• Title/Summary/Keyword: High shear rate

Search Result 352, Processing Time 0.031 seconds

Thermal Decomposition and Mechanical Properties of Polycarbonate/ABS Blends Prepared by High Shear Rate Processing (고속전단에 의한 폴리카보네이트/ABS 블렌드의 열분해 및 기계적 특성 연구)

  • Yoo, Jae Jung;Yong, Da Kyoung;Lee, Han Ki;Kim, Dae Sik;Lee, Hyung Il;Kim, Sun Hong;Lee, Kee Yoon;Lee, Seung Goo
    • Polymer(Korea)
    • /
    • v.38 no.4
    • /
    • pp.471-476
    • /
    • 2014
  • Polycarbonate (PC) and acrylonitrile-butadiene-styrene (ABS) blends were prepared using a high shear extruder to investigate their thermal decomposition and mechanical properties with shear rate and shear time. In this experiment, high shear rate, from 1000 to 3000 rpm, in blending process was applied for 10 to 40 sec, respectively. At high shear rate over than 2000 rpm, the initial decomposition temperature was dropped significantly compared to a compounded sample because of thermal decomposition of the blend by high shear. Consequently, high shear processing gave an important effect on the mechanical and thermal properties of the PC/ABS blend. In particular, elongation of the blend decreased significantly with shear rate.

Experimental study on the shear thinning effects of viscosity index improver added lubricant by in-situ optical viscometer

  • Jang, Siyonl
    • Korea-Australia Rheology Journal
    • /
    • v.15 no.3
    • /
    • pp.117-124
    • /
    • 2003
  • Elastohydrodynamic lubrication (EHL) film is measured under the condition of viscosity index improver added to base oil. In-situ optical contact method using the interference principle make the measuring resolution of ~5 nm possible and enables the measuring range all over the contact area of up to ~300 $\mu\textrm{m}$ diameter. What is more important to the developed method by the author is that the measurement of EHL film thickness is possible in the range from 100 nm to 2 $\mu\textrm{m}$, which is the regime of worst contact failures in precision machinery. Viscosity index improver (VII) is one of the major additives to the modem multigrade lubricants for the viscosity stability against temperature rise. However, it causes shear thinning effects which make the film thickness lessened very delicately at high shear rate (over $10^5 s^{-1}$) of general EHL contact regime. In order to exactly verify the VIIs performance of viscosity stability at such high shear rate, it is necessary to make the measurement of EHL film thickness down to ~100 nm with fine resolution for the preliminary study of viscosity control. In this work, EHL film thickness of VII added lubricant is measured with the resolution of ~5 nm, which will give very informative design tool for the synthesis of lubricants regarding the matter of load carrying capacity at high shear rate condition.

Rheological Characterization of Hydrogen Peroxide Gel Propellant

  • Jyoti, B.V.S.;Baek, Seung Wook
    • International Journal of Aeronautical and Space Sciences
    • /
    • v.15 no.2
    • /
    • pp.199-204
    • /
    • 2014
  • An experimental investigation on the rheological behavior of gelled hydrogen peroxide at different ambient temperature (283.15, 293.15 and 303.15 K) was carried out in this study. The gel propellant was rheologically characterized using a rheometer, in the shear rate ranges of 1 to $20s^{-1}$, and 1 to $1000s^{-1}$. Hydrogen peroxide gel was found to be thixotropic in nature. The apparent viscosity value with some yield stress (in-case of shear rate 1 to $20s^{-1}$) drastically fell with the shear rate. In the case of the shear rate range of 1 to $20s^{-1}$, the apparent viscosity and yield stress of gel were significantly reduced at higher ambient temperatures. In the case of the shear rate range of 1 to $1000s^{-1}$, no significant effect of varying the ambient temperature on the gel apparent viscosity was observed. The up and down shear rate curves for hydrogen peroxide gel formed a hysteresis loop that showed no significant change with variation in temperature for both the 1 to $20s^{-1}$ and the 1 to $1000s^{-1}$ shear rate ranges. No significant change in the thixotropic index of gel was observed for different ambient temperatures, for both low and high shear rates. The gel in the 1 to $20s^{-1}$ shear rate range did not lead to a complete breakdown of gel structure, in comparison to that in the 1 to $1000s^{-1}$ shear rate range.

