• 제목/요약/키워드: High Frequency Heat Treatment

검색결과 135건 처리시간 0.032초

Ar 이온빔 조사에 따른 SnO2 박막의 물성 연구 (Effect of Ar Ion Irradiation on the Hydrogen Gas Sensitivity of SnO2 Thin Films)

  • 허성보;이영진;김선광;유용주;최대한;이병훈;김민규;김대일
    • 열처리공학회지
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    • 제25권6호
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    • pp.279-282
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    • 2012
  • $SnO_2$ thin films were prepared on the Si substrate by radio frequency (RF) magnetron sputtering and then surface of the films were irradiated with intense Ar ion beam to investigate the effect of Ar ion irradiation on the properties and hydrogen gas sensitivity of the films. From atomic force microscope observation, it is supposed that intense Ar bombardments promote rough surface and increase gas sensitivity of $SnO_2$ films for hydrogen gas. The films that Ar ion beam irradiated at 6 keV show the higher sensitivity than the films were irradiated at 3 keV and 9 keV. These results suggest that the $SnO_2$ thin films irradiated with optimized Ar ion beam are promising for practical high-performance hydrogen gas sensors.

Fast Precessional Motion of Co/Pd Multilayer Systems Induced by Heat Treatment

  • Sohn, Jeong-Woo;Lee, Kyeong-Dong;Song, Hyon-Seok;Kim, Seon-Ock;Kim, Ji-Wan;Jeong, Jae-Woo;Shin, Sung-Chul
    • 한국자기학회:학술대회 개요집
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    • 한국자기학회 2010년도 임시총회 및 하계학술연구발표회
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    • pp.94-94
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    • 2010
  • Co/Pd multilayer systems have been investigated with much attention for a long time due to the high and easily controllable perpendicular magnetic anisotropy. Two [Pd(1)/Co(0.4 nm)]5 multilayer systems - one is as-deposit, and the other is annealed at $350^{\circ}C$ - are studied with an all-optical approach. A two-color optical pump probe setup using 30 fs laser pulse at 82 MHz repetition rate is used to measure the time-resolved magneto-optical Kerr signal. It turns out the heat treatment enhances the perpendicular magnetic anisotropy, and leads to faster magnetization precession. The frequency reaches 30 GHz in the annealed sample, which is a factor of 2 larger compared to the as-deposit film.

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In situ 법에 의한 Cu-Nb3Sn 복합재료선재의 초전도특성과 이에 미치는 Ti의 영향(I) (Superconducting Properties of in situ Formed Multifilamentary Cu - Nb3Sn Composites and the Effects of Ti Addition on the Superconducting Properties (I))

  • 박현순;서수정;이은덕;안재민
    • 열처리공학회지
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    • 제6권1호
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    • pp.17-25
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    • 1993
  • The Cu - $Nb_3Sn$ composites wire as a superconducting material was prepared by in situ method as follow: Cu - 15wt.% Nb alloys which were melted in a high -frequency induction furnace and casted in bar were cold-worked up to the final diameter of 0.24 mm, electroplated with Sn, pre-treated in two steps and then diffused at $550{\sim}650^{\circ}C$ for 24 ~ 96 hrs. The overall $J_c$ and $T_c$ of the specimens were measured by the four point-probe method at 10 K in the magnetic field of 0 Tesla. The overall $J_c$ of the composites wire which diffused at $550^{\circ}C$ after pre-treating in two steps were generally higher than those of the wire at either $600^{\circ}C$ or $650^{\circ}C$. For the specimens diffused at $550^{\circ}C$, the overall $J_c$ were increased until 72 hrs. of diffusion time and then decreased. However, in case of diffusion at $600^{\circ}C$ and $650^{\circ}C$, the overall $J_c$ were gradually decreased from the beginning. The maximum overall $J_c$ obtained in this experiment was $1.3{\times}10^4\;A/cm^2$, which was measured for the specimen diffused at $550^{\circ}C$ for 72 hrs. When the specimens were diffused at $550^{\circ}C$ for 72 hrs, after pre-treating, the measured critical temperature, $T_c$ was 16.19 K. Similar $T_c$ value were obtained in other specimens regardless of diffusion time and temperature.

