• 한국표면공학회지
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• 제47권5호
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• pp.221-226
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• 2014

A low temperature plasma nitrocarburizng was implemented on the duplex stainless steel to achieve the enhancement of surface hardness without degradation of its corrosion resistance. Attempts were made to investigate the influence of Pulse frequency and Duty factor of pulsed power in a high Pulse frequency regime on the surface characteristics of the hardened layer. The hardened layer (S-phase) was formed on all of the treated surfaces. Surface hardness reached up to 1300 $HV_{0.1}$ which is about 4.6 times higher than that of the untreated material (280 $HV_{0.1}$). The thickness of the hardened layer tends to increase lightly with the higher Pulse frequency and the higher Duty factor. The corrosion resistance of nitrocarburized duplex stainless steel was almost similar to that of the untreated material. Both the Pulse frequency and the Duty factor do not have a significant influence on the corrosion property of plasma treated duplex stainless steel.

• The Journal of Advanced Prosthodontics
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• 제12권3호
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• pp.114-123
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• 2020

PURPOSE. The aim of this study was to evaluate the corrosion resistance of the specimens produced by five different commercial metal laser sintering (MLS) systems with their recommended Co-Cr alloy powders. MATERIALS AND METHODS. The MLS machines and the alloy powders used were, ProX 100-ST2724G (St-Pro), Mysint 100-EOS SP2 (SP2-Mys), EOSINT 270-EOS SP2 (SP2-EOS), SLM 100-Starbond CoS (SB-SLM), and MLab Cusing-Remanium^® Star (RS-MLab), respectively. Eight specimens from each group were prepared. Open circuit potential (E_ocp) and electrochemical impedance spectroscopy (EIS) measurements of polished surfaces of the specimens were conducted in a three-electrode cell using a potentiostat-galvanostat in Fusayama-Meyer artificial saliva (AS). Specimens from each group were immersed in AS and de-ionized water for seven days. E_ocp, charge transfer resistance (R_ct) values, and released ions (㎍/㎠ × 7d) in different solutions were determined. The specimen surfaces were observed with SEM/EDS. Results were analyzed statistically. RESULTS. E_ocp values have shifted to potentials that are more positive over time. Steady-state E_ocp values were from high to low as follows, SB-SLM, SP2-Mys, SP2-EOS, RS-MLab, and ST-Pro, respectively. After 60 mins, RS-MLab specimens had the highest R_ct value, followed by SP2-Mys, SB-SLM, SP2-EOS, and ST-Pro. In all groups, ion release was higher in AS than that in de-ionized water. CONCLUSION. There were small differences among the corrosion resistances of the Co-Cr alloy specimens produced with MLS systems; meanwhile, the corrosion resistances were quite high for all specimens.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2007년도 추계학술대회 논문집
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• pp.429-429
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• 2007

For various applications of liquid crystal displays (LCDs), the uniform alignment of liquid crystal (LC) molecules on treated surfaces is significantly important. Generally, a rubbing method has been widely used to align the LC molecules on polyimide (PI) surfaces. Rubbed PI surfaces have suitable characteristics, such as uniform alignment. However, the rubbing method has some drawbacks, such as the generation of electrostatic charges and the creation of contaminating particles. Thus, we strongly recommend a non contact alignment technique for future generations of large high-resolution LCDs. Most recently, the LC aligning capabilities achieved by ultraviolet and ion-beam exposures which are non contact methods, on diamond-like carbon (DLC) inorganic thin film layers have been successfully studied because DLC thin films have a high mechanical hardness, a high electrical resistivity, optical transparency, and chemical inertness. In addition, nitrogen-doped DLC (NDLC) thin films exhibit properties similar to those of the DLC thin films and a higher thermal stability than the DLC thin films because C:N bonding in the NDLC thin filmsis stronger against thermal stress than C:H bonding in the DLC thin films. Our research group has already studied the NDLC thin films by an ion-beam alignment method. The $SiN_x$ thin films deposited by plasma-enhanced chemical vapor deposition are widely used as an insulation layer for a thin film transistor, which has characteristics similar to those of DLC inorganic thin films. Therefore, in this paper, we report on LC alignment effects and pretilt angle generation on a $SiN_x$, thin film treated by ion-beam irradiation for various N ratios

