• Journal of the Korean Ceramic Society
• /
• v.24 no.3
• /
• pp.257-262
• /
• 1987

The characteristics of cobalt oxide powders prepared by hot petroleum drying method from the cobalt acetate were evaluated by DTA/TGA, XRD, BET, SEM and density measurement. The cobalt oxide powder could be prepared by hot petroleum drying of the emulsion of cobalt acetate salt solution and the subsequent thermal decomposition of the acetate at 300$^{\circ}C$. As the concentration of the salt solution and the calcination temperature of the dried powder increased, the surface area of the synthesized powder decreased due to the particle growth, so that after sintering the density and grain size decreased. For the same concentration of the salt solution, the surface area and sinterability of the powder by hot petroleum drying increased in comparision with those by conventional drying.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2007.10a
• /
• pp.215-222
• /
• 2007

Coating of Hot-dip galvannealed steel consists of various Fe-Zn intermetallic compounds. Since the coating is hard and there for is very brittle, the surface of steel sheet is easy to be ruptured during second manufacturing processing. This is called as powdering. In addition, forming equipment might be polluted with debris by powdering. Therefore, various research have been carried out to prohibit powdering fur improving the quality of GA steel. This paper carried out finite element analysis combined with damage model which simulate the failure of local layer of hot-dip galvannealed steel surface during v-bending test. Since the mechanical property of intermetallic compound was unknown exactly, we used the properties calculated from measurements. The specimen was divided into substrate, coating layer and interface layer. Local failure at coating layer or interface layer was simulated when elemental strain reached a prescribed strain.

• Journal of the Korean institute of surface engineering
• /
• v.39 no.3
• /
• pp.87-92
• /
• 2006

The characteristic of interface layer and the effect of bias voltage on the microstructure of c-BN films were studied in the microwave plasma hot filament C.V.D process. c-BN films were deposited on a high speed steel(SKH-51) substrate by hot filament CVD technique assisted with a microwave plasma to develop a high performance of resistance coating tool. c-BN films were obtained at a gas pressure of 20 Torr, vias voltage of 300 V and substrate temperature of $800^{\circ}C$ in $B_2H_6-NH_3-H_2$ gas system. It was found that a thin layer of hexagonal boron nitride(h-BN) phase exists at the interface between c-BN layer and substrate.

• Journal of the Korean institute of surface engineering
• /
• v.36 no.1
• /
• pp.42-47
• /
• 2003

Hot-dip galvanizing process is used widely in industry to achieve corrosion resistant coatings. Poor drainage during this process often leads to problems such as icicle formation and bridging In this work, mild steel specimens were hot-dip galvanized. Influence of the addition of bismuth, aluminum and both (bismuth and aluminum) to the zinc bath on the zinc drainage were determined. Bismuth additions improved the drainage significantly. Zinc bath containing 0.1 wt.% Bi and 0.025∼0.05 wt.% Al showed uniformity of coatings. Industrial trials with this bath composition showed reduction in zinc consumption, reduction of ash and dross, and good luster of workpiece.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2008.05a
• /
• pp.493-496
• /
• 2008

The residual stress generated in the boron steel blank formed via hot press forming process was predicted by JMatPro, a material property modeler, and Abaqus. The numerical predictions were compared by the experimental measurements obtained by the instrumented indentation. Both the predicted and measured principal stresses monitored at the outer surface of central bending position were qualitatively in good agreement. It was concluded that the residual stresses generated from hot forming process is not negligible as it has been generally assumed, although the spring back deformation is quite small. This should be specially considered from the part design stage since the tensile nature of the residual stress exhibited on the surface may lead to the stress corrosion cracking.

• Journal of Advanced Marine Engineering and Technology
• /
• v.22 no.6
• /
• pp.880-887
• /
• 1998

In order to study heat transfer characteristics of spray cooling for the purpose of uniform and soft cooling of high temperature surface a series of experiments for a hot horizontal copper flat plate was performed by downflow spray water using flat spray nozzle. Cooling curves were mea-sured under the various experimental conditions of flow rates and temperatures of cooling water Surface temperature surface heat fluxes and heat transfer coefficients of horizontal upward-facing flat surface were calculated with cooling curves measured at each radial positions near the cooling surface by TDMA method. Generally heat transfer characteristics for spray cooling is simi-lar to boiling phenomenon of pool boiling. The minimum heat flux(MHF) appear at the surface temperature of about ${\Delta}Tsat=250^{\circ}C$ and the critical heat flux(CHF) appear at about ${\Delta}Tsat=250^{\circ}C$.

