stoichiometry of the films and the presence of secondary phases. $Bi_2O_3$ buffer layer was found to be effective to achieve the low temperature crystallization and improve the ferroelectric properties of SBT thin films. Ferroelectric properties and crystallinities of SBT thin films with various post annealing of $Bi_2O_3$ buffer layer were observed as various annealing temperature, using X-Ray Diffraction (XRD), scanning electron microscopy (SEM), Keithley 237 and HP 4192A Impedance Analyzer.

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