• 제목/요약/키워드: Hot pressing method

검색결과 127건 처리시간 0.029초

Microcracking에 의한 세라믹 복합재료의 고인성화 특성 (Toughening Characteristic of Ceramic Composites by Microcracking)

  • 장병국;우상국
    • 한국재료학회지
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    • 제9권2호
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    • pp.132-138
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    • 1999
  • In order to investigate the toughening characteristic by microcrack formation in ceramic composites, $Al_2$O$_3$/(0~20)vol% YAG composites containing equiaxed second grains were fabricated using$ Al_2$$O_3$ during hot-pressing. AE(acoustic emission) measurements have been coupled with fracture toughness experiments of SENB method, to evaluate the microcrack formation and the improvement in fracture toughness of ceramic composites. Formation of microcrack was detected by Ae. The generation of AE events increased with increasing of load when load was applied at specimen. The AE events are generated mainly around at maximum load. Specially, the detected AE evetns of composites are many as compared with monolithic $Al_2$$O_3$. Fracture toughness of composites was improved than that of monolithic alumina. $Al_2$O$_3$/YAG composites exhibit main toughening effects by microcracking, results from mutual coalesence of microcracks being generated under applied load. However, there are few toughening mechanism like microcracking in monolithic alumina.

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나노 다이아몬드가 첨가된 초고분자량 폴리에틸렌의 마모특성에 대한 연구 (Tribological performance of UHMWPE reinforced with nano-diamond)

  • 임동필;임대순
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2003년도 학술대회지
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    • pp.72-77
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    • 2003
  • Nano-diamonds were added to Ultra-high molecular weight polyethylene (UHMWPE) to improve the tribological properties of UHMWPE. Nano-diamonds which have a diameter of about 5-10nm were produced by detonation. UHMWPE/nano-diamonds composites were fabricated by hot pressing method. It is shown that friction coefficient was increased and wear resistance was improved as nano-diamonds were added to UHMWPE because of excellent mechanical properties of nano-diamonds located on UHMWPE surface.

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합판용 페놀수지 접착제에 대한 TCA침전 혈액분말의 첨가효과 (Adding Effect of TCA-Precipitated Blood Powder to the Phenol Formaldehyde Resin for Plywood)

  • 이화형;이종신;장상식
    • Journal of the Korean Wood Science and Technology
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    • 제24권2호
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    • pp.15-19
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    • 1996
  • To utilize the waste materials and develope wood adhesive from isolated bloods of slaughtered cow and pig and also to prevent water pollution, simple and rapid method of isolation and purification of plasma proteins from pig bloods with trichloroacetic acid(TCA) treatment was developed. Adding of TCA-precipitated blood powder to the phenol formaldehyde resin(PF) improved dry and wet strength of plywood and resulted in fast hot pressing times.

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Investigation of Microstructure Inhomogeneity in SiCp-reinforced Aluminum Matrix Composites

  • Gacsi, Zoltan;Gur, C.Hakan;Makszimus, Andrea;Pieczonka, Tadeusz
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.1303-1304
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    • 2006
  • The type, volume fraction, size, shape and arrangement of embedded particles influence the mechanical properties of the particle reinforced metal matrix composites. This presents the investigation of the SiC particle and porosity distributions in various aluminum matrix composites produced by cold- and hot-pressing. The microstructures were characterized by optical microscopy and stereological parameters. SiC and porosity volume fractions, and the anisotropy distribution function were measured to establish the influence of the consolidation method.

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PZT/PVDF O-3형 복합전체에 있어서 PZT 체적비 변화가 유전 및 압전특성에 미치는 영향 (Effects on PZT volume fraction on the dielectric and piezoelectric properties with PZT/PVDF O-3 composites)

  • 이덕출;김용혁
    • E2M - 전기 전자와 첨단 소재
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    • 제1권1호
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    • pp.44-53
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    • 1988
  • In this study, PZT/PVDF composites with O-3 phase connectivity were prepared by hot pressing method, and the dielectric and piezoelectric properties as a function of PZT volume fraction were investigated. A modified cubic model was introduced to explain the influence of the PZT volume fraction on the experimentally determined dielectric constant. As A n=0.125, the measured dielectric constant values agreed with the calculated values. It was found that dielectric constant .xi.$_{33}$ and piezoelectric coefficient d$_{33}$ increased with indreasing PZT volume fraction, and hydrostatic piezoelectric figure of merit d/aub h/.g$_{h}$ was improved relative to that of the PZT single phase material.l.l.l.

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Thermo-electrical properties of randomly oriented carbon/carbon composite

  • Raunija, Thakur Sudesh Kumar;Supriya, N.
    • Carbon letters
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    • 제22권
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    • pp.25-35
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    • 2017
  • The aim of the work was to investigate the thermo-electrical properties of low cost and rapidly produced randomly oriented carbon/carbon (C/C) composite. The composite body was fabricated by combining the high-pressure hot-pressing (HP) method with the low-pressure impregnation thermosetting carbonization (ITC) method. After the ITC method step selected samples were graphitized at $3000^{\circ}C$. Detailed characterization of the samples' physical properties and thermal properties, including thermal diffusivity, thermal conductivity, specific heat and coefficient of thermal expansion, was carried out. Additionally, direct current (DC) electrical conductivity in both the in-plane and through-plane directions was evaluated. The results indicated that after graphitization the specimens had excellent carbon purity (99.9 %) as compared to that after carbonization (98.1). The results further showed an increasing trend in thermal conductivity with temperature for the carbonized samples and a decreasing trend in thermal conductivity with temperature for graphitized samples. The influence of the thickness of the test specimen on the thermal conductivity was found to be negligible. Further, all of the specimens after graphitization displayed an enormous increase in electrical conductivity (from 190 to 565 and 595 to 1180 S/cm in the through-plane and in-plane directions, respectively).

