• Title/Summary/Keyword: High Pressure Freezing

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A Study on Anti-Icing Design by Conjugate Heat Transfer Analysis in a Lab-Scale Printed Circuit Heat Exchanger for Supply of Cryogenic High Pressure Liquid Hydrogen (극저온 고압액체수소 공급을 위한 실험실 규모 인쇄기판 열교환기의 복합열전달 해석을 통한 방빙설계에 관한 연구)

  • SOHN, SANGHO;KIM, WOOKYOUNG
    • Transactions of the Korean hydrogen and new energy society
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    • v.33 no.5
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    • pp.541-549
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    • 2022
  • This study investigates anti-icing design by conjugate heat transfer analysis in lab-scale printed circuit heat exchanger (PCHE) for supply of cryogenic high pressure liquid hydrogen. The conjugate heat transfer analysis by using computational dynamics (CFD) provided various temperature distributions at important locations in PCHE heat exchanger and predicted the possibility of freezing in hot channel. And, the effect of inlet temperature of glycol water was analyzed in order to resolve the freezing problem in PCHE.

CLSM [Confocal Laser Scanning Microscope] Observation of the Surface Roughness of Pressurized Rock Samples During Freeze/Thaw Cycling

  • Kim, Hye-jin;Choi, Junghae;Chae, Byung-gon;Kim, Gyo-won
    • The Journal of Engineering Geology
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    • v.25 no.2
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    • pp.165-178
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    • 2015
  • Physical and chemical weathering degrades rock, affecting its structural properties and thus the stability of stone buildings or other structures. Confocal laser scan microscopy (CLSM) is used here to observe temporal changes in the surface roughness of rock samples under simulated accelerated weathering. Samples were pressurized to 50, 55, or 70 MPa using a pressure frame, and subjected to freeze/thaw cycling controlled by a thermostat. The temperature was cycled from -20℃ to 40℃ and back. After each 20 cycles, CLSM was used to assess the change in surface roughness, and roughness factors were calculated to quantify the progression of the surface condition over time. Variations in cross-section line-roughness parameters and surface-roughness parameters were analyzed for specific parts of the sample surfaces at 5× and 50× magnification. The result reveals that the highest and lowest values of the roughness factors are changed according to elapsed time. Freezing/thawing at high pressure caused larger changes in the roughness factor than at low pressure.

The Analysis of Textbook Contents and Science Teachers' Conceptions on Freezing Point Depression Phenomenon (어느점 내림 현상에 대한 교과서 내용 및 중등 과학 교사들의 개념 분석)

  • Ha, Seong-Ja;Kim, Bum-Gi;Paik, Seoung-Hey
    • Journal of The Korean Association For Science Education
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    • v.25 no.2
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    • pp.88-97
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    • 2005
  • The purpose of this study was to investigate explanations of science textbooks and science teachers' conceptions related to freezing point depression phenomenon. Seven kinds of middle school science textbooks and five kinds of high school chemistryII textbooks were analyzed for the purpose. The teachers' conceptions were searched by a questionnaire developed in this study. The subjects were 146 science teachers. The explanation types of science textbooks were divided into two; 'Description of the phenomenon' and 'Vapor pressure lowering'. The explanations in most of middle school science textbooks and high school chemistryII textbooks belong to 'Description of the phenomenon' and there was no explanation of the reason. The graphs related to depression of freezing point were diverse, too. Most of the science teachers also did not have scientific conception. The percentage of the teachers who thought that the cause of freezing point depression was blocking of solute in solution was high. But the teacher could not find meaningful relation the 'Blocking of solute' explanation represented for elevation of boiling point with depression of freezing point. It is insisted that entropy concept is need to explain depression of freezing point phenomenon in this study.

Effect of Casting Temperature and Speed on Formation of Surface Defect in Al-8Zn-2Mg-2Cu Billets Fabricated by Direct-Chill Casting Process (수직 연속주조 공정으로 제조된 Al-8Zn-2Mg-2Cu 빌렛의 표면 결함 형성에 미치는 주조 온도와 주조 속도의 영향)

