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Physical Properties of the Nonstoichiometric Perovskite $Dy_{1-x}Sr_xCoO_{3-y}$ System

  • 정수경;김민규;김규홍;여철현
    • Bulletin of the Korean Chemical Society
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    • v.17 no.9
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    • pp.794-798
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    • 1996
  • Solid solutions of the nonstoichiometric Dy1-xSrxCoO3-y system with the compositions of x=0.00, 0.25, 0.50, 0.75, and 1.00 have been synthesized by the solid state reaction at 1000 ℃ under atmospheric air pressure. The crystallographic structures of the solid solutions are analyzed by the powder X-ray diffraction patterns at room temperature. The analyses assign the compositions of x=0.00 and 0.25 to the orthorhombic system with space group of Pbnm/D2h16, the compositions of x=0.50 and 0.75 to the tetragonal system like a typical SrCoO2.86, and the composition of x=l.00 or SrCoO2.50 to the brownmillerite type system with space group of I**a. The reduced lattice volumes increase with x value due to the larger radius of Sr2+ ion than that of Dy3+ ion. The mole ratio of Co4+ ion to total Co ion with mixed valence state between Co3+ and Co4+ ions at B sites or τ value has been determined by an iodometric titration. All the samples except for the DyCoO3 compound show the mixed valnce state and thus the composition of x=0.50 has the maximum τ value in the system. The oxygen vacancies increasing with x value are randomly distributed over the crystal lattice except for the composition of x=l.00 which have the ordering of the oxygen vacancies. The nonstoichiometric chemical formulas of the Dy1-xSrxCo3+1-τCo4+τO3-(x-τ)/2 system are formulated from the x, τ, and y values. The electrical conductivity in the temperature range of 100 to 900 K increases with τ value linearly because of positive holes of the Co4+ ions in π* band as a conducting carrier. The activation energy of the x=0.50 as Ea=0.17 eV is minimum among other compouds. Broad and high order transition due to the overlap between σ* and π* bands broadened by the thermal activation is observed near 1000 K and shows a low temperature-semiconducting behavior. Magnetic properties following the Currie-Weiss law show the low to high spin transition in the cobaltate perovskite. Especially, the composition of x=0.75 presents weak ferromagnetic behavior due to the Co3+-O2--Co4+ indirect superexchange interaction.

Seismic Velocity Structure Along the KCRT-2008 Profile using Traveltime Inversion of First Arrivals (초동주시 역산을 통한 KCRT-2008 측선 하부의 지진파 속도구조)

  • Kim, Ki-Young;Lee, Jung-Mo;Baag, Chang-Eob;Jung, Hee-Ok;Hong, Myung-Ho;Kim, Jun-Yeong
    • Geophysics and Geophysical Exploration
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    • v.13 no.2
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    • pp.153-158
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    • 2010
  • To investigate the velocity structure in the central and southern parts of the Korean peninsula, a 299-km NW-SE seismic refraction profile KCRT-2008was obtained across major tectonic boundaries. Seismic waves were generated by detonating 250 ~ 1500 kg explosives at depths of 50 ~ 100 m in eight drill holes located at intervals of 21 ~ 113 km. The seismic signals were detected by 4.5 Hz geophones at a nominal interval of 500 m. The first-arrival times were inverted to derive a velocity tomogram. The raypaths indicate several mid-crust interfaces including those at approximate depths of 2 ~ 3, 11 ~ 13, and 20 km. The Moho discontinuity with refraction velocity of 7.7 to 8.1 km/s has a maximum depth of 34.5 km under the central portion of the peninsula. The Moho becomes shallower as the Yellow Sea and the East Sea are approached on the west and east coasts of the peninsula, respectively. The depth of the 7.6 km/s velocity contour varies from 31.3 km to 34.4 km. The velocity tomogram shows the existence of a 129 km wide low-velocity zone centered at 7.2 km depth under the Okchon fold belt and Gyeonggi massif and low-velocity(< 5.4 km/s) rocks in the Gyeongsang sedimentary basin with a maximum thickness of 2.6 km

Postharvest Handling and Marketing Management for Making High Salability of Sweetpotatoes (상품성 제고를 위한 고구마 수확 후 관리 및 출하기술)

