• 제목/요약/키워드: High-Nitrogen Steel

검색결과 143건 처리시간 0.027초

The preparation of ultra hard nitrogenated DLC film by $N_2^+$ implantation

  • Olofinjana, A.O.;Chen, Z.;Bell, J.M.
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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    • pp.165-166
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    • 2002
  • Hydrogen free diamond like carbon (DLC) films were prepared on steel substrates by using a single ion beam in a configuration that allowed sputtering of a graphite target and at the same time allowed to impact the substrate at a grazing angle. The DLC films so prepared have improved properties with increased disorder and with modest hardness that is slightly higher than previously reported values. We have studied the effects of $N_2^+$ ions implantation on such films. It is found that the implantations of nitrogen ions into DLC films lead to chemical modifications that allowed N atoms to be incorporated into the carbon network to produce a nitrogenated DLC. Nano-indentation experiments indicated that the nitrogenated films have consistently higher hardnesses ranging from 30 to 45GPa, which represents a considerable increase in surface hardness, compared with non-nitrogenated precursor films. The investigations by XPS and Raman spectroscopy suggests that the $N_2^+$ implanted DLCs had undergone both chemical and structural modifications through the incorporation of N atoms and the increased ratio of $sp^3/sp^2$ type bonding. The observed high hardness was therefore attributable to these structural and chemical modifications. This result has implication for the preparation of super hard wear resistant films required for tribological functions in devices.

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상압 마이크로 글로우 방전 분사 소자 (Atmospheric Micro Glow Plasma-jet Device)

  • 김강일;홍용철;김근영;양상식
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2009년도 제40회 하계학술대회
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    • pp.1533_1534
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    • 2009
  • This paper presents an atmospheric micro glow plasma-jet device. The device consists of four components; a thin Ni anode, a porous alumina insulater, a stainless steel cathode and an aluminum case. The Ni anode is fabricated using micromachining technology. The anode has 10 holes, of which the hole diameter and the depth are $250{\mu}m$ and $60{\mu}m$, respectively. The discharge test is performed in nitrogen gas at atmospheric pressure for 20 kHz AC bias. The breakdown voltage is 3.5 kV at gas flow rate of 4 L/min and the the plasma-jet is blown out to ambient at 5.5 kV. In order to verify the characteristics of plasma, the current and the voltage of device are measured. The maximum temperature of plasma is $37^{\circ}C$. The plasma is well generated and stable at high voltage.

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이온빔 보조 증착에 의한 TiN 박막의 특성 (Characteristics of TiN Films by ion Beam Assisted Deposition)

  • 김상현;김대현
    • 한국안광학회지
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    • 제9권1호
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    • pp.161-166
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    • 2004
  • 본 연구에서는 이온빔 증착방법을 사용하여 스테인레스 스틸 기판 위에 TiN 박막을 성장하였다. $10^{-5}$ Torr의 질소 분위기에서 아르곤 가스를 보조 이온빔으로 사용하여 TiN 박막을 성장하였다. TiN 박막의 화학 조성, 색상, 밀착력 등을 En의(원자당 이용에너지) 변화에 따라서 측정하였다. En이 증가 할 때 질소와 Ti의 비율은 선형적으로 변화 하였고, 높은 En의 경우에는 질소와 Ti의 비율은 1.2를 가지며 포화되었다. 밝은 금색은 En이 어떤 임계값(Ecn)에 도달 하였을 때 얻어졌다. 이때의 질소와 Ti의 비율은 0.9 이다.

