• Title/Summary/Keyword: High-nitrogen steel

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The preparation of ultra hard nitrogenated DLC film by $N_2^+$ implantation

  • Olofinjana, A.O.;Chen, Z.;Bell, J.M.
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 2002.10b
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    • pp.165-166
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    • 2002
  • Hydrogen free diamond like carbon (DLC) films were prepared on steel substrates by using a single ion beam in a configuration that allowed sputtering of a graphite target and at the same time allowed to impact the substrate at a grazing angle. The DLC films so prepared have improved properties with increased disorder and with modest hardness that is slightly higher than previously reported values. We have studied the effects of $N_2^+$ ions implantation on such films. It is found that the implantations of nitrogen ions into DLC films lead to chemical modifications that allowed N atoms to be incorporated into the carbon network to produce a nitrogenated DLC. Nano-indentation experiments indicated that the nitrogenated films have consistently higher hardnesses ranging from 30 to 45GPa, which represents a considerable increase in surface hardness, compared with non-nitrogenated precursor films. The investigations by XPS and Raman spectroscopy suggests that the $N_2^+$ implanted DLCs had undergone both chemical and structural modifications through the incorporation of N atoms and the increased ratio of $sp^3/sp^2$ type bonding. The observed high hardness was therefore attributable to these structural and chemical modifications. This result has implication for the preparation of super hard wear resistant films required for tribological functions in devices.

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Atmospheric Micro Glow Plasma-jet Device (상압 마이크로 글로우 방전 분사 소자)

  • Kim, Kang-Il;Kim, Geun-Young;Hong, Yong-Cheol;Yang, Sang-Sik
    • Proceedings of the KIEE Conference
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    • 2009.07a
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    • pp.1533_1534
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    • 2009
  • This paper presents an atmospheric micro glow plasma-jet device. The device consists of four components; a thin Ni anode, a porous alumina insulater, a stainless steel cathode and an aluminum case. The Ni anode is fabricated using micromachining technology. The anode has 10 holes, of which the hole diameter and the depth are $250{\mu}m$ and $60{\mu}m$, respectively. The discharge test is performed in nitrogen gas at atmospheric pressure for 20 kHz AC bias. The breakdown voltage is 3.5 kV at gas flow rate of 4 L/min and the the plasma-jet is blown out to ambient at 5.5 kV. In order to verify the characteristics of plasma, the current and the voltage of device are measured. The maximum temperature of plasma is $37^{\circ}C$. The plasma is well generated and stable at high voltage.

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Characteristics of TiN Films by ion Beam Assisted Deposition (이온빔 보조 증착에 의한 TiN 박막의 특성)

  • Kim, Sang Hyun;Kim, Dae Hyeon
    • Journal of Korean Ophthalmic Optics Society
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    • v.9 no.1
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    • pp.161-166
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    • 2004
  • In this research, TiN films has been grown to the stainless steel substrate by ion beam assisted deposition. TiN film was grown to the nitrogen atmosphere of around $10^{-15}$ Torr with Arion bombardment. The chemical composition, color and adhesion of TiN films were examined as a variation of En(ion energy per atom). The N/Ti ratio increased linearly as the increase of En and saturated around 1.2 at high En. As a results, the bright golden color was obtained when En reached a certain value of Ecn. As a results, the N/Ti ratio is about 0.9.

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Effect of Reuse of Onggi Containers on the Quality of Anchovy Soy Sauce (옹기의 재 사용이 어간장의 품질에 미치는 영향)

  • Chung, Sun-Kyung;Choi, Dong-Man;Joung, Yong-Myeon;Shin, Dong-Ju
    • Food Science and Preservation
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    • v.17 no.2
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    • pp.223-229
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    • 2010
  • Anchovy soy sauce was fermented at ambient temperature in 20 L new Onggi, used Onggi, stainless steel, and plastic containers, and sauce quality was analyzed. Microporous insulated Onggi containers were found to promote fermentative microbial growth, thus creating desirable conditions for the preparation of good-quality anchovy soy sauce. The use of used Onggi containers yielded an anchovy soy sauce with high contents of total nitrogen and free amino acids, which afforded good sensory qualities with respect to odor, taste, and overall acceptability.

Effects of Nitrogen Gas Ratio on Nitride Layer and Microhardness of Tool Steel(SKH51) in Plasma Nitriding (플라즈마질화시 방전가스중 질소가스의 비율이 공구강(SKH51)의 질화층 및 미소경도에 미치는 영향)

  • Kim, Deok-Jae;Lee, Hae-Ryong;Gwak, Jong-Gu;Jeong, U-Chang;Jo, Yeong-Rae
    • Korean Journal of Materials Research
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    • v.12 no.6
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    • pp.447-451
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    • 2002
  • Pulsed DC-plasma nitriding has been applied to form nitride layer having only a diffusion layer. The discharge current with the variation of discharge gases is proportional to the intensity of $N_2^+$ peak in optical emission spectroscopy during the plasma nitriding. The discharge current, microhardness in surface of substrate and depth of nitride layer increased with the ratio of $N_2\;to\;H_2$ gas in discharge gases. When the ratio of $N_2\;to\;H_2$ is lower than 60% in the discharge gases, high microhardness value of 1100Hv nitride layer which contains no compound layer has been formed.