Numerical simulation of dimensional changes during sintering of tungsten carbides compacts

  • Bouvard, D.;Gillia, O.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 1997년도 추계학술강연 및 발표대회 강연 및 발표논문 초록집
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    • pp.7-7
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    • 1997
  • During sintering of very porous green bodies, as obtained by compaction of hard powders - such as tungsten carbide or ceramics - or by injection moulding, important shrinkage occurs. Due to heterogeneous green density field, gravity effects, friction on the support, thermal gradients, etc., this shrinkage is often non-uniform, which' may induce significant shape changes. As the ratio of compact dimension to powder size is very high, the mechanics of continuum is relevant to model such phenomena. Thus numerical techniques, such as the finite element method can be used to simulate the sintering process and predict the final shape of the sintered part. Such type of simulation has much been developed in the last decade firstly for hot isostatic pressing and next for die compaction. Finite element modelling has been recently applied to free sintering. The simulation of sintering should be based on constitutive equations describing the thermo-mechanical behaviour of the material under any state of stress and any temperature which may arise within the sintering body. These equations can be drawn either from experimental data or from micromechanical models. The experiments usually consist in free sintering and sinter-forging tests. Indeed applying more complex loading conditions at high temperature under controlled atmosphere is delicate. Micromechanical models describe the constitutive behaviour of aggregates of spheres from the deformation of two-sphere contact either by viscous flow or grain boundary diffusion. Such models are not able to describe complex microstructure and mechanisms as observed in real materials but they can give some basic information on the formulation of constitutive equations. Practically both experimental and theoretical approaches can be coupled to identify the constitutive equations. Such procedure has been performed for modelling the sintering of compacts obtained by die pressing of a mixture of tungsten carbide and cobalt powders. The constitutive behaviour of this material during sintering has been described by a linear viscous constitutive model, whose functions have been fitted from results of free sintering and sinter-forging experiments. This model has next been introduced in ABAQUS finite element code to simulate the sintering of heterogeneous green compacts of various geometries at constant temperature. Examples of simulations are shown and compared with experiments.

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Rheo-compocasting법에 의한 SiC입자분산 복합재료의 마모특성에 관한 연구 (A Study on the Wear Characteristics of SiC Particle Dispersed Composites by Rheo-Compocasting Method)

  • 곽현만;최창옥
    • 한국주조공학회지
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    • 제13권3호
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    • pp.238-247
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    • 1993
  • Microstructure, hardness and wear characteristics of $SiC_p/Al-6.5wt%Si-1.7wt%Mg$ alloy composites fabricated by the method of rheo-compocasting and hot pressing are investigated in this study. The dispersion of SiC particles in the composites is homogeneous and the hardness improves as additional amount increases. The wear amount of the matrix metal increases highly as wear rates increase, for the wear mechanism changes from adhesive wear to melt wear, and the matrix metal was coated on the surface of revolving disc and its weight increases. In the 5vol% composites, Fe is adhered on the surface of specimen by the projection of the dispersed hard SiC particles which have net-work structure and the coating layer is about $300{\mu}m$. But in the composite more than 20vol%, the wear amount of composite decreases because the SiC particles which have superior hardness, wear resistance and heat resistance properties resist wear, the abrasive wear turn out predominant wear mechanism and so the wear amount of revolving disc increases.

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미세채널 전사성 향상을 위한 사출성형 공정최적화 기초연구 (A study on the process optimization of injection molding for replicability enhancement of micro channel)

  • 고영배;김종선;유재원;민인기;김종덕;윤경환;황철진
    • Design & Manufacturing
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    • 제2권1호
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    • pp.45-50
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    • 2008
  • Micro channel is to fabricate desired pattern on the polymer substrate by pressing the patterned mold against the substrate which is heated above the glass transition temperature, and it is a high throughput fabrication method for bio chip, optical microstructure, etc. due to the simultaneous large area patterning. However, the bad pattern fidelity in large area patterning is one of the obstacles to applying the hot embossing technology for mass production. In the present study, stamper of cross channel with width $100{\mu}m$ and height $50{\mu}m$ was manufactured using UV-LiGA process. Micro channel was manufactured using stamper manufactured in this study. Also replicability appliance was evaluated for micro channel and factors affected replicability were investigated using Taguchi method.

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가온 가압법에 의한 밀랍도포한지의 탈랍율이 탈랍지의 열화 거동에 미치는 영향 (Effect of Dewaxing Ratio of Beeswax-treated Hanji by Heat and Pressure Method on Aging Behavior of Dewaxed Hanji)

  • 조병욱;최도침;조병묵
    • 펄프종이기술
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    • 제44권3호
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    • pp.15-21
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    • 2012
  • The optimum dewaxing ratio in dewaxing treatment by the heat and pressure method was investigated by considering aging stability of dewaxed Hanji. Commercial Hanji was coated with beeswax and thermally aged at $150^{\circ}C$ for 24 hours. Then it was dewaxed using the laboratory sheet press equipped with hot plates on both top and bottom sides. Dewaxing ratio was controlled by pressing temperature and time. Four type of dewaxed Hanji samples with different dewaxing ratio were prepared and thermally aged at $150^{\circ}C$. Then the aging stability of dewaxed Hanji samples was evaluated in terms of optical and strength properties. It was found that the aging stability of dewaxed Hanji was superior with higher dewaxing ratio. The result concluded that, in the aspect of aging stability, the coated beeswax in beeswax-treated Hanji shall be completely removed if the coated wax would be dewaxed.