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Effects of Retained Austenite on Mechanical Properties of 2.3%C-26%Cr-1%Ni-0.5%Mo White Cast Iron

  • Yu, Sung-Kon
    • Journal of Korea Foundry Society
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    • v.18 no.6
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    • pp.586-592
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    • 1998
  • 2.3%C-26%Cr-1%Ni-0.5%Mo 조성의 아공정 백주철을 여러형태로 열처리를 한 후 잔류오스테나이트함량(Vr), 거시 및 미소경도 그리고 내마찰마모성사이의 상호관계를 연구하였다. 주방상태에서의 Vr가 70.2%인 반면 열처리시편들의 경우 0.3-65.4%의 분포를 나타내었다. 초기마모구간 이외에는 마찰마모량과 마모시간과의 사이에 직선적 관계가 얻어졌으며 그 직선의 기울기(Rw)를 내마모성의 비교시 지표로 사용하였다. Rw는 주방상태에서 $2.77{\times}10^{-2}\;mg/s$로 가장 낮았으며 l173k에서 18ks동안 균질화 열처리만 한 시편의 경우 $4.12{\times}10^{-2}\;mg/s$로 내마모성이 가장 열악하였다. 주방상태에서 내마모성이 가장 좋은 이유는 마찰마모시 오스테나이트가 가공경화를 일으켜 마르텐사이트로 변태되었기 때문으로 여겨진다. 미소경도는 HV 358-HV 756, 거시경도는 이 보다 높은 HV 529-HV 785의 분포를 나타내었는데 이는 거시경도의 측정시 공정탄화물인 $M_7C_3$가 포함되었기 때문이다. 가장 높은 미소 및 거시경도는 1323k에서 7.2ks동안 오스테나이화열처리한 시편에서 얻어졌으며 주방상태의 시편이 가장 낮은 경도치를 나타내었다.

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Micro and Nano Engineered High Volume Ultrafine Fly Ash Cement Composite with and without Additives

  • Roychand, R.;De Silva, S.;Law, D.;Setunge, S.
    • International Journal of Concrete Structures and Materials
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    • v.10 no.1
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    • pp.113-124
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    • 2016
  • This paper presents the effect of silica fume and nano silica, used individually and in combination with the set accelerator and/or hydrated lime, on the properties of class F high volume ultra fine fly ash (HV-UFFA) cement composites, replacing 80 % of cement (OPC). Compressive strength test along with thermogravimetric analysis, X-ray diffraction and scanning electron microscopy were undertaken to study the effect of various elements on the physico-chemical behaviour of the blended composites. The results show that silica fume when used in combination with the set accelerator and hydrated lime in HV-UFFA cement mortar, improves its 7 and 28 day strength by 273 and 413 %, respectively, compared to the binary blended cement fly ash mortar. On the contrary, when nano silica is used in combination with set accelerator and hydrated lime in HV-UFFA cement mortar, the disjoining pressure in conjunction with the self-desiccation effect induces high early age micro cracking, resulting in hindering the development of compressive strength. However, when nano silica is used without the additives, it improves the 7 and 28 day strengths of HV-UFFA cement mortar by 918 and 567 %, respectively and the compressive strengths are comparable to that of OPC.

Mechanical Characteristic Evaluation by Spin Tool of Different Pin Shapes in Friction Stir Welding Al6061-T6 (Al6061-T6의 마찰교반용접 시 회전 Tool Pin 형상에 따른 기계적 특성 평가)

  • Lim, ByungChul;Kim, DaeHwan;Park, SangHeup
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.23 no.4
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    • pp.345-349
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    • 2014
  • In this study, an age-hardened 6061-T6 alloy sheet was used, which is commonly utilized for auto parts. The junction strength characteristics in relation to the stirring speed and welding speed were studied in accordance with the friction stir welding rotation of the tool pin. Micro hardness measurements of A type and B type pins, for a welding speed of 400 mm/min and a tool rotational speed 3000 rpm, were obtained as Hv104 and Hv111, respectively. For a welding speed of 200 mm/min and a tool rotational speed of 2000 rpm, we obtained Hv48 and Hv50 for A and B type pins, respectively. Microstructure observation showed that the stirring portion was fine and uniform, which occurred because of its plastic deformation. In the thermomechanically affected zone, partial recrystallization was present because of the plastic deformation. The crystal grains in the heat affected zone were coarsened due to the heat generated by friction stir welding.

