• Title/Summary/Keyword: High Strength Nitrogen

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MICROSTRUCTURAL EVOLUTION OF A HIGH CR FE-BASED ODS ALLOY BY DIFFERENT COOLING RATES

  • Shen, Yin-Zhong;Cho, Hae-Dong;Jang, Jin-Sung
    • Nuclear Engineering and Technology
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    • v.40 no.2
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    • pp.99-106
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    • 2008
  • Through mechanical alloying, hot isostatic pressing and hot rolling, a 9%Cr Fe-based oxide dispersion-strengthened alloy sample was fabricated. The tensile strength of the alloy is significantly improved when the microstructure is modified during the post-consolidation process. The alloy samples were strengthened as the cooling rates increased, though the elongation was somewhat reduced. With a cooling rate of $800^{\circ}C/s$ after normalization at $1150^{\circ}C$, the alloy sample showed a tensile strength of 1450 MPa, which is about twice that of the hot rolled sample; however, at $600^{\circ}C$ the tensile strength dramatically decreased to 620 MPa. Optical microscope and transmission electron microscope were used to investigate the microstructural changes of the specimens. The resultant strengthening of the alloy sample could be mainly attributed to the interstitially dissolved nitrogen, the fraction of the tempered martensite, the fine grain and the presence of a smaller precipitate. The decrease in the tensile strength was mainly caused by the precipitation of vanadium-rich nitride.

Flexural Strength and Dielectric Properties of in-situ Si3N4-SiO2-BN Composite Ceramics (반응소결된 Si3N4-SiO2-BN 복합체의 기계적 강도 및 유전물성에 관한 연구)

  • Lee, Hyun Min;Lee, Seung Jun;Baek, Seungsu;Kim, Do Kyung
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.386-391
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    • 2014
  • Silicon nitride ($Si_3N_4$) is regarded as one of the most promising materials for high temperature structural applications due to its excellent mechanical properties at both room and elevated temperatures. However, one high-temperature $Si_3N_4$ material intended for use in radomes has a relatively high dielectric constant of 7.9 - 8.2 at 8 - 10 GHz. In order to reduce the dielectric constant of the $Si_3N_4$, an in-situ reaction process was used to fabricate $Si_3N_4-SiO_2$-BN composites. In the present study, an in-situ reaction between $B_2O_3$ and $Si_3N_4$, with or without addition of BN in the starting powder mixture, was used to form the composite. The in-situ reaction process resulted in the uniform distribution of the constituents making up the composite ceramic, and resulted in good flexural strength and dielectric constant. The composite was produced by pressure-less sintering and hot-pressing at $1650^{\circ}C$ in a nitrogen atmosphere. Microstructure, flexural strength, and dielectric properties of the composites were evaluated with respect to their compositions and sintering processes. The highest flexural strength (193 MPa) and lowest dielectric constant (5.4) was obtained for the hot-pressed composites. The strength of these $Si_3N_4-SiO_2$-BN composites decreased with increasing BN content.

A study on the construction characteristic of bath cryostat (Bath cryostat의 제작특성에 관한 연구)

  • Kim, G.Y.
    • Journal of the Korean Society for Precision Engineering
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    • v.10 no.2
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    • pp.138-145
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    • 1993
  • The bath cryostat of cryogenic apparatuses which are generally used to study physical phenomena under low temperature and ultra low temperature has been desigened and constructed. The practical use of the cryostat is verified by the measurement of the storage life of liquid heloum and liquid nitrogen vessels. The cryostat consists of triple structure of high vacuum environment in order to minimize the evaporation rate of liquid helium and liquid nitrogen by thermal conductivity and radiant heat. The minimum thickness which can stand against inner and outer pressures is calculated from considering the strength of the material.