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옹기의 재 사용이 어간장의 품질에 미치는 영향 (Effect of Reuse of Onggi Containers on the Quality of Anchovy Soy Sauce)

  • 정순경;최동만;정용면;신동주
    • 한국식품저장유통학회지
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    • 제17권2호
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    • pp.223-229
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    • 2010
  • 20 L 부피의 발효용기에서 어간장을 발효하면서 용기의 내부 온도 변화와 염도, pH, 산도, 총질소, 유리아미노산, 미생물 변화를 분석하였고 4개월 발효후의 어간장의 관능적 품질을 평가하였다. 발효용기로는 새 옹기와 재사용한 옹기, 스테인레스, 플라스틱 용기를 사용하였고 발효숙성은 외기조건에서 이루어졌다. 옹기가 가지는 통기성 및 보온성으로 인하여 발효 중 관여하는 미생물의 생육환경을 적절하게 조성하여 여러 가지 품질에 긍정적인 영향을 미치는 것을 확인할 수 있었다. 특히 옹기는 새 것보다는 재사용한 옹기에서 제품의 발효에 좋은 영향을 미쳐서, 높은 총질소, 유리아미노산함량, 향, 맛 전체적인 수용도의 관능적 품질을 보여주었다.

플라즈마질화시 방전가스중 질소가스의 비율이 공구강(SKH51)의 질화층 및 미소경도에 미치는 영향 (Effects of Nitrogen Gas Ratio on Nitride Layer and Microhardness of Tool Steel(SKH51) in Plasma Nitriding)

  • 김덕재;이해룡;곽종구;정우창;조영래
    • 한국재료학회지
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    • 제12권6호
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    • pp.447-451
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    • 2002
  • Pulsed DC-plasma nitriding has been applied to form nitride layer having only a diffusion layer. The discharge current with the variation of discharge gases is proportional to the intensity of $N_2^+$ peak in optical emission spectroscopy during the plasma nitriding. The discharge current, microhardness in surface of substrate and depth of nitride layer increased with the ratio of $N_2\;to\;H_2$ gas in discharge gases. When the ratio of $N_2\;to\;H_2$ is lower than 60% in the discharge gases, high microhardness value of 1100Hv nitride layer which contains no compound layer has been formed.

3상 10kVA 더블 팬케익 코일형 고온초전도 변압기 특성시험 결과 (Test Results of a Three Phase 10㎸A HTS Transformer With Double Pan Cake Coils)

  • 이승욱;이희준;차귀수;이지광;최경달;류경우;한송엽
    • 대한전기학회논문지:전기기기및에너지변환시스템부문B
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    • 제52권3호
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    • pp.101-106
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    • 2003
  • The high temperature superconductor transformers gain interests from the industries. This paper described construction and test results of 10㎸A HTS transformer Three phase transformer with double pancake windings were constructed. To reduce the leakage magnetic field, secondary coil were placed between the two primary coils. BSCCO-2223 wire. silicon sheet steel core and FRP cryostats were used to construct the transformer. Three coils were stacked in one cryostat. Two double pancake coils were connected in series for the primary coil and one double pancake coil was used for the secondary coil. Total number of turns of the primary winding and the secondary winding were 112turns and 98urns, respectively, The rated voltages of each winding were 440/220V. The rated currents of each winding were 13.1/26.2A. After the tests of basic properties of the three phase HTS transformer using no-load test, short-circuit test and full-load test, continuous operation of 100 hours with pure resistive load has been carried out. Test results proved over-load capability and reliability of the HTS transformer.

Fabrication and Characteristic Tests of a 1 MVA Single Phase HTS Transformer with Concentrically Arranged Windings

  • Kim, S.H.;Kim, W.S.;Choi, K.D.;Joo, H.G.;Hong, G.W.;Han, J.H.;Lee, H.G.;Park, J.H.;Song, H.S.
    • 한국초전도ㆍ저온공학회논문지
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    • 제6권4호
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    • pp.37-40
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    • 2004
  • A 1 MV A single phase high temperature superconducting (HTS) transformer was manufactured and tested. The rated voltages of primary and secondary of the HTS transformer are 22.9 kV and 6.6 kV respectively. BSCCO-2223 HTS tape was used for HTS windings of 1 MV A HTS transformer. In order to reduce AC loss generated in the HTS winding, the type of concentric arrangement winding was adopted to a 1 MV A HTS transformer. Single HTS tape for primary windings and 4 parallel HTS tapes for secondary windings were used considering the each rated current of the HTS transformer. A core of HTS transformer was fabricated as a shell type core made of laminated silicon steel plate. And a GFRP cryostat with a room temperature bore was also manufactured. The characteristic tests of 1 MV A HTS transformer were performed such as no load test, short circuit test and several insulation tests at 65 K using sub-cooled liquid nitrogen. From the results of tests, the validity of design of HTS transformer was ascertained.