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 1998년도 하계종합학술대회논문집
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• pp.437-440
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• 1998

We studied phosphorus doping effect on the epitaxial growth of $Si_{1-x}Ge_{x}$ film with high Ge fraction on Si substates at 550.deg. C by LPCVD. In a low $Ph_{3}$ partial pressure region such as below 1.25 mPa, the phosphorus dopant concentration increased linearly with increasing $PH_{3}$ partial pressure while the deposition rate and the Ge fraction were constant. In a higher $PH_{3}$ partial pressure region, the phosphorus dopant concentration and the deposition rate decreased, while the Ge fraction slightly increased. The deposition arate and the Ge fraction increased with increasing $GeH_{4}$ partial pressure while the phophours dopant concentration decreased. But the increasing rate of Ge fraction with incrasing $PH_{3}$ partial pressure was reduced at a high $GeH_{4}$ partial pressure. According to test results, it suggests that high surface coverage of phosphorus atoms suppress both the $SiH_{4}$ adsorption/reasction and the $GeH_{4}$ adsorption/reaction on the surfaces, and the effect is more stronger on $SiH_{4}$ than on $GeH_{4}$. In a higher $PH_{3}$ partial pressure region, the epitaxial growth is largely controlled by surface coverage effect of phosphorus atoms. The phosphorus surface coverage was slimited at a high $GeH_{4}$ partial pressure because adsorbed Ge atoms effectively suppresses the adsorption of phosphorus atoms.

• 소성∙가공
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• 제18권4호
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• pp.296-303
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• 2009

The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore for its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 춘계학술대회 논문집
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• pp.350-352
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• 2009

The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore fur its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

• 한국환경과학회지
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• 제26권9호
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• pp.1057-1072
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• 2017

In order to investigate the effect of air temperature reduction on an urban neighborhood park, air temperature data from five inside locations (forest, pine tree, lawn, brick and pergola) depending on surface types and three outside locations (Suwon, Maetan and Kwonsun) depending on urban forms were collected during the summer 2016 and compared. The forest location had the lowest mean air temperature amongst all locations sampled, though the mean difference between this and the other four locations in the park was relatively small ($0.2-0.5^{\circ}C$). In the daytime, the greatest mean difference between the forest location and the two locations exposed to direct beam solar radiation (brick and lawn) was $0.5-0.8^{\circ}C$ (Max. $1.6-2.1^{\circ}C$). In the nighttime, the mean difference between the forest location and the other four locations in the park was small, though differences between the forest location and locations with grass cover (pine tree and lawn) reached a maximum of $0.9-1.7^{\circ}C$. Comparing air temperature between sunny and shaded locations, the shaded locations showed a maximum of $1.5^{\circ}C$ lower temperature in the daytime and $0.7^{\circ}C$ higher in the nighttime. Comparing the air temperature of the forest location with those of the residential (Kwonsun) and apartment (Maetan) locations, the mean air temperature difference was $0.8-1.0^{\circ}C$, higher than those measured between the forest location and the other park locations. The temperatures measured in the forest location were mean $0.9-1.3^{\circ}C$ (Max. $2.0-3.9^{\circ}C$) lower in the daytime than for the residential and apartment locations and mean $0.4-1.0^{\circ}C$ (Max. $1.3-3.1^{\circ}C$) lower in the nighttime. During the hottest period of each month, the difference was greater than the mean monthly differences, with temperatures in the residential and apartment locations mean $1.0-1.6^{\circ}C$ higher than those measured in the forest location. The effect of air temperature reduction on sampling locations within the park and a relatively high thermal environment on the urban sampling locations was clearly evident in the daytime, and the shading effect of trees in the forest location must be most effective. In the nighttime, areas with a high sky view factor and surface types with high evapotranspiration potential (e.g. grass) showed the maximum air temperature reduction. In the urban areas outside the park, the low-rise building area, with a high sky view factor, showed high air temperature due to the effect of solar (shortwave) radiation during the daytime, while in the nighttime the area with high-rise buildings, and hence a low sky view factor, showed high air temperature due to the effect of terrestrial (longwave) radiation emitted by surrounding high-rise building surfaces. The effect of air temperature reduction on the park with a high thermal environment in the city was clearly evident in the daytime, and the shading effect of trees in the forest location must be most effective. In the nighttime, areas with high sky view factor and surface types (e.g., grass) with evapotranspiration effect showed maximum air temperature reduction. In the urban areas outside the park, the high sky view factor area (low-rise building area) showed high air temperature due to the effect of solar (shortwave) radiation during the daytime, but in the nighttime the low sky view factor area (high-rise building area) showed high air temperature due to the effect of terrestrial (longwave) radiation emitted surrounding high-rise building surfaces.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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• pp.379-380
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• 2002