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대기압 플라즈마 제트를 이용한 실버페이스트 전극의 표면처리 (Surface treatment of silver-paste electrode by atmospheric-pressure plasma-jet)

  • Sheik Abdur Rahman;Shenawar Ali Khan;Yunsook Yang;Woo Young Kim
    • 한국응용과학기술학회지
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    • 제40권1호
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    • pp.71-80
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    • 2023
  • 실버 페이스트는 상대적으로 낮은 열처리로 공정이 가능하기 때문에 전자 소자 응용분야에서 유용한 전극 재료이다. 본 연구에서는 은 페이스트 전극에 대기압 플라즈마 제트를 이용하여 전극 표면을 처리 했다. 이 플라즈마 제트는 11.5 kHz 작동 주파수에서 5.5 ~ 6.5 kV의 고전압을 사용하여 아르곤 분위기에서 생성되었다. 플라즈마 제트는 대기압에서 수행함으로써 인쇄 공정에 더 유용할 수 있다. 플라즈마 처리시간, 인가된 전압, 가스유량에 따라 전극의 표면은 빠르게 친수성화 되었으며 접촉각의 변화가 관찰되었다. 또한, 대면적 샘플에서 플라즈마 처리 후 접촉각의 편차가 없었는데, 이는 기판의 크기에 관계없이 균일한 결과를 얻을 수 있었다는 것을 의미한다. 본 연구의 결과는 대면적 전자소자의 제조 및 향후 응용 분야에서 적층 구조를 형성하는데 매우 유용할 것으로 기대된다.

Ti-3Al-2.5V 합금의 고온피로에 미치는 온도 및 미세조직의 영향 (The Effect of Temperature and Microstructure on High Temperature Fatigue Crack Propagation Property in Ti-3Al-2.5V Alloy)

  • 김현철;임병수
    • 한국자동차공학회논문집
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    • 제6권3호
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    • pp.198-207
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    • 1998
  • To determine the effect of temperature and microstructure on the fatigue crack propagation behavior in Ti-3Al-2.5V alloy, experimental investigations have been carried out with the specimens of different temperatures and different volume fractions of prime $\alpha$-phase. The temperatures employed were room temperature, 20$0^{\circ}C$, 30$0^{\circ}C$ and 40$0^{\circ}C$ under the same frequency of 20Hz. To obtain the different volume fractions of the primary $\alpha$-phase, specimens were solution-treated at $\alpha$+$\beta$ and above the $\beta$ region. From the experimental results, following conclusions were obtained. (1) ΔKth was observed to increase with the less volume fraction of the primary $\alpha$-phase. (2) As the temperature increased. (3) Microstructures having more primary $\alpha$-phase showed higher strength at the high temperatures.

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A Development of High Power Activated Carbon Using the KOH Activation of Soft Carbon Series Cokes

  • Kim, Jung-Ae;Park, In-Soo;Seo, Ji-Hye;Lee, Jung-Joon
    • Transactions on Electrical and Electronic Materials
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    • 제15권2호
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    • pp.81-86
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    • 2014
  • The process parameter in optimized KOH alkali activation of soft carbon series coke material in high purity was set with DOE experiments design. The activated carbon was produced by performing the activation process based on the set process parameters. The specific surface area was measured and pore size was analyzed by $N_2$ absorption method for the produced activated carbon. The surface functional group was analyzed by Boehm method and metal impurities were analyzed by XRF method. The specific surface area was increased over 2,000 $m^2/g$ as the mixing ratio of activation agent increased. The micro pores in $5{\sim}15{\AA}$ and surface functional group under 0.4 meq/g were obtained. The contents of the metal impurity in activated carbon which is the factor for reducing the electrochemical characteristics was reduced less than 100 ppm through the cleansing process optimization. The electrochemical characteristics of activated carbon in 38.5 F/g and 26.6 F/cc were checked through the impedance measuring with cyclic voltammetry scan rate in 50~300 mV/s and frequency in 10 mHz ~100 kHz. The activated carbon was made in the optimized activation process conditions of activation time in 40 minutes, mixing ratio of activation agent in 4.5 : 1.0 and heat treatment temperature over $650^{\circ}C$.