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The effect of shielding gases on the characteristics of super duplex weld metal (슈퍼 듀플렉스 용접부에 미치는 보호가스의 영향)

  • Hong, In-Pyo;Lee, Cheol-Hwan;Kim, Yu-Gi;Kim, Dae-Sun
    • Proceedings of the KWS Conference
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    • 2005.06a
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    • pp.209-211
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    • 2005
  • Super duplex stainless steels have been used for offshore oil and gas piping systems which are subject to corrosion atmosphere, because they have excellent resistance to Stress Corrosion Cracking (SCC) and Pitting corrosion and high strength/weight ratio. Normally, the welding for duplex stainless steels has been peformed using GTAW with Ar shielding gas. However, in case of using Ar as shielding gas, the corrosion resistance at root weld metal will be deteriorated due to loss of nitrogen from weld deposit during welding. It is wellknown that the corrosion resistance of super duplex stainless can be restored by addition of nitrogen as shielding gas. In this study, we made super duplex welding with using several kinds of shielding and purging gases and investigated the relationship between shielding gas and corrosion resistance. Consequently, it was shown that corrosion resistance of weld deposit can be restored by addition of $N_{2}$ as shielding gas.

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Optimal condition for efficient DNA transfer in filamentous cyanobacteria by electroporation

  • Poo, Ha-Ryoung
    • Journal of Microbiology
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    • v.35 no.3
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    • pp.181-187
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    • 1997
  • Filamentous cyanobacteria are an ecologically important group of bacteria because they are able to provide both organic carbon fixed nitrogen that can support the nutritional requirements for other microorganisms. Because of their prokaryotic nature, they can also be used as potentially powerful model systems for the analysis of oxygenic photosynthesis and nitrogen fixation. Gene transfer is an indispensable procedure for genetic analysis of filamentous cyanobacteria. Electroporation was used to introduce foreign DNA into cyanobacterial cells. In experiments designed to optimize the electroporation technique, the effects of the field strength (amplitude of pulse) and time constant (duration of pulse), DNA concentration and host restriction/modification of DNA on the efficiency of electro-transformation were investigated. The results of this research revelaed that a high voltage pulse of short duration was effective for the electro-transformation of Anabaene sp. M131. The maximal number of transformants was obtained at 6 kV/cm with a pulse duration of 5 msec. The efficiency of electro-transformation was also sensitive to concenetration of DNA; even small amounts of DNA (0.01 .mu.g/ml) were able to gie a large number of transformants (1.0 * 10$\^$3/ cfu/ml).

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Electrical Insulation for Superconducting Apparatus (초전도 기기의 전기절연)

  • 곽동주
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1989.06a
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    • pp.11-14
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    • 1989
  • Some experimental studies on the dielectric strength characteristics of organic material under compressive stress associated with high magnetic fields and of liquid coolant in the presence of thermally induced bubble, which might be generated at unexpected quench of immersed-cooling superconducting devices, was performed to obtain the basic data on the electrical insulation design for superconducting apparatus. PET and liquid nitrogen were used as test mediums.

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Influence of Biaxial Loads on Impact Fracture of High-Strength Membrane Materials

  • Kumazawa, Hisashi;Susuki, Ippei;Hasegawa, Osamu;Kasano, Hideaki
    • Advanced Composite Materials
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    • v.18 no.4
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    • pp.395-413
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    • 2009
  • Impact tests on high-strength membrane materials under biaxial loads were experimentally conducted in order to evaluate influence of biaxial loads on impact fracture of the membrane materials for the inflated applications. Cruciform specimens of the membrane materials were fabricated for applying biaxial loadings during the impact test. A steel ball was shot using a compressed nitrogen gas gun, and struck the membrane specimen. Impact tests on uniaxial strip specimens were also conducted to obtain the effect of specimen configuration and boundary condition on the impact fracture. The results of the measured crack length and the ultra-high speed photographs indicate the impact fracture properties of the membrane fabrics under biaxial loadings. Crack length due to the impact increased with applied tensile load, and the impact damages of the cruciform membrane materials under biaxial loadings were smaller than those of under uniaxial loadings. Impact fracture of the strip specimen was more severe than that of the cruciform specimen due to the difference of boundary conditions.