A Study on the Welding Process of High Strength Steel Pipe in GTAW-SMAW and SAW (GTAW-SMAW와 SAW를 이용한 고장력강관의 용접에 대한 연구)

  • 이철구;조선근
    • Journal of Welding and Joining
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    • v.12 no.4
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    • pp.41-49
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    • 1994
  • This study is to compare the welding quality of API 5L-X65 Steel- pipe's for natural gas transmission piping applied by SAW at shop and by GTAW-SMAW at site. The results can be summarized as follows; 1) Tensile strength of the welded zone by SAW(611.5 MPa) and by GTAW-SMAW(608.6 MPa) was maintained greater than that of the base metal(583.5 MPa). 2) Hardness of the welded zone and HAZ by SAW(Hv 194.8) & GTAW-SMAW (Hv 196.1) was slightly increased above that of the base metal (Hv 168.8), but less than the maximum allowable hardness(Hv 248). 3) Impact value of the welded zone by SAW(126.8 J) & GTAW-SMAW(88 J) became lower than that of the base metal(282.5 J), but was above the requirement of API 5L(68J). 4) Microscopic structure of the welded zone and HAZ by both SAW & GTAW-SMAW became fine-grained.

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Rapid Selection of Multiple Gene Integrant for the Production of Recombinant Hirudin in Hansenula polymorpha

  • Kim Hwa Young;Sohn Jung Hoon;Kim Chul Ho;Rao K. Jagannadha;Choi Eui Sung;Kim Myung Kuk;Rhee Sang Ki
    • Biotechnology and Bioprocess Engineering:BBE
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    • v.5 no.1
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    • pp.1-6
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    • 2000
  • For the rapid selection of higher recombinant hirudin producing strain in a methylotrophic yeast Hansenula polymorpha, a multiple gene integration and dose-dependent selection vector, based on a telomere-associated ARS and a bacterial aminoglycoside 3-phosphotransferase (aph) gene, was adopted. Two hirudin expression cassettes (HV1 and HV2) were constructed using the MOX promoter of H. polymorpha and the mating factor $\alpha$ secretion signal of S. cerevisiae. Multiple integrants of a transforming vector containing hirudin expression cassettes were easily selected by using an antibiotic, G418. Hirudin expression level and integrated plasmid copy number of the tested transformants increased with increasing the concentration of G418 used for selection. The expression level of HV1 was consistently higher than that of HV2 under the similar conditions, suggesting that the gene context might be quite important for the high-level gene expression in H. polymorpha. The highest hirudin producing strain selected in this study produced over 96 mg/L of biologically active hirudin in a 500-mL flask and 165 mg/L in a 5-L fermentor.

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Effect of Cd Addition on the SCC Properties of Al-Cu-Mn Cast Alloys (Al-Cu-Mn주조합금의 SCC특성에 미치는 Cd첨가의 영향)

  • Lee, Chan-Hui;Kim, Gyeong-Hyeon;Kim, In-Bae
    • Korean Journal of Materials Research
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    • v.11 no.4
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    • pp.266-271
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    • 2001
  • Effect of Cd addition on the stress corrosion cracking(SCC) resistance of Al-Cu-Mn cast alloy was investigated by C-ring test and electrical conductivity measurement. With increasing Cd contents, the electrical conductivity and the SCC resistance were increased. The PFZ and coarse precipitates along the grain boundary were observed from TEM micrographs. The fracture made of the alloys was confirmed as intergranular type and showed brittle fracture surface. As a result, it was concluded that the SCC mechanism of these alloys is the anodic dissolution model. The maximum hardness was increased from 127Hv in the Cd-free alloy to 138∼145Hv in the Cd addition alloys.

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HV-SoP Technology for Maskless Fine-Pitch Bumping Process

  • Son, Jihye;Eom, Yong-Sung;Choi, Kwang-Seong;Lee, Haksun;Bae, Hyun-Cheol;Lee, Jin-Ho
    • ETRI Journal
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    • v.37 no.3
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    • pp.523-532
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    • 2015
  • Recently, we have witnessed the gradual miniaturization of electronic devices. In miniaturized devices, flip-chip bonding has become a necessity over other bonding methods. For the electrical connections in miniaturized devices, fine-pitch solder bumping has been widely studied. In this study, high-volume solder-on-pad (HV-SoP) technology was developed using a novel maskless printing method. For the new SoP process, we used a special material called a solder bump maker (SBM). Using an SBM, which consists of resin and solder powder, uniform bumps can easily be made without a mask. To optimize the height of solder bumps, various conditions such as the mask design, oxygen concentration, and processing method are controlled. In this study, a double printing method, which is a modification of a general single printing method, is suggested. The average, maximum, and minimum obtained heights of solder bumps are $28.3{\mu}m$, $31.7{\mu}m$, and $26.3{\mu}m$, respectively. It is expected that the HV-SoP process will reduce the costs for solder bumping and will be used for electrical interconnections in fine-pitch flip-chip bonding.

