• Composites Research
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• v.33 no.6
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• pp.395-400
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• 2020

In this paper, we manufactured silsesquiaznae (SSQZ)-coated carbon nanotube (CNT) surface heating elements, which allowed stable heating at high temperatures. The prepared composite sheet was confirmed by FE-SEM that the SSQZ fully coated the surface of CNT sheet. Furthermore, it was also confirmed that the silicon carbonitride (SiCN) ceramic formed by heat treatment of 800℃ have no defects found and maintain intact structure. The CNT/SiCN composite sheet was able to achieve higher thermal stability than raw CNT sheets in both nitrogen and air atmosphere. Finally, the CNT/SiCN composite sheet was possible to heat up at a temperature of over 700℃ in the atmosphere, and the re-heating was successfully operated after cooling.

• Composites Research
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• v.29 no.3
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• pp.111-116
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• 2016

The tilting pad journal bearing for the turbo compressor application has a role to support high speed and heavy loading rotor. White metal has been widely used for the bearing material but the conventional bearing is immediately suspended and induces serious serious damage to the rotor under the unexpected oil cut situation or the insufficient oil film formation. The carbon fiber reinforced composite having high specific stiffness, specific strength and excellent tribological characteristics can solve these seizure problems. In this work, the study on the durability of high thermal resistance carbon fiber/epoxy composite tilting pad journal bearing under oil cut situation was conducted. The material properties of the composite materials including tensile, compressive and interlaminar properties were measured at room and high temperature of oil cut situation. To investigate the possibility of failure of composite tilting pad journal bearing under oil cut situation, the stress distribution of the composite bearing was analyzed via finite element analysis and the Tsai-Wu Failure index was calculated. To verify the failure analysis results, the oil cut tests for the composite tilting pad journal bearing were conducted using industrial test bench.

• Composites Research
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• v.30 no.6
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• pp.422-428
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• 2017

The moisture absorption behavior, tensile properties, and thermal analysis properties of MWCNT embedded nanocomposites exposed to temperature and moisture were evaluated. The contents of MWCNT were 0 wt%, 1 wt%, and 2 wt%, respectively. The specimens were exposed to immersed conditions at $25^{\circ}C$ and $75^{\circ}C$ for up to 600 hours. According to the results, the apparent moisture content increased as the exposure time increased, but the difference between the maximum moisture content and the moisture content at 600 hours was almost constant. The tensile modulus decreased with increasing exposure time and the degree of decrease was increased significantly as the MWCNT content and exposure temperature increased. The tensile strength decreased with longer exposure time without MWCNT, but increased with MWCNT due to the reinforcing effect of MWCNT. The storage modulus, glass transition temperature, tan d peak magnitude were low as the exposure time increased, but tan d curves with two peaks appeared when exposed to high exposure temperature for more than 300 hours.

• Journal of Powder Materials
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• v.18 no.3
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• pp.290-296
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• 2011

Titanium carbonitride is more perspective materials compared to titanium carbide. It can be used in tool industry and special products because of its higher strength, abrasive wear-resistance and especially its strong chemical stability at high temperatures. We produced STS+TiCxNy composite by the spark plasma sintering for higher strength and studied the characteristics. The planar and cross-sectional microstructures of the specimens were observed by scanning electron microscopy. Characterizations of the carbon and nitride phases on the surface of composite were carried out using an X-ray diffractometer. During annealing TiCxNy particles diffusion into STS 430 was observed. After annealing, sintering isolations between particles were formed. It causes decreasing of mechanical strength. In addition when annealing temperature was increased hardness increased. Heterogeneous distribution of alloying elements particles was observed. After annealing composites, highest value of hardness was 738.1 MHV.

• Bulletin of the Korean Chemical Society
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• v.33 no.11
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• pp.3706-3710
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• 2012

A novel silicon-containing arylacetylene resin (MSAR) modified by dipropargyl ether of bisphenol A (DPBPA) and dipropargyl ether of perfluorobisphenol A (DPPFBPA) was prepared separately. The curing behaviors of modified resins, DPBPA/MSAR and DPPFBPA/MSAR, were characterized with differential scanning calorimeter (DSC). The kinetic parameters of modified resins were obtained by the Kissinger and Ozawa methods. The results of dynamic mechanical analysis (DMA) revealed that the glass transition temperature ($T_g$) of the cured DPBPA/MSAR reached $486^{\circ}C$. According to the thermogravimetric analysis (TGA), the decomposition temperature ($T_{d5}$) of the cured resins and char yield ($Y_c$, $800^{\circ}C$) decreased as the dipropargyl ether loadings increased, especially in air. With the same weight loading, thermal stability of DPBPA/MSAR was better than that of DPPFBPA/MSAR. The carbon fiber (T300) reinforced composites exhibited excellent flexural properties at room temperature with a high property retention at $300^{\circ}C$.