  • Jeong, Byeong-Choon
    • Proceedings of the Korean Society of Postharvest Science and Technology of Agricultural Products Conference
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    • 2001.06a
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    • pp.51-64
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    • 2001
  • The qualities including taste of sweetpotato stored during the winter which can display in the spring market in Korea are affected by availability of storage for the roots. In order to make high storage availability of sweetpotato, the postharvest handlings should be done thoroughly from the moment of harvest until shipping them to the market. A lot of procedures that must be handled carefully for improving postharvest management are as follows; digging, trimming, gathering, putting in storage containers, carrying them from field to house, curing, storing, washing, drying, selecting marketable roots, packing and shipping to the market, etc.. Sweetpotatoes have a high moisture content, and a relatively thin and delicate skin, and are sensitive to chilling, so careless postharvest handling can lead to both quantitative and qualitative losses which may be extremely high in some circumstances. From now on research has concentrated on the improvement of postharvest conditions to increase yield and lower disease rates. Storage, which makes sweetpotatoes available through out the year, benefits both the producer and the consumer. Seven very important points must be needed in order to get the best quality marketable roots in the storing of sweetpotatos : $\circled1$The storage house must be clean and sanitary, $\circled2$The crop must be harvested before the first frost to avoid low-temperature injury, $\circled3$Particular care must be taken to avoid cutting, bruising, or other injuries of the sweetpotatoes during digging, picking up, grading, placing in containers, and moving to the storage house, $\circled4$Select sound, disease-free roots for storage $\circled5$Sweetpotatoes should be stored in properly stacked containers $\circled6$Cure immediately after harvest, preferably at 32∼33$^{\circ}C$ and 90 to 95 percent relative humidity for 4 to 7 days, After curing the temperature should be reduced to 13$^{\circ}C$ to 16$^{\circ}C$ by ventilating the storage with outside air. $\circled7$Store at 12$^{\circ}C$ to 14$^{\circ}C$ and a relative humidity of 80 to 85 percent. Storage houses should be located on suitable sites and should be tightly constructed and insulated so that temperature and humidity will be uniform. Sweetpotatoes are usually not washed and graded, and lately sometimes washed, graded, waxed, before being shipped to market. Consumer packaging of sweetpotatoes in paper boxes(10-15kg) or film bags is done mainly to aid marketing. The shelf life of washed roots in consumer packs in only 1 to 2 weeks. Weight loss of roots during marketing is much less in perforated film bags than in mesh and paper bags. Perforation of 0.8 to 1kg polyethylene bags with about six 6mm holes is essential ; to lower the internal relative humidity and avoid excessive sprouting, rooting, and dampness. Development and use of better postharvest handling with good storage facilities or marketing methods can minimize sweetpotate losses and has an effect of indirectly increasing productivity and farmer’s income.

Environment Factors for Germination, Growing and Storage of Sprout Vegetables of Coreopsis tinctoria Nutt., Saussurea pulchella (Fisch.) Fisch. and Matricaria recutica L. (국화과 기생초, 각시취 및 저먼캐모마일 새싹채소의 발아, 재배 및 저장에 미치는 환경요인)

  • Lee, Moo-Yeul;Shin, So-Lim;Chang, Young-Deug;Lee, Cheol-Hee
    • Korean Journal of Plant Resources
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    • v.22 no.2
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    • pp.136-144
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    • 2009
  • Germination tests on 3 species that have potential for use as sprout vegetables, such as Coreopsis tinctoria, Saussurea pulchella, and Matricaria recutica, were conducted for 20 days under different temperatures of $15{\sim}30^{\circ}C$, and conditions of light and dark. C. tinctoria showed germination of 83% under $15^{\circ}C$ and dark condition after 4 days, S. pulchella 51.7% under $25^{\circ}C$ and light condition after 20 days, and M. recutica 90.3% under $25^{\circ}C$ and dark condition after 4 days. To investigate optimum plantlet size before greening treatment, seeds germinated were allowed to grow under darkness. The optimum growth of C. tinctoria was obtained under $30^{\circ}C$ after 5 days, S. pulchella under $25^{\circ}C$ after 6 days, and M. recutica under $20^{\circ}C$ after 6 days. Greening treatment resulted in diminished longitudinal growth, but C. tinctoria and S. pulchella showed more vigorous latitudinal growth. Days required before marketing as sprout vegetables were different according to species - Three days of greening was good for C. tinctoria, 2 for S. pulchella, no greening for M. recutica. Generally, tightly sealed containers for minimum water loss were recommended for storage of sprout vegetables after harvest. However, storage methods for each species were different depending on various factors like temperature of storage, presence of ventilation holes of storage packages and forms of marketing. More detailed research for above 3 species is proposed.