2.25Cr-1Mo 강 인공 열화재의 고주파수 초음파 감쇠특성에 관한 연구 (A Study on the High Frequency Ultrasonic Attenuation Characterization in Artificially Aging Degraded 2.25Cr-1Mo Steel)

  • 박익근;박은수;김정석;김현묵;권숙인;변재원
    • 비파괴검사학회지
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    • 제21권4호
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    • pp.439-445
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    • 2001
  • 재료나 설비의 고온 장시간 사용으로 인하여 발생되는 재질열화 평가에는 파괴적인 방법이 널리 사용되고 있으며, 신뢰도가 높다. 그러나, 시험편의 채취가 어렵고 많은 경비와 시간이 소요된다. 전기저항법, 레프리카법, 바크하우젠 노이즈법, 전기화학적방법, 초음파법 등과 같은 비파괴적인 열화손상 평가 방법이 주목을 받고 있다. 본 연구에서는 2.25Cr-1Mo 강을 $630^{\circ}C$에서 장시간 등온열처리로 모의 열화시험편을 제작하고, 고온설비부재에서 발생되는 미세조직의 변화와 고주파 초음파의 전파특성(감쇠계수)과의 일대일 상관관계를 규명하여 초음파 비파괴평가에 의한 열화도 평가의 유용성 유모를 실험적으로 검증하였다. 그 결과 2.25Cr-1Mo 인공열화재의 경우 열화가 진행됨에 따라 탄화물의 석출 및 조대화가 일어나며 초음파 감쇠계수는 증가하는 경향을 나타내었으며, 그 정도는 침상의 탄화물이 거의 소멸되는 1,000시간 이후에 초음파 감쇠계수가 급격히 증가하는 매우 좋은 상관성을 나타내었다.

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Nanocomposite-Based Energy Converters for Long-Range Focused Ultrasound Treatment

  • Lee, Seung Jin;Heo, Jeongmin;Song, Ju Ho;Thakur, Ujwal;Park, Hui Joon;Baac, Hyoung Won
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.369-369
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    • 2016
  • A nanostructure composite is a highly suitable substance for photoacoustic ultrasound generation. This allows an input laser beam (typically, nanosecond pulse duration) to be efficiently converted to an ultrasonic output with tens-of-MHz frequency. This type of energy converter has been demonstrated by using a carbon nanotube (CNT)-polydimethylsiloxane (PDMS) composite film that exhibit high optical absorption, rapid heat transition, and mechanical durability, all of which are necessary properties for high-amplitude ultrasound generation. In order to develop the CNT-PDMS composite film, a high-temperature chemical vapor deposition (HTCVD) method has been commonly used so far to grow CNT and then produce a CNT-PDMS composite structure. Here, instead of the complex HTCVD, we use a mixed solution of hydrophobic multi-walled CNT and dimethylformamid (DMF) and fabricate a solution-processed CNT-PDMS composite film over a spherically concave substrate, i.e. a focal energy converter. As the solution process can be applied over a large area, we could easily fabricate the focal transmitter that focuses the photoacoustic output at the moment of generation from the CNT-PDMS composite layer. With this method, we developed photoacoustic energy converters with a large diameter (>25 mm) and a long focal length (several cm). The lens performance was characterized in terms of output pressure amplitude for an incident pulsed laser energy and focal spot dimension in both lateral and axial. Due to the long focal length, we expect that the new lens can be applied for long-range ultrasonic treatment, e.g. biomedical therapy.