• Composites Research
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• v.30 no.2
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• pp.116-125
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• 2017

The purpose of this study is to develop silicon carbide fiber showing an excellent mechanical properties under highly oxidative conditions at high temperature. Polycarbosilane(PCS) as a preceramic precursor was used for making the SiC fiber. PCS fiber was taken by melt spinning method followed by melting the PCS at $300{\sim}350^{\circ}C$ in N2 gas. The Curing of PCS fiber was carried out in air oxygen chamber, prior to high temperature pyrolysis. Degree of cure was calculated by characteristic peak's ratio of Si-H to $Si-CH_3$ in FT-IR spectra before and after curing of PCS fiber. The properties of SiC fiber was affected greatly by the degree of cure. The SiC fiber produced by controlling fiber tension during heat treatment showed good properties. The SiC fiber exposed to $1000^{\circ}C$ at air from 1 min. up to maximum 50 hrs showed around 60% reduction in tensile strength. We found that large amount of carbon content on the fiber surface after long-term exposure has resulted in lower tensile strength.

• Composites Research
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• v.30 no.2
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• pp.132-137
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• 2017

The purpose of this paper is to investigate failure characteristics of Carbon/BMI-Nomex honeycomb sandwich on design parameters. A total of 6 types sandwich specimens were manufactured according to core height, face thickness and density, and environmental condition were applied to evaluate temperature and humidity effects of one of these specimens. The test results show that the core shear buckling loads was commonly observed in all specimens except for the joint with density of $64kg/m^3$. After core shear buckling, however, the joint carried additional loads over the buckling loads and then finally failed in the upper face and lower face at the same time. In the case of specimen having high stiffness, the maximum failure load was low due to interfacial failure of the upper face and core without initial core shear buckling. The ETW1 and ETW2 conditions, which were carried out to evaluate the environmental condition of the sandwich specimen, show an initial failure mode which was significantly different from RTD condition. Also, the ETW2 condition with increased temperature under the same humidity shows that the core shear buckling load was 18% less than ETW1 condition.

• Composites Research
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• v.33 no.5
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• pp.275-281
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• 2020

The mechanical property related to lap shear strength of the joint structure between carbon fiber reinforced polymer (CFRP) composite and metal (Ni-Cr Alloy) under varying environmental conditions (temperature and humidity) was studied in order to apply to the aircraft fan blade. Room temperature dry (RTD), elevated temperature wet (ETW), and cold temperature dry (CTD) environmental conditions were chosen for investigation based on the flight conditions of aircraft. Lap shear strength tests were conducted according to ASTM Standard D3528 to evaluate the shear strength. The microstructure characteristic of failure zone was analyzed by SEM images to check the adhesive shear strength with the three environmental conditions. In comparison with shear strength for the RTD condition, the shear strength in the ETW condition was reduced by 72.8% while those for the CTD condition increased by 56.5%. The moisture absorption and high temperature in ETW condition strongly had an affect on mechanical property of adhesive, while cold temperature could enhance the adhesive shear strength due to the higher brittleness.

• Composites Research
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• v.30 no.4
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• pp.235-240
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• 2017

Animal glue, a water-soluble adhesive, has been used historically for high-performance traditional furniture despite the disadvantage of weakness against moisture. Many scientists studied the ways to improve water resistance of animal glue. Improvements on the interfacial, thermal, and water resistance properties of wood sandwich composites (WSC) was studied with carbon nanotube (CNT) wt% in animal glue. Real-time temperature of WSC was measured after WSC was heated with increasing CNT wt%. Lap shear test was performed to determine the interfacial properties of wood and animal glue with CNTs. Water resistance properties of animal glue were determined by lap shear test using specimens dipped in water and the results were compared with the dry case. Hydrophobicity of animal glue by static contact angle was correlated with the variation of lap shear test. Interfacial, thermal, and water resistance properties for animal glue were improved with properly added CNTs.

• Journal of the Microelectronics and Packaging Society
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• v.28 no.1
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• pp.67-71
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• 2021

In this study, graphene layer was grown on metal microwire using chemical vapor deposition. The difference of carbon solubility between copper and nickel resulted in the formation of mono-layer and multi-layer graphene were formed on the surfaces of copper and nickel microwires, respectively. During the growth of graphene at high temperature, copper and nickel were recrytallized and the grain size increased. The ampacity of graphene/copper microwire was improved by approximately 27%, 1.91×105 A/㎠, compared to pristine copper microwire. Similar to this behavior, the ampacity of multilayer graphene/nickel microwire was 4.41×104 A/㎠ which is about about 36% improved compared to the pure nickel microwire. The excellent electrical properties of graphene/metal composites are beneficial for supplying the electrical energy to the high-power electronic devices and equipment.