Effects of ibuprofen-loaded TiO2 nanotube dental implants in alloxan-induced diabetic rabbits

  • Kim, Young-Gyo;Kim, Wan-Tae;Jung, Bo Hyun;Yoo, Ki-Yeon;Um, Heung-Sik;Chang, Beom-Seok;Lee, Jae-Kwan;Choi, Won-Youl
    • Journal of Periodontal and Implant Science
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    • v.51 no.5
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    • pp.352-363
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    • 2021
  • Purpose: Some systemic conditions, especially diabetes mellitus (DM), adversely affect dental implant success. This study aimed to investigate the effects of ibuprofen-loaded TiO2 nanotube (ILTN) dental implants in alloxan-induced diabetic rabbits. Methods: Twenty-six New Zealand white rabbits were treated with alloxan monohydrate to induce DM. At 2 weeks following DM induction, 3 types of implants (sandblasted, large-grit, and acid-etched [SLA], ILTN, and machined) were placed into the proximal tibia in the 10 rabbits that survived following DM induction. Each type of implant was fitted randomly in 1 of the holes (round-robin method). The animals were administered alizarin (at 3 weeks) and calcein (at 6 weeks) as fluorescent bone markers, and were sacrificed at 8 weeks for radiographic and histomorphometric analyses. Results: TiO2 nanotube arrays of ~70 nm in diameter and ~17 ㎛ in thickness were obtained, and ibuprofen was loaded into the TiO2 nanotube arrays. A total of 26 rabbits were treated with alloxan monohydrate and only 10 rabbits survived. The 10 surviving rabbits showed a blood glucose level of 300 mg/dL or higher, and the implants were placed in these diabetic rabbits. The implant stability quotient (ISQ) and bone-to-implant contact (BIC) values were significantly higher in the ILTN group (ISQ: 61.8, BIC: 41.3%) and SLA group (ISQ: 62.6, BIC: 46.3%) than in the machined group (ISQ: 53.4, BIC: 20.2%), but the difference in the BIC percentage between the SLA and ILTN groups was not statistically significant (P=0.628). However, the bone area percentage was significantly higher in the ILTN group (78.0%) than in the SLA group (52.1%; P=0.000). Conclusions: The: ILTN dental implants showed better stability (ISQ) and BIC than the machined implants; however, these values were similar to the commercially used SLA implants in the 2-week diabetic rabbit model.

Numerical Analysis on Effect of Stemming Condition in Mine Ventilation Shaft Blasting (광산 통기수갱발파에서 전색조건이 발파효율에 미치는 영향에 관한 수치해석적 연구)

  • Kim, Jun-ha;Kim, Jung-gyu;Jung, Seung-won;Ko, Young-hun;Baluch, Khaqan;Kim, Jong-gwan
    • Explosives and Blasting
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    • v.39 no.3
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    • pp.15-23
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    • 2021
  • Ventilation shafts are pathways in mines and tunnels for the removal of dust or smoke during underground space construction and operation. In mines, blasting with long blast holes is preferred for the excavation of a ventilation shaft in the 10~20m long crown pillar section. In this case, the bottom part of the blast hole is completely drilled in order to determine the drilling error, and this causes a problem of lowering the explosive charge and blasting efficiency. It is possible to solve the problem of explosive loading and to increase the blast efficiency by covering the curb of the blasthole by using stemming material. In this study, simulations for the blasting of a ventilation shaft were performed with various stemming lengths and the blasthole diameters(45, 76mm) using AUTODYN 2D SPH(Smooth particle hydrodynamics) analysis technique. Also the optimal bottom stemming column was derived by checking the size of the boulder and burden line according to blasting. Analysis result, blasting efficiency is lessened in case of stemming length less than 30cm and the optimal length of the stemming material should be 30cm or higher to achieve high efficiency of blasting.

Smoke Control Experiment of a Very Deep Underground Station Where Platform Screens Doors are Installed - Analysis on Smoke Control Performance by Fans equipped in Tunnel (스크린도어가 설치된 대심도 지하역사의 제연 실험 - 터널 송풍기에 의한 제연의 효과 분석)

  • Park, Won-Hee;Kim, Chang-Yong;Cho, Youngmin
    • Asia-pacific Journal of Multimedia Services Convergent with Art, Humanities, and Sociology
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    • v.9 no.9
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    • pp.721-736
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    • 2019
  • In this paper, the behavior of the fire smoke due to the operation of the ventilation systems when the fire occurred in the underground station (6 basement floors) and the tunnel at the great depth was measured. Fire smoke was generated by using a smoke generator which realized heat buoyancy effect by using hot air blower. The two locations of the fire were selected on the platform and on the platform of the tunnel located outside the screen door. A ventilation mode is generally used in which smoke is exhausted through a vent hole provided in a platform when a platform fire occurs. The tests were performed by operating the exhaust through the ventilation holes of the tunnel part located at both ends of the platform. The smoke density and the wind speed/velocity were measured at various positions, and the videos were taken to analyze the movement and smoke of the smoke. In both cases for fire inside the platform and in the railway tunnel, due to the ventilation mode operation of the fan for the platform and the exhaust of the fans in the tunnel smoke were well exhausted and the smoke propagation to the area near the smoke zone was suppressed. The smoke-control mode, which is applied to both fans for the platform and fans for in the tunnel at both ends of the platform, can provide a safer evacuation environment to the passengers from the fire smoke when the platform fire or fire train stops.

