• 한국세라믹학회지
• /
• 제54권5호
• /
• pp.395-399
• /
• 2017

The thermal properties and crystallization behavior of calcium phosphate glass fabricated using eggshell were examined. Nature eggshell has several impurities in the main component of $CaCO_3$. To manufacture calcium phosphate glass, washed eggshell was dissolved in aqua-regia while adding a solution of isopropyl alcohol, D. I. water and phosphoric acid. The calcined precursor was melted at $1000^{\circ}C$, and the glass ($T_g$ : $540^{\circ}C$) was crystallized at $620{\sim}640^{\circ}C$, which temperature range is relatively low compared to the crystallization temperature of other general types of calcium phosphate glass. The calcium phosphate glass using eggshell was successfully crystallized without any additional nucleating agents due to the multiple effects of impurities such as $Fe_2O_3$, $Al_2O_3$, SrO and $SiO_2$ in the eggshell. The main crystalline phase was ${\beta}-Ca(PO_3)_2$ and a biocompatible material, hydroxyapatite, was also observed. The crystallization process was completed under the condition of a holding time of only 1 h at the low temperature.

• 한국조경학회지
• /
• 제27권5호
• /
• pp.48-56
• /
• 2000

This study aims to find out the norms and principles reflected in the spatial organization of royal tombs in the Chosun Dynasty through the modern interpretation of traditional oriental philosophy theory. We examined the characteristics of royal tomb sites including Jeshil(Shrine), Hongjunmun, tomb mound, ponds, and attached buildings employing an analysis of the spatial formation and landscape. This study covered 36 tombs of kings and queens in the Chosun Dynasty. The entire layout of royal tombs, including annexed buildings, was informal in may cases. This was due to following the natural contour rather than adhering to certain philosophical principles. The royal tomb site is divided into three zones. Jeshil and pond constitute a space for living people, visitors. Secondly, the semi-scared space includes the space from Hongjunmun to the entrance to the Chungjaka. The last space is for the dead, from the back of Chungjakak to tomb mound. This is in line with the layout of palaces of the Chosun Dynasty which is characterized by "three gates and three zones": outer yard-court yard- back yard. The size of the space for holding memorial ceremonies, from Hongjunmun to the Chungjakak entrance, was set at 900m until the early Chosun Dynasty. Since that time the distance varied according to the land topography due to the influence of metaphysics. It can be summarized that the spatial organization of royal tombs in the Chosun Dynasty is based on the Confucianism value, the natural contour of the site, and inner spiritual value.ual value.

• 대한기계학회논문집
• /
• 제12권6호
• /
• pp.1296-1302
• /
• 1988

The study has been carried out under various experimental conditions to investigate mechanical properties by the transformation conditions of austempered low-alloy ductile cast iron. The amount of retained austenite and bainite after quenching was determined by the X-ray diffractometer and the point counting method and which the microstructure was investigated by the S.E.M. The mechanical properties of austempered low-alloy ductile cast iron can be varried over a comparatively wide range by changing the transformation conditions. During isothermal transformation of austenite in the bainite region, low-alloy ductile cast iron austempered at holding time of 40 minute has the maximum volume fraction(24%) of retained austenite in the cast iron matrix and which optimum values of mechanical properties correspond to the maximum amount of retained austenite, which falls with decreasing transformation temperature. The low values of both tensile strength and elongation in the initial stage of bainite transformation can be explained by premature fracture of tensile specimens and the tensile strength, hardness and elongation do not change considerably after a certain period. With a decreasing transformation temperature the tensile strength increase while the elongation decrease, especially the elongation has the maximum value at temperature $370^{\circ}C$.

• 한국자동차공학회논문집
• /
• 제13권6호
• /
• pp.128-134
• /
• 2005

In order to fabricate the aluminum alloys with good drawability, the textures evolution of the AA5182 sheets after rolling and annealing was studied. The measurement of the deformation textures was carried out for the sheets which were cold rolled with high reduction ratio by using the symmetric roll. In addition, the change of the recrystallization texture was investigated after heat-treatments of the rolled sheets with various heat treatment conditions. Rolling without lubrication and subsequent annealing led to the formation of favorable $rot-C_{ND}\;\{001\}<110>\;and\;{\gamma}-fiber ND//<111>$ textures in AA5182 sheets. From the results, the ${\gamma}$-fiber ND//<111> component well evolved during rolling at highest reduction ratio (over $90\%$, l/d parameter of 6.77). Among shear deformation textures, the ${\gamma}$-fiber ND//<111> was not rotated in holding time of $180\~7,200$ seconds at $350^{\circ}C$. The Monte-Carlo technique was used and could be representatively simulated these textures evolution during recrystallization.

• 조명전기설비학회논문지
• /
• 제15권2호
• /
• pp.73-79
• /
• 2001

본 논문은 심플한 단상 에어컨의 역률 개선회로에 관해 설명한다. 정류기에 역률제어회로를 적용함에 의해서 전원선으로의 고조파 삽입을 줄일 수 있고, 효율을 향상시킬 수 있으며, 기존의 인버터와 비교해서 전체 시스템 가격을 낮출 수 있다. 또한 역률제어회로의 출력전압을 안정화함에 의해서 시스템 성능을 향상시킨다. 다이오드 정류기의 전류 파형을 향상시키기 위해 전압 다이오드 정류기에 대한 새로운 원리를 제안한다. 제안한 회로의 설계방법은 시뮬레이션과 실험에 의해 확인하였다. 그리고 기존의 펄스폭변조 인버터와 반펄스폭변조 인버터를 비교하였으며, 제안된 HPWM 인버터에 의해서 낮은 스위칭 손실과 오버슈팅을 제어할 수 있다.