Effects of the High Shear Rate Processing on the Thermal Properties of PC/ABS Blends (고속 전단 가공에 의한 PC/ABS 블렌드의 열적 물성 변화 연구)

  • Lee, Hyeong Il;Lee, Han Ki;Kim, Dea Sik;Choi, Seok Jin;Kim, Seon Hong;Yoo, Jea Jung;Yong, Da Kyoung;Lee, Seung Goo;Lee, Kee Yoon
    • Polymer(Korea)
    • /
    • v.38 no.3
    • /
    • pp.320-326
    • /
    • 2014
  • The effects of high shear rate processing on the thermal properties of PC/ABS blends were studied. It was executed by the high shear processing machine (NHSS2-28) at the varied conditions of screw speeds and loaded duration. After the samples were processed with NHSS2-28, the $T_gs$ were shifted from 143 to $133^{\circ}C$, and the behavior of degradation determined by TGA showed two distinct steps before high shear rate processing, while it showed a straight line after the processing. In order to provide the reasons of the properties, it was showen by SEM and UTM that the droplet sizes morphologically decreased after the processing, and the elongations decreased slightly until 1000 rpm of screw speed and then sharply decreased, according to the conditions of high shear rate processing. Therefore, it can be confirmed that $T_g,s$ of PC/ABS blends were considerably shifted under an appropriate high shear rate condition, and rapidly dropped, so that blends degraded above the condition, due to stress-induced degradation.

High Strain-rate Deformation Behavior of NiAl/Ni Micro-laminated Composites (NiAl/Ni 미세적층복합재료의 고속변형거동)

  • Kim Hee-Yeoun;Kim Jin-Young;Jeong Dong-Seok;Enoki Manabu;Hong Soon-Hyung
    • Proceedings of the Korean Society For Composite Materials Conference
    • /
    • 2004.04a
    • /
    • pp.237-240
    • /
    • 2004
  • High strain-rate deformation behavior of NiAl/Ni micro-laminated composites was characterized by split hopkins on pressure bar(SHPB). When the strain rate increased, the compressive stress of micro-laminated composites were increased a little. When the intermetallic volume fraction increased, the compressive stress of micro-laminated composites increased linearly irrespective of strain rate. Absorbed energy during the quasi-static and SHPB tests was calculated from the integrated area of stress-strain curve. Absorbed energy of micro-laminated composites deviated from the linearity in terms of the intermetallic volume fraction but merged to the value of intermetallic as the strain rate increased. This was due to high tendency of intermetallic layer for the localization of shear deformation at high strain rate. Microstructure showing adibatic shear band(ASB) confirmed that the shear strain calculated from the misalignment angle of each layer increased and ASB width decreased when the intermetallic volume fraction. Simulation test impacted by tungsten heavy alloy cylinder resulted that the absorbed energies multiplied by damaged volume of micro-laminated composites were decreased as the intermetallic volume fraction increased. Fracture mode were changed from delamination to single fracture when the intermetallic volume fraction and this results were good matched with previous results[l] obtained from the fracture tests.

  • PDF

Rheological Properties and Particle Size Distribution of Northeast Mixed Hardwood for Enzymatic Saccharification Processing with High Substrates Loading

  • Um, Byung-Hwan
    • Journal of the Korean Wood Science and Technology
    • /
    • v.36 no.5
    • /
    • pp.56-65
    • /
    • 2008
  • In this paper experimental results are presented for the rheological behavior of high-solids saccharification of mixed northeast hardwood as a model feedstock. The experimental determination of the viscosity, shear stress, and shear rate relationships of the 10 to 20 percent slurry concentrations with constant enzyme concentrations were performed under variable rotational speed of a viscometer (2.0 to 200 RPM) at combined temperatures (50 to $30^{\circ}C$) for the initial four hours. The viscosities of saccharification slurries observed were in the ranges of 0.024 to 0.028, 0.401 to 0.058, and 0.840 to 0.087 Pa s for shear rates up to 100 reciprocal seconds at 10, 15, and 20 percent initial solids (w/v) respectively. The fluid behavior of the suspensions was modeled using the power-law, the Herschel-Bulkley, the Casson, and the Bingham model. The results showed that broth slurries were pseudoplastic with a yield stress. The model slope increased and the model intercept decreased with increasing fermentation time at shear rates normal for the fermentor. The broth slurries exhibited Newtonian behavior at high and low shear rates during initial saccharification process. The solid particle size ranged from 57.8 to $70.0{\mu}m$ for $40^{\circ}C$ and from 44.0 to 57.5 11m for combined temperatures at 10, 15, and 20 percent initial solids (w/v) respectively.