A Study on the Properties in Friction Weldability of Ni-Cr-Mo and SM45C (Ni-Cr-Mo과 SM45C의 마찰용접특성(摩擦熔接特性)에 관한 연구(硏究))

  • Lim, Hyung-Taek;Min, Taeg-Ki
    • Transactions of the Korean Society of Machine Tool Engineers
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    • v.16 no.6
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    • pp.29-36
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    • 2007
  • The present study examined the mechanical properties of the friction welding of Ni-Cr-Mo to SM45C. Friction welding was conducted at welding conditions of 2,000 rpm, friction pressure of 100MPa, friction time of 0.8, 1.0, 1.2, 1.4, 1.6, 1.8, 2.0 seconds, upset pressure of 150MPa, and upset time of 3.0 seconds. When the friction time was 1.6 seconds, the maximum tensile strength of the friction weld happened to be 1,020MPa, which is 120% of the base material's tensile strength(850MPa). At the same condition, the maximum shear strength was 438MPa, which is equivalent to 103% of the base material's shear strength(425MPa). At the same condition, the maximum vickers hardness was Hv490 at Ni-Cr-Mo nearby weld interface, which is higher Hv40 than condition of the friction time 0.8 seconds, and the maximum vickers hardness was Hv305 from weld interface of SM45C, which is higher Hv12 than condition of the friction time 0.8 seconds. The results of microstructure analysis show that the structures of two base materials have fined and rearranged along a column due to heating and axial force during friction, which has affected in raising hardness and tensile strength.

A study on the high temperature properties of CoNiCrAlY coating fabricated by HVOF and LPPS process (LPPS용사법과 HVOF 용사법으로 제조된 CoNiCrAlY 코팅의 고온물성에 관한 연구)

  • 강현욱;권현옥;송요승
    • Journal of the Korean institute of surface engineering
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    • v.34 no.2
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    • pp.161-168
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    • 2001
  • A Thermal Barrier Coating (TBC) can play an important role in protecting parts from harmful environments at high temperatures such as oxidation, corrosion, and wear in order to improve the efficiency of aircraft engines by lowering the surface temperature of the turbine blade. The TBC can increase the life span of the product and improve the operating properties. Therefore, in this study the mechanical and thermal properties of the TBC such as oxidation, fatigue and shock at high temperatures were evaluated. A samples of a bond coat (CoNiCrAlY) produced by the High Velocity Oxygen Fuel (HVOF) and Low Pressure Plasma Spray (LPPS) method were used. The thickness of the HVOF coating layer was approximately $450\mu\textrm{m}$ to 500$\mu\textrm{m}$ and the hardness number of the coating layer was between 350Hv and 400Hv. The thickness of the LPPS coating was about 350$\mu\textrm{m}$ to 400$\mu\textrm{m}$ and the hardness number of the coating was about 370Hv to 420Hv. The X-ray diffraction analysis showed that CoNiCrAlY coating layer of the HVOF and LPPS was composed of the $\beta$and ${\gamma}$phase. After the high temperature oxidation test, the oxide scale with about l0$\mu\textrm{m}$ to 20$\mu\textrm{m}$ thickness appeared at the coating surface on the Al-depleted zone was observed under the oxide scale layer.

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Pathogenesis of Hantaan Virus Infection in Suckling Mice -Clinical, Virologic and Serologic Observations-

  • Kim, Gum-Ryong;Mckee, Jr, Kelly T.;Lee, Ho-Wang
    • The Journal of the Korean Society for Microbiology
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    • v.20 no.1
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    • pp.115-125
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    • 1985
  • Hemorrhagic fever with renal syndrome (HFRS) is a debilitating disease of humans caused by Hantaan virus (HV), the prototype member of a newly proposed genus of Bunyaviridae. Studies of HV pathogenesis have been limited by the absence of a well defined model for a virus-induced disease state. In an attempt to devise a model for HV pathogenesis in laboratory rodents, newborn outbred suckling ICR mice were shown to be uniformly susceptible to lethal infection with non- mouse adapted HV by intracerebral (IC), intraperitoneal (IP), intramuscular (IM), and subcutaneous (SC) inoculation routes. Clinical coures, mean time to death, and fatal outcome were age-dependent. With an inoculum of 10 $LD_{50}$, mortality was 100% in mice infected within 72h of birth, but declined to 50% by 7 days. By 2-2.5 weeks, animals developed complete resistance to clinical disease. Virus was consistently detected in serum by day 6 post-infection in IC- and IP- inoculated animals, and reached peak levels of $10^5\;PFU/ml$ by day 8 Mice infected IM and SC showed delays in onset of viremia, but achieved similar titers. Immunofluorescent antibody appeared by 17-18 days, and neutralizing antibody by 15 days, in all experimental groups. Two of 8 inbred mouse strains were identified as resistant to clinical disease : SJL/J and A/J. Manipulation of this model will allow investigation of natural rodent pathogenesis with HV, as well as offer insight into disease mechanisms and therapy of HFRS.

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