Steam generators (S/G) of pressurized water reactors are large heat exchangers that use the heat from the primary reactor coolant to make steam in the secondary side for driving turbine generators. Reciprocating sliding wear experiments have been performed to examine the wear properties of Incoloy 800 and Inconel 690 steam generator tubes in high temperature water. In present study, the test rig was designed to examine the reciprocating and rolling wear properties in high temperature (room temperature - $300^{\circ}C$) water. The test was performed at constant applied load and sliding distance to investigate the effect of test temperature on wear properties of steam generator tube materials. To investigate the wear mechanism of material, the worn surfaces were observed using scanning electron microscopy. At $290^{\circ}C$, wear rate of Inconel 690 was higher than that of Incoloy 800. It was assumed to be resulted from the oxide layer property difference due to the a\loy composition difference. Between 25 and $150^{\circ}C$ the wear loss increased with increasing temperature. Beyond $150^{\circ}C$, the wear loss decreased with increasing temperature. The wear loss change with temperature were due to the formation of wear protective oxide layer. From the worn surface observation, texture patterns and wear particle layers were found. As test temperature increased, the proportion of particle layer increased.

• 한국전산유체공학회지
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• 제7권3호
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• pp.9-16
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• 2002

Most of modem aerospace gas turbines must be operated at a gas temperature which is several hundreds of degrees higher than the melting temperatures of the materials used in their construction. Complicated cooling schemes need to be employed in the combustor walls and in the high pressure turbine stages. Internal passages are cast or machined into the hot sections of aero-gas turbine engines and air from the compressor is used for cooling. In many cases, the cooling system is engineered to utilize jets of high velocity air, which impinge on the internal surfaces of the components. They are categorized as 'Impinging Cooling Method' and 'Vortex Cooling Method'. Specially, research of new cooling system(Vortex Cooling Method) that overcomes inefficiency of film cooling and limitation of space. The focus of new cooling system that improves greatly cooling efficiency using less amount of cooling air on surface heat transfer elevation. Therefore, in this study, a numerical analysis has been peformed for characteristics of flow and heat transfer in the swirl chamber and compared with the flow measurements by LDV. Especially, for understanding high heat transfer efficiency in the vicinity of wall, we considered flow structure, vortex mechanism and heat transfer characteristics with variation of the Reynolds number.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2002년도 춘계 학술발표강연 및 논문개요집
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• pp.132-132
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• 2002

Diamond is well known as the hardest material in nature. It also has other unique bulk physical and mechanical properties, such as very high thermal conductivity and broad optical transparency, which enable a number of new applications now that large areas of diamond can be fabricated by the new diamond plasma chemical vapor deposition (CVD) technologies. A study on the effects of growth kinetics and properties of diamond films obtained by addition of argon (~7 vol. %) into the methane/hydrogen mixture is carried out using HFCVD system. A negative bias was used as a nucleation enhancement method in addition to the argon dilution. The scanning electron microscopy (SEM) image of surface morphology shows well faceted crystallites with a predominance of angular shapes corresponding to <100> and <110> crystalline surfaces. The nucleation density and growth rate with argon dilution is two orders of magnitude higher than without argon deposition. The Raman spectra show a good quality film whereas XPS spectra show existence of only diamond phase.