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치주수술 후 상아질 지각과민증에 대한 저수준 레이저 처치의 임상적 효과 (Clinical Effect Of Low Level Laser Therapy In The Treatment Of Dentin Hypersensitivity Following Periodontal Surgery)

  • 김남윤;임성빈;정진형
    • Journal of Periodontal and Implant Science
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    • 제26권1호
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    • pp.230-243
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    • 1996
  • Root surface exposure due to gingival recession after periodontal surgery, dentin exposure after root planing elicit pain response when exposed to mechanical, heat, chemical or osmotic stimulation. Especially, patients treated with periodontal surgery, show high frequency and there have been reports showing the 1 out of 7 patients have dentin hypersensitivity. There have been many studies on the clinical effects of various materials on the treatment of dentin hypersensitivity. but, none could provide absolute clinical efficacy. In this study, 45 teeth from 30 patients, who had had periodontal surgery and showed dentin hypersensitivity after surgery were chosen for the experimental group and they were illuminated with laser, 15teeth were chosen for the control group and they were not exposed to laser. After this dentin hypersensitivity was elicited by tactile, compressed air, cold water and then, the degree was evaluated using NRS(Numerical Rating Scale). And during LLLT(Low Level Laser Therapy) semiconductor laser using Gallium - Arsenide as a diode was illuminated for 180 seconds at a frequency of 7(500Hz). This therapy was done 10 times, and each time the changes in dentin hypersensitivity was evaluated using NRS. The results were as follows : 1. After treat with LLLT on dentin hypersensitivity due to periodontal surgery, 22.2% showed total loss of dentin hypersensitivity, 60.0% showed loss of tactile dentin hypersensitivity, 48.8% showed loss of compressed air dentin hypersensitivity, 22.2% showed loss of cold water dentin hypersensitivity. 2. As a result of clinical evaluation of dentin hypersensitivity using NRS, there was significant increase in improvement of dentin hypersensitivity in the experimental group compare to the control group(P<0.05). And there was almost no natural loss of dentin hypersensitivity in the control group. 3. In comparison of the stages of evaluation, there was significant difference in between experimental and control group. after the second visit(P<0.05), and the difference increased with each visit.

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상백피(桑白皮)가 주약(主藥)으로 배오(配伍)된 방제(方劑)의 활용(活用)에 대한 고찰(考察) (동의보감 상백피 가미방 중심으로) (Study on Application of the Morus Cortex Mainly Used in Herbal Prescription (On the Focus of Prescriptions including Morus Cortex in Donguibogam))

  • 서창우;이장천
    • 대한한의학방제학회지
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    • 제12권2호
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    • pp.1-17
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    • 2004
  • This study was investigated to make sure the range of the Morus Cortex's treatment, the nature of disease, the chief virtue of medicine, the pathology and the usage quantity of it in Donguibogam The results were as follows; 1. The frequency of being used the Morus Cortex in the consumption or cough-relative chapter is as high as a ratio of 40.6%. 2. The Morus Cortex is used in a realm of the consumption or cough-relative disease, an otorhinolalyngology, an edema, a skin-relative disease, a bleeding trouble, a thirsty and diabetes melitus, etc. 3. The Morus Cortex is used in a realm of the pathology of the pulmonary heat, the pulmonary noxious vigor, the damage from external winds and colds, fatigue, etc. 4. The Morus Cortex is used in a range of $1g{\sim}12g$ in herbal-prescription. The main using dosage is 4g(about 42%). 5. The Morus Cortex is used with various crude herbs in accordance with the pathogeny. The Morus Cortex has been used to reduce heat from the lungs and soothe asthma, to promote urination and reduce edema from shinnongboncho era. According to the results, I suggest that we use the Morus Cortex in a various pathogenic fields. The Morus Cortex is able to remove not only pathogenic heat from the consumption or cough-relative disease, but also pathogenic otorhinolalyngology, an edema, a skin-relative disease, a bleeding trouble, a thirsty and diabetes melitus, etc.

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