Integrated Assessment for Commercialization of Road Hazardous Information Colleted by Commercial Vehicles (사업용 차량 기반 도로위험정보 제공의 상용화를 위한 통합 평가)

  • Yoo, Kyung-su;Chung, Kyungmin;Chae, Chandle
    • The Journal of The Korea Institute of Intelligent Transport Systems
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    • v.20 no.2
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    • pp.30-42
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    • 2021
  • The amount of compensation and the number of cases owing to car damage from pot holes on highways across the country increased by about 4.2 times and 3.5 times, respectively, in 2019 compared to 2015. Due to the increase in damage caused by these road hazards, the Ministry of Land, Infrastructure and Transport is developing technologies and services that can collect road hazard information by using devices on commercial vehicles (DTGs, black boxes, ADASs). In preparation for the development of these technologies, this study conducted an integrated assessment of algorithms developed for interrupted-flow and uninterrupted-flow traffic under three scenarios in order to provide road hazard information to drivers and road managers. As a result, the overall accuracy of the integrated assessment was derived at 81.88%. Errors generated in this integrated assessment reflect only missing data in less than 1 minute, GPS coordinate location and algorithm related errors, taking into account the purpose and assumptions of the assessment. Among them, we derive an accuracy of 90.15%overall by calibrating GPS error data. The results of this study can be used as basic data for improving the accuracy of location-based information collected by commercial vehicles and for policy development.

A Study on the Uniform Mixing of Ammonia-Air with the Change of Ammonia Supply Device Shape in a De-NOx System (탈질설비에서 암모니아 혼합기의 형상에 따른 암모니아-공기 균일 혼합에 관한 연구)

  • Ha, Ji Soo
    • Journal of the Korean Institute of Gas
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    • v.23 no.3
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    • pp.20-26
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    • 2019
  • Selective catalytic reduction(SCR) method is widely used among various methods for reducing nitrogen oxides in combustion devices of coal power plant. In the present study, the computational fluid dynamic analysis was accomplished to derive the optimal shape of ammonia-dilution air mixing device in a ammonia injection grid. The distribution characteristics of flow and $NH_3$ concentration had been elucidated for the reference shape of ammonia mixing device(Case 1). In the mixing device of Case 1, it could be seen that $NH_3$ distribution was shifted to the wall opposite to the inlet of the ammonia injection pipe. For the improvement of $NH_3$ distribution, the case(Case 2) with closing one upper injection hole and 4 side injection holes, the case(Case 3) with installing horizontal plate at the upper of ammonia injection pipe, the case(Case 4) with installing horizontal plate and horizontal arc plate at he upper of ammonia injection pipe were investigated by analyzing flow and $NH_3$ concentration distributions. From the present study, it was found that the % RMS of $NH_3$ for Case 4 was 4.92%, which was the smallest value among four cases, and the range of $R_{NH3}$ also has the optimally uniform distribution, -10.82~8.34%.

Numerical Analysis on Development of Nozzle Shape for NOVEC Gas Extinguishing System (NOVEC가스 소화설비용 노즐 형상 설계에 대한 수치해석)

  • Yun, Jeong In;Jung, Kyung Kuk;Kim, Ji Sung;Kim, Sung Yoon;Rho, Beom-Seok;Choi, Jae-Hyuk
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.24 no.7
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    • pp.939-944
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    • 2018
  • Clean fire extinguishing agents refer to chemical that can replace Halon 1211 and Halon 1310 according to the Montreal Protocol fermented to protect the Earth's ozone layer. In Korea and abroad, system standardization and performance evaluation of clean fire extinguishing agents are being carried out. This paper proposes an optimal nozzle shape by modeling and numerical analysis of various nozzle shapes based on general clean fire extinguishing system. The ejection speed of the nozzle can be improved by studying three - dimensional modeling of the nozzle for two shapes, Type A and B. Flow analysis was performed on the two types of nozzles and the gas velocity and pressure distribution were measured with different nozzle diameters. It was confirmed that the jetting speed was changed at the nozzle outlet according to the number and diameter of the nozzle holes. The flow rate increased with increasing the pressure regardless of the nozzle hole diameter. Based on the results obtained from the experiment, the K-factor value was deduced. Finally, a nozzle with a 12-hole structure with a 5-mm nozzle hole was proposed.