• 한국전기전자재료학회논문지
• /
• 제20권6호
• /
• pp.496-501
• /
• 2007

In order to enhance sintering characteristics on the $ZnO-Pr_6O_{11}$ based multilayer chip varistors (MLVs), a response surface analysis using central composite design method were carried out. As a result, varistor voltage($V_{1mA}$), nonlinear coefficient ($\alpha$), leakage current ($I_L$) and capacitance (C) were considered to be mainly affected by sintered temperature and holding time. MLVs sintered at $1200^{\circ}C$ and above $1200^{\circ}C$ revealed poor electrical characteristics, possibly due to the reaction between electrode materials(Pd) and $ZnO-Pr_6O_{11}$ based ceramics. On the sintering temperature range $1150{\sim}1175^{\circ}C$, nonlinear coefficient ($\alpha$) and leakage current ($I_L$) were shown to be $60{\sim}69$ and below $0.3{\mu}A$, respectively. In particular, MLVs sintered at $1175^{\circ}C$, 1.5 hr and $2^{\circ}C/hr$ (cooling speed) showed stable ESD(Electrical Static Discharge) characteristics under the condition of 10 times at 8 Kv with deviation varistor voltage, and deviation nonlinear coefficient were 0.3% and 0.33% (at positive), 0.55% (at negative), respectively.

• 한국전기전자재료학회논문지
• /
• 제11권12호
• /
• pp.1139-1145
• /
• 1998

In this paper, to fabricate a superconducting fault current limiter(FCL) of thick film type, $YBa_2Cu_3O_X superconducting thick films were fabricated by surface diffusion process using the screen printing method. Powder mixture of $3BaCuO_2$+2CuO was screen printed on $Y_2BaCuO_5$(d=15mm). And critical current densities of the thick films were observed as the sintering temperature(92$0^{\circ}C$~95$0^{\circ}C$) and holding time(2h~10h). Based on experimental data, the thick films for superconducting FCL were sintered at $940^{\circ}C$ in 2 hours. The superconducting FCL with a current limiting area of 1mm wide and 66mm long was prepared on $Y_2BaCuO_5$ substrate. To measure the characterization of the fabricated FCL, an alternating voltage (60Hz) was applied to the FCL in 77K liquid nitrogen. At an applied voltage of 4V, the FCL was limited from 20A into 0.6A not farther than 0.5ms.

• 한국분말재료학회지
• /
• 제17권6호
• /
• pp.494-498
• /
• 2010

The p-type thermoelectric compounds of $Bi_2Te_3$ based doped with 3wt% Te were fabricated by a combination of rapid solidification and spark plasma sintering (SPS) process. The effect of holding time during spark plasma sintering (SPS) on the microstructure and thermoelectric properties were investigated using scanning electron microscope (SEM), X-ray diffraction (XRD) and thermoelectric properties. The powders as solidified consisted of homogeneous thermoelectric phases. The thermoelectric figure of merit measured to be maximum ($3.41{\times}10^{-3}/K$) at the SPS temperature of $430^{\circ}C$.

• 한국주조공학회지
• /
• 제20권1호
• /
• pp.38-45
• /
• 2000

The remelting for recycling or thin aluminum scrap, such as aluminum chip generally involves melting of these pieces submerged in molten salt flux. In this study, the effects of salt flux compositions and alloying elements on the aluminum dropletscoalescence and oxide film removal were studied in 99.8%Al, Al-1.01%Cu, Al-1.03%Si, and Al-1.38%Mg alloys as a function of holding time at $740^{\circ}C$ Salt fluxes based on NaCl-KCl(1:1) with addition of 5wt.% fluorides(NaF, $Na_3AlF_6$, $CaF_2$) or 5 wt.% chloride($MgCl_2$, $AlCl_3$) were used. The experimental results show that NaCl-KCl(1:1) with addition of 5 wt.% fluorides exhibits better coalescence ability than that with chlorides. The oxide film is not removed by NaCl-KCl(1:1) with addition of 5 wt.%chlorides, while it is removed by NaCl-KCl(1:1) with addition of 5 wt.% fluorides. The aluminum droplets coalescence and oxide film removal by salt fluxes are related to interfacial tension tension between metal and salt flux.

• 한국주조공학회지
• /
• 제19권5호
• /
• pp.427-432
• /
• 1999

Most investment castings contain some porosities and microcavities. In this study, we investigated the elimination trends of various internal defects in IN738LC investment castings for industrial gas turbine blade by hot isostatic pressing. The results showed that cylindrical defects which are under $0.6mm{\Phi}{\times}7mm$ size are mostly eliminated and aspect ratio of defects is more sensitive factor than their cross section shape in removing these defects. Increasing hot isostatic pressure and holding time doesn't affect the elimination trend of cylindrical defects over $0.6mm{\Phi}{\times}7mm$ size because first step(plastic deformation) of HIP densification doesn't occur under these HIPping conditions.