  • Lee, Yoon-Ho;Kim, Yong-You;Lee, Sang-Hwa;Kim, Min-Seok;Euh, Kwangjun;Lee, Dong-Geun
    • Journal of Korea Foundry Society
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    • v.41 no.3
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    • pp.241-251
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    • 2021
  • 7000-series aluminum alloys are noted for their superior strength compared with other Al alloys, and their billets are generally fabricated by direct-chill (DC) casting. Surface defects in a DC-cast aluminum billet are mainly related to exudation and the meniscus freezing phenomenon, which are influenced by alloy compositions, casting speed, and casting temperature. 7000-series aluminum alloys have a wide freezing range during solidification, which makes it easy for casting defects to occur. In this study, we investigated surface defect evolution in casting billets of Al-8Zn-2Mg-2Cu alloy fabricated by a DC casting process. The billets showed "wavy" or "dotted" surfaces. The wavy surface was formed by meniscus freezing at a lower casting speed (200 mm/min) and temperature (655 ℃). In the wavy surface, refined dendritic cells were observed in a concave region due to the constitutional supercooling caused by meniscus freezing. Meanwhile, at a higher casting temperature (675 ℃), the dotted surface was formed by pore formation. In the dotted surfaces in the billet formed at a high casting speed (230 mm/min), an exudation layer was formed by the high metallostatic head pressure. The dotted region and the smooth region had a refined dendritic morphology and a columnar morphology at the exudation layer, respectively. This is attributed to the formation of gas pores in the dotted region.

Realization of silver fixed-point and application for the high temperature platinum resistance thermometry using the gas-pressure controlled sodium heat-pipe furnace (가스압력조절식 나트륨 열관전기로를 이용한 은 고정점 실현과 고온백금저항온도 계측에의 응용)

  • Gam, K.S.;Choi, I.M.;Yang, I.;Kim, Y.G.
    • Journal of Sensor Science and Technology
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    • v.18 no.2
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    • pp.116-121
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    • 2009
  • Pressure-controlled sodium heat pipe furnace was designed and fabricated, and its characteristics was investigated. Pressure control system was controlled within ${\pm}0.5\;Pa$ at 150 kPa and the stability of pressure was decreased to ${\pm}2.5\;Pa$, when the pressure-controlled system connected with the heat pipe. The melting curve of Ag fixed-point realized well by the adiabatic method using the pressure-controlled sodium heat pipe furnace and its accuracy showed ${\pm}2.27\;mK$ from the calculation of 20% to 80% at the plateau. The freezing curve of Ag fixed-point also realized and its plateau value was 2.23 mK lower than that of the melting curve.

Effects of the Freeze/Thaw Process on the Strength Characteristics of Soils(1) (동결-융해작용이 흙의 제강도특성에 미치는 영향(I))

  • 유능환;박승법
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.31 no.2
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    • pp.43-53
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    • 1989
  • In this research programs, a series test was conducted to show the effects of freeze/thaw process on the various soil properties. The tests were carried out taken from the west sea shore of Korean peninsular and the west sea shore of Scotland, and their results are as follows; 1. There was a positive total heave in a freezing run, although water may he expelled for the sample initially. The water flow must he reverse' from expulsion to intake. 2. The confining pressure had an overriding influence on the heave and frost penetration, a sudden change of the axial strain at failure with strain rate was observed occuring at a strain rate between 10-5 and 10-6, and the initial friction angle of frozen clay was appeared zero. 3. There was shown a significant decrease in liquid limit of soil which was subjected to freeze/thaw process for the initial value of about 20% because of soil particles aggregation. 4. The cyclic freeze/thaw caused a sinificant reduction in shear strength and its thixotropic regain. The frozen/thawed soil exibited negative strength regain, particularly at high freeze/thaw cycles. 5. The freezing temperature greatly influenced on the failure strength of soils and this. Trend was more pronounced the lower the freezing temperature and shown the ductile failure with indistinct peaks.

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Preparation and Its Stability of a Coenzyme Q10 Nanoemulsion by High Pressure Homogenization with Different Valve Type Conditions (초고압균질기 밸브 타입에 따른 coenzyme Q10 나노에멀젼의 제조 및 안정성)