• Korean Journal of Materials Research
• /
• v.14 no.6
• /
• pp.379-388
• /
• 2004

To investigate the effect of D-ferrite on the hot workability and surface defect of STS 304 billets containing 3 wt. % Cu, microstructure observations and high temperature mechanical properties test were carried out for the specimens extracted mainly from raw or oxidized billets. It was found that the total $\delta$-ferrite content has little influence on the hot workability, even though the fracture cracks due to high temperature tension or compression test were initiated and propagated mostly along $\delta$/${\gamma}$ boundary in the specimens. On the other hand, it was supposed that the direct causes of surface defects in the wire rolled from the as-continuously cast billet were the grain boundary embrittlement arose from the deep diffusion of oxygen into the grain boundary, and the oxidation of $\delta$-ferrite connected by a grain boundary to the surface during the billet reheating process as well.

• Fire Science and Engineering
• /
• v.14 no.3
• /
• pp.13-18
• /
• 2000

The objective of the present work is to examine the cooling characteristics of water droplet on the unburned surface. The hot solid surface material used brass, carbon steel and copper at temperature ranging from 70 to $116^{\circ}$. the droplet size is from 2.4 mm to 3.0 mm. The CCD camera was used to record the evaporation histories of the droplets. and the evaporation time of the droplet on the hot solid surface could be determined by using frame-by-frame analysis of the video records. It is found that during the droplet evaporation process for copper the temperature remains nearly constant, whereas for carbon steel the temperature continuously decreases about $1^{\circ}$. During the droplet evaporation process on the hot solid surface, regardless of solid materials, nondimensional droplet volume decreases nondimensional evaporation time increases.

• Journal of the Korean Society of Manufacturing Technology Engineers
• /
• v.18 no.6
• /
• pp.697-701
• /
• 2009

A simple method for the fabrication of porous nano-master for the anti-reflection effect on the transparent substrates is presented. In the conventional fabrication methods for antireflective surface, coating method using materials with low refractive index has usually been used. However, it is required to have a high cost and long processing time for mass production. In this paper, we developed a porous nano-master with anti-reflective surface for the molding stamper of the injection mold, hot embossing and UV imprinting by using the aluminum anodizing process. Through two-step anodizing and etching processes, a porous nano-master with anti-reflective surface was fabricated at the large area. Pattern size Pore diameter and inter-pore distance are about 130nm and 200nm, respectively. In order to replicate anti-reflective structure, hot embossing process was performed by varying the processing parameters such as temperature, pressure and embossing time etc. Finally, antireflective surface can be successfully obtained after etching process to remove selectively silicon layer of AAO master.

• Journal of the Korean institute of surface engineering
• /
• v.51 no.4
• /
• pp.224-230
• /
• 2018

In this study, Mg films were prepared on hot dip aluminized steel (HDA) by using a sputtering method as a high corrosion resistance coating. The corrosion resistance of the Mg films was improved by controlling the morphology and the crystal structure of films by adjusting the Ar gas pressure during the coating process. Anodic polarization measurement results confirm that the corrosion resistance of the Mg films was affected by surface morphology and crystal structure. The corrosion resistance of the Mg coated HDA specimen increased with decreasing crystal size of the Mg coating and it was also improved by forming a film with denser morphology. The crystal structure oriented at Mg(101) plane showed the best corrosion resistance among crystal planes of the Mg metals, which is attributed to its relatively low surface energy. Neutral salt spray test confirmed that corrosion resistance of HDA can be greatly improved by Mg coating, which is superior to that of HDG (hot dip galvanized steel). The reason for the improvement of the corrosion resistance of Mg films on hot dip aluminized steel was due to the barrier effect by the Mg corrosion products formed by the corrosion of the Mg coating layer.