Manufactures of Agricultural grade Gelatin from Cr Tanned Leather Wastes (중금속 Cr 함유 피혁 폐기물로부터 농업용 Gelatin 제조)

  • Kim, Won-Ju;Ko, Jae-Yong;Heo, Jong-Soo
    • Journal of the Korea Organic Resources Recycling Association
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    • v.9 no.3
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    • pp.93-103
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    • 2001
  • Once of recent issue in the leather industry is disposal of shaving scrap containing chromium. Shaving scrap is indispensible generated by control of the final thickness in the leather making process. It is the flesh layer of the skin consisting mainly of collagen. More recently, we have tried to improve the quality of the isolated gelatin. The purpose of this research was to extract gelatin for agricultural usage. As a result, it does not contain Cr and could obtained to a good gelatin that have more than 130,000Da. average molecular weight, more than 30 mps viscosity and more than 100g jelly strength. Gelatin that is extracted by alkaline condition expected to be available to high performance gelatin such as material of organic fertilizer(ex, Nitrogen-release fertilizer).

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A Study on Allocation of Air Pollution Monitoring Network by Spatial Distribution Analysis of Ozone and Nitrogen Dioxide Concentrations in Busan (부산지역 오존 및 이산화질소 농도의 공간분포해석에 따른 대기오염측정망 배치연구)

  • Yoo, Eun-Chul;Park, Ok-Hyun
    • Journal of Korean Society for Atmospheric Environment
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    • v.20 no.5
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    • pp.583-591
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    • 2004
  • In this study, methodologies for the rational organization of air pollution monitoring network were examined by understanding the characteristics of temporal and spatial distribution of secondary air pollution, whose significance would increase hereafter. The data on $O_3$ and $NO_2$ concentrations during high ozone period in 1998~1999 recorded at the nine air pollution monitoring station in Busan were analysed using principal component analysis (PCA) and cumulative semivariogram. It was found that the ozone concentration was deeply associated with the daily emission characteristics or the $O_3$ precusors, and nitrogen dioxide concentration largely depends on the emission strength of regional sources. According to the spatial distribution analysis of ozone and nitrogen dioxide in Busan using cumulative semivariograms, the number of monitoring stations for the secondary air pollution can be reduced in east-west direction, but reinforced in north-south direction to explain the spacial variability. More scientific and rational relocation of air pollution monitoring network in Busan would be needed to investigate pollution status accurately and to plan and implement the pollution reduction policies effectively.

A study on the characteristics of arc discharge and radiated electromagnetic wave in liquid nitrogen (액체질소중에 있어서 아크방전 및 방사 전자파의 특성에 관한 연구)

  • Shin, Dong-Hwa;Park, Kwang-Seo;Ju, Jae-Hyun;Choi, Byung-Ju;Kim, Ki-Chai;Lee, Kwang-Sik;Lee, Dong-In
    • Proceedings of the KIEE Conference
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    • 1997.07e
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    • pp.1669-1671
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    • 1997
  • Liquid nitrogen has many adventages. It is cheaper than other cooling medium. It is easy to obtain high purity. It's utilized with easy. In future, liquid nitrogen is able to be accepted cooling medium for the superconducting and cryogenic applicated equipments. Cryogenic liquid may be atmospheric pressure state because thermoinsulation is ineffective, airtight decreasing by long time using and bubble occured by flowing current. If it is to be atmospheric pressure state, the electrical insulation strength is dropped and processed partial discharge, finally breakdown. Processing of breakdown has anticipated by measuring radiated-electromagnetic wave which is happened in time of breakdown. There is a measurement of radiated electromagnetic wave as a method that proceeding breakdown is anticipated. In this paper, radiated electromagnetic wave was measured in arc discharge by above conditions as a basic experiment.

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