  • Lim, Ji-Sun;Gang, Ho-Jin;Yoon, Sung-Woo;Kim, Hyeong-Min;Suk, Jong-Woo;Kim, Do-Un;Lim, Jae-Kag
    • Korean Journal of Food Science and Technology
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    • v.42 no.5
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    • pp.565-570
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    • 2010
  • A coenzyme Q10 nanoemulsion was prepared using high pressure homogenization with different valve type conditions (A, B, and C) and cycle numbers (1, 2, and 3). The particle size, transmittance, zeta potential, and coenzyme Q10 content of the prepared coenzyme Q10 nanoemulsion were measured. The stability of the prepared coenzyme Q10 nanoemulsion was evaluated on heating ($95^{\circ}C$), freezing ($-20^{\circ}C$), and different pH (2-10) conditions. Also, the prepared coenzyme Q10 nanoemulsion was stored at different temperatures of 4, 25, and $40^{\circ}C$ for 12 weeks to evaluate its storage stability. In this study, the optimal conditions of high pressure homogenization for the preparation of a coenzyme Q10 nanoemulsion were identified to be 150 MPa, C valve, and a cycle number of 3. The results showed that the prepared coenzyme Q10 nanoemulsion had an average particle size of 40 nm, generated no deposits or floating matter when stored at either 4 or $25^{\circ}C$ for 12 weeks, and displayed excellent dispersibility and transparency when processed at different pHs (4-10) or heating ($95^{\circ}C$) and, freezing ($-20^{\circ}C$) conditions. Our results indicated that a coenzyme Q10 nanoemulsion prepared by high pressure homogenization can be used for preparing beverages in the food industry.

The Frost Heaving Susceptibility Evaluation of Subgrade Soils Using Laboratory Freezing System (실내 동상시스템을 이용한 노상토의 동상민감성 평가)

  • Shin, Eun Chul;Ryu, Byung Hyun;Park, Jeong Jun
    • Journal of the Korean Geosynthetics Society
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    • v.12 no.2
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    • pp.13-23
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    • 2013
  • The Korean Peninsula is considered as a seasonal frozen area that is thawed in the spring and frozen in the winter. The influence of fines of the frost susceptibility of subgrade soils were established by laboratory freezing tests simulating closely the thermal conditions in the field. During the winter season, the climate is heavily influenced by the cold and dry continental high pressure. Because of siberian air mass, the temperature of January is $-6{\sim}-7^{\circ}C$ on average. This chilly weather generate the frost heaving by freezing the moisture of soil and damage potential of the geotechnical structure. In the freezing soil, the ice lenses increase the freeze portion of soil by absorbing the ground water with capillary action. However, the capillary characteristics differ from the sort of soil on the state of freezing condition. In this study, ten soil samples are prepared. The basic physical property tests were performed by following the Korean Industrial Standard and the soil specimens were classified by the Unified Soil Classification System (USCS). These classified soils are used to perform the laboratory opened systems freezing test in order to determine the frost heaving characteristics of soils such as unfrozen water content, heaving amount, and freezing depth.

Selection of working fluid for cryosurgical probe considering biological heat transfer

  • Hwang, Gyu-Wan;Jeong, Sang-Kwon
    • Progress in Superconductivity and Cryogenics
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    • v.9 no.4
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    • pp.46-49
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    • 2007
  • This paper describes the sensitive cooling performance change of J-T refrigerator for cryosurgical probe due to its working fluid. The analytical results of using 50 bar nitrous oxide are compared with the case of 300 bar argon. Bio-heat equation is numerically solved to investigate the effect of the probe temperature and the cooling power of the J-T refrigerator. The refrigerator using 50 bar nitrous oxide has larger cooling power above 185 K than the one with 300 bar argon, which enables fast cooling at early stage of cryosurgery, but the biological tissue away from the probe tends to be cooled slowly after the probe reaches its lowest operating temperature. When the repeated freeze-thaw cycle is employed for main tissue destruction mechanism, using high pressure nitrous oxide is more advantageous than argon if the freezing operation is within 2-3 minutes. The probe with high pressure argon is more suitable for the case of longer freeze-thaw cycle with fewer repetitions.

Numerical Study on the Production of Methane Hydrate by Depressurization Method (감압법을 이용한 메탄하이드레이트 생산에 대한 수치적 연구)

  • Kim, Jin-Hong;Chun, Won-Gee;Kim, Nam-Jin
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.519-523
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    • 2007
  • Gas(or methane) hydrates are solid solutions when water molecules are linked through hydrogen bonding and create host lattice cavities that can enclose a large variety of guest gas molecules. The natural gas hydrate crystal may exist at low temperature above the normal freezing point of water and high pressure greater than about 30 bars. A lot of quantities of natural gas hydrates exists in the earth and many production schemes are being studied. In the present investigation, depressurization method was considered to predict the production of gas and the simulation of the two phase flow - gas and water - in porous media is being carried out. The simulation show about the fluid flow in porous media have a variety of applications in industry. Results provide the appearance of gas and water production, the pressure profile, the saturation of gas/ water/ hydrates profiles and the location of the pressure front.

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