Freeze Casting of Aqueous Alumina/Silicon Carbide Slurries and Fabrication of Layered Composites: (I) Dispersion and Rheology of Slurries (수성 알루미나/탄화규소 슬러리의 동결주조와 층상복합체의 제조: (I) 슬러리의 분산과 유동성)

  • Yang, Tae-Young;Cho, Yong-Ki;Kim, Young-Woo;Yoon, Seog-Young;Park, Hong-Chae
    • Journal of the Korean Ceramic Society
    • /
    • v.45 no.2
    • /
    • pp.99-104
    • /
    • 2008
  • Zeta potential, sedimentation bulk density and rheology in the dispersion system have been studied in terms of solid loading (40-55 vol%), and types of additives. Ammonium polymethacrylate, glycerol, ethoxylated acetylenic diol, and polyvinyl alcohol have been used as the dispersant, cryo-protectant, surfactant, and binder, respectively. Sedimentation density greatly increased upon adding dispersant; the effect was more pronounced with ionic alumina suspension compared with covalent silicon carbide. With further addition of cryo-protectant and surfactant to dispersant, the sedimentation density increased somewhat. The suspension viscosity generally behaviored in an opposite manner to the sedimentation density, i.e., high sedimentation gave low high-shear viscosity, indicative of low order structure formation in the suspended particles. Shear rate rheology in shear rate of $2-300\;sec^{-1}$ showed a shear thinning and its onset began at similar shear rate (${\sim}100\;sce^{-1}$), regardless of solid loading.

Tensile strength of unidirectional CFRP laminate under high strain rate

  • Taniguchi, Norihiko;Nishiwaki, Tsuyoshi;Kawada, Hiroyuki
    • Advanced Composite Materials
    • /
    • v.16 no.2
    • /
    • pp.167-180
    • /
    • 2007
  • The tensile strength of unidirectional carbon fiber reinforced plastics under a high strain rate was experimentally investigated. A high-strain-rate test was performed using the tension-type split Hopkinson bar technique. In order to obtain the tensile stress-strain relations, a special fixture was used for the impact tensile specimen. The experimental results demonstrated that the tensile modulus and strength in the longitudinal direction are independent of the strain rate. In contrast, the tensile properties in the transverse direction and the shear properties increase with the strain rate. Moreover, it was observed that the strain-rate dependence of the shear strength is much stronger than that of the transverse strength. The tensile strength of off-axis specimens was measured using an oblique tab, and the experimental results were compared with the tensile strength predicted based on the Tsai-Hill failure criterion. It was concluded that the tensile strength can be characterized quite well using the above failure criterion under dynamic loading conditions.

A Study on the Effect and Formation of Shear Lip for Al 2024-T3 Materials (Al 2024-T3재에 있어서 Shear Lip의 생성과 그 영향에 관한 연구)

  • 최병기;오환교
    • Journal of the Korean Society of Safety
    • /
    • v.8 no.4
    • /
    • pp.41-46
    • /
    • 1993
  • This Paper aims to examine the effect of shear lip formation from cross-sections on fatigue crack propagation rate in order to study the fatigue fracture behavior of the high strength aluminum material (Al 2024-T3). The following tests were achieved from this research. 1. As a result of depressing shear lip artificially by adding a side groove to a specimen, it is shown that the propagation rate of fatigue crack is faster than that of general specimen. 2. Through the two-step load test, the phenomenon that the shear lip decreases In the part of changed load gets observed. Consequently It Is shown that the crack propagation rate gets faster.

  • PDF

Effects of normal stress, shearing rate, PSD and sample size on behavior of ballast in direct shear tests using DEM simulation

  • Md Hussain;Syed Khaja Karimullah Hussaini
    • Geomechanics and Engineering
    • /
    • v.35 no.5
    • /
    • pp.475-486
    • /
    • 2023
  • Ballast particles have an irregular shape and are discrete in nature. Due to the discrete nature of ballast, it exhibits complex mechanical behaviour under loading conditions. The discrete element method (DEM) can model the behaviour of discrete particles under a multitude of loading conditions. DEM is used in this paper to simulate a series of three-dimensional direct shear tests in order to investigate the shear behaviour of railway ballast and its interaction at the microscopic level. Particle flow code in three dimension (PFC3D) models the irregular shape of ballast particles as clump particles. To investigate the influence of particle size distribution (PSD), real PSD of Indian railway ballast specification IRS:GE:1:2004, China high-speed rail (HSR) and French rail specifications are generated. PFC3D built-in linear contact model is used to simulate the interaction of ballast particles under various normal stresses, shearing rate and shear box sizes. The results indicate how shear resistance and volumetric changes in ballast assembly are affected by normal stress, shearing rate, PSD and shear box size. In addition to macroscopic behaviour, DEM represents the microscopic behaviour of ballast particles in the form of particle displacement at different stages of the shearing process.