Test Results of a Three Phase 10㎸A HTS Transformer With Double Pan Cake Coils (3상 10kVA 더블 팬케익 코일형 고온초전도 변압기 특성시험 결과)

  • 이승욱;이희준;차귀수;이지광;최경달;류경우;한송엽
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.52 no.3
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    • pp.101-106
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    • 2003
  • The high temperature superconductor transformers gain interests from the industries. This paper described construction and test results of 10㎸A HTS transformer Three phase transformer with double pancake windings were constructed. To reduce the leakage magnetic field, secondary coil were placed between the two primary coils. BSCCO-2223 wire. silicon sheet steel core and FRP cryostats were used to construct the transformer. Three coils were stacked in one cryostat. Two double pancake coils were connected in series for the primary coil and one double pancake coil was used for the secondary coil. Total number of turns of the primary winding and the secondary winding were 112turns and 98urns, respectively, The rated voltages of each winding were 440/220V. The rated currents of each winding were 13.1/26.2A. After the tests of basic properties of the three phase HTS transformer using no-load test, short-circuit test and full-load test, continuous operation of 100 hours with pure resistive load has been carried out. Test results proved over-load capability and reliability of the HTS transformer.

Fabrication and Characteristic Tests of a 1 MVA Single Phase HTS Transformer with Concentrically Arranged Windings

  • Kim, S.H.;Kim, W.S.;Choi, K.D.;Joo, H.G.;Hong, G.W.;Han, J.H.;Lee, H.G.;Park, J.H.;Song, H.S.
    • Progress in Superconductivity and Cryogenics
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    • v.6 no.4
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    • pp.37-40
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    • 2004
  • A 1 MV A single phase high temperature superconducting (HTS) transformer was manufactured and tested. The rated voltages of primary and secondary of the HTS transformer are 22.9 kV and 6.6 kV respectively. BSCCO-2223 HTS tape was used for HTS windings of 1 MV A HTS transformer. In order to reduce AC loss generated in the HTS winding, the type of concentric arrangement winding was adopted to a 1 MV A HTS transformer. Single HTS tape for primary windings and 4 parallel HTS tapes for secondary windings were used considering the each rated current of the HTS transformer. A core of HTS transformer was fabricated as a shell type core made of laminated silicon steel plate. And a GFRP cryostat with a room temperature bore was also manufactured. The characteristic tests of 1 MV A HTS transformer were performed such as no load test, short circuit test and several insulation tests at 65 K using sub-cooled liquid nitrogen. From the results of tests, the validity of design of HTS transformer was ascertained.

Hybrid Welding Process for Sheet Metal and Narrow Gap Fill Pass (하이브리드 용접방식을 이용한 박판 및 후판용접공정)

  • Choi, Hae-Woon;Shin, Hyun-Myung;Im, Moon-Hyuk
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.11
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    • pp.978-983
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    • 2008
  • An application of innovative laser+GMA hybrid welding process is presented for reducing bead humping defects in high speed welding and increasing side wall fusion in narrow groove welding without torch or wire oscillation. In this hybrid process, the laser heat input is applied adjacent to the weld pool at a relatively low power density to produce a wider, flatter weld bead. In bead on plate in sheet metal gauges, the hybrid process was able to produce hump-free welds from 70ipm (${\sim}1780mm/min$) to over 150ipm (${\sim}3810mm/min$) of the travel speed compared to the un-assisted GMAW process. A square-butt joint in 15mm A572 Gr50 steel welds was investigated. A square butt joint with a gap of 3.2mm was filled with 6 passes. Liquid Nitrogen calorimetry and innovative $CO_2$ laser reflective optics were also developed to demonstrate the concept of hybrid welding.

Analysis of Over-current Characteristics in YBCO Coated Conductor (YBCO Coated Conductor의 과전류 특성해석)

  • Lee, C.;Nam, K.;Kang, H.;Ko, T.K.;Seok, B.Y.
    • Proceedings of the KIEE Conference
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    • 2006.07b
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    • pp.693-694
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    • 2006
  • In order to develop a high temperature superconducting(HTS) coil for the fault current limiter(FCL), the over-current characteristics in YBCO coated conductor(CC) with Ni-W alloy substrate are analyzed. The HTS wire is wound by bifilar winding method for resistive current limitation and it is operated in 65K sub-cooled nitrogen. In order to analyze the resistance and the temperature characteristics of the CC wire, an analysis program is developed considering all the composition materials except the buffer layer. Using this program, the temperature rise, the resistance development and the current limitation of CC are calculated depending on the applied voltage and the stabilizer materials. According to the analysis results, under the temperature restriction of 300K, the maximum voltage per meter is determined as 40V/m if the stabilizer is $25{\mu}m$ thick stainless steel at each side. Finally, the wire length needed for the distribution level HTS FCL is estimated.

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Synthesis and Lubricant Properties of Nitrogen doped Amorphous Carbon (a-C:N) Thin Films by Closed-field unbalanced Magnetron Sputtering Method (비대칭 마그네트론 스퍼터링법에 의한 비정질 질화탄소 박막의 합성 및 윤활 특성)

  • Park, Yong-Seob;Cho, Hyung-Jun;Choi, Won-Seok;Hong, Byung-You
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.20 no.8
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    • pp.701-705
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    • 2007
  • The incorporation of N in a-C film is able to improve the friction coefficient and the adhesion to various substrates. In this study, a-C:N films were deposited on Si and steel substrates by closed-field unbalanced magnetron (CFUBM) sputtering system in $Ar/N_2$ plasma. The lubricant characteristics was investigated for a-C:N deposited with total working pressure from 4 to 7 mTorr. We obtained high hardness up to 24GPa, friction coefficient lower than 0.1 and the smooth surface of having the extremely low roughness (0.16 nm). The physcial properties of a-C:N thin film are related to the increase of cross-linked $sp^2$ bonding clusters in the film. However, the decrease of hardness, elastic modulus and the increase of surface roughness, friction coefficient with the increase of $N_2$ partial pressrue might be due to the effect of energetic ions as a result of the increase of ion bombardment with the increase of ion density in the plasma.