하이브리드 용접방식을 이용한 박판 및 후판용접공정 (Hybrid Welding Process for Sheet Metal and Narrow Gap Fill Pass)

  • 최해운;신현명;임문혁
    • 대한기계학회논문집A
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    • 제32권11호
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    • pp.978-983
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    • 2008
  • An application of innovative laser+GMA hybrid welding process is presented for reducing bead humping defects in high speed welding and increasing side wall fusion in narrow groove welding without torch or wire oscillation. In this hybrid process, the laser heat input is applied adjacent to the weld pool at a relatively low power density to produce a wider, flatter weld bead. In bead on plate in sheet metal gauges, the hybrid process was able to produce hump-free welds from 70ipm (${\sim}1780mm/min$) to over 150ipm (${\sim}3810mm/min$) of the travel speed compared to the un-assisted GMAW process. A square-butt joint in 15mm A572 Gr50 steel welds was investigated. A square butt joint with a gap of 3.2mm was filled with 6 passes. Liquid Nitrogen calorimetry and innovative $CO_2$ laser reflective optics were also developed to demonstrate the concept of hybrid welding.

YBCO Coated Conductor의 과전류 특성해석 (Analysis of Over-current Characteristics in YBCO Coated Conductor)

  • 이찬주;남관우;강형구;고태국;석복렬
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2006년도 제37회 하계학술대회 논문집 B
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    • pp.693-694
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    • 2006
  • In order to develop a high temperature superconducting(HTS) coil for the fault current limiter(FCL), the over-current characteristics in YBCO coated conductor(CC) with Ni-W alloy substrate are analyzed. The HTS wire is wound by bifilar winding method for resistive current limitation and it is operated in 65K sub-cooled nitrogen. In order to analyze the resistance and the temperature characteristics of the CC wire, an analysis program is developed considering all the composition materials except the buffer layer. Using this program, the temperature rise, the resistance development and the current limitation of CC are calculated depending on the applied voltage and the stabilizer materials. According to the analysis results, under the temperature restriction of 300K, the maximum voltage per meter is determined as 40V/m if the stabilizer is $25{\mu}m$ thick stainless steel at each side. Finally, the wire length needed for the distribution level HTS FCL is estimated.

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비대칭 마그네트론 스퍼터링법에 의한 비정질 질화탄소 박막의 합성 및 윤활 특성 (Synthesis and Lubricant Properties of Nitrogen doped Amorphous Carbon (a-C:N) Thin Films by Closed-field unbalanced Magnetron Sputtering Method)

  • 박용섭;조형준;최원석;홍병유
    • 한국전기전자재료학회논문지
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    • 제20권8호
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    • pp.701-705
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    • 2007
  • The incorporation of N in a-C film is able to improve the friction coefficient and the adhesion to various substrates. In this study, a-C:N films were deposited on Si and steel substrates by closed-field unbalanced magnetron (CFUBM) sputtering system in $Ar/N_2$ plasma. The lubricant characteristics was investigated for a-C:N deposited with total working pressure from 4 to 7 mTorr. We obtained high hardness up to 24GPa, friction coefficient lower than 0.1 and the smooth surface of having the extremely low roughness (0.16 nm). The physcial properties of a-C:N thin film are related to the increase of cross-linked $sp^2$ bonding clusters in the film. However, the decrease of hardness, elastic modulus and the increase of surface roughness, friction coefficient with the increase of $N_2$ partial pressrue might be due to the effect of energetic ions as a result of the increase of ion bombardment with the increase of ion density in the plasma.