• Bulletin of the Korean Chemical Society
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• v.32 no.10
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• pp.3575-3580
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• 2011

This paper reports a methodology for preparing close-packed two dimensional gold nanoprism films and hexagonal nanoplate films at a hexane/water interface. By controlling the concentration of linker molecules in the hexane layer and the temperature of the colloid solution, highly ordered close-packed nanoplate arrays can be fabricated. These films were investigated to compare their corresponding surface enhanced Raman scattering (SERS) efficiencies. It was demonstrated that the Au nanoprism films resulted in a stronger SERS enhancement than the Au hexagonal nanoplate films. The difference in the SERS enhancement is attributed to the film array difference, demonstrating that Au nanoprism films have a higher line contact density than their Au hexagonal analogues.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.72-82
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• 2004

The deformation mechanism of hexagonal close-packed materials is quite complicate including slips and twins. A deformation mechanism, which accounts for both slip and twinning, was investigated for polycrystalline hop materials. The model was developed in a finite element polycrystal model formulated with initial strain method where the stiffness matrix in FEM is based on the elastic modulus. We predicted numerically the texture of Mg alloy(AZ31B) sheet by using FEM based on crystal plasticity theory. Also, we introduced the recrystallized texture employed the maximum energy release theory after rolling. From the numerical study, it was clarified that the shrink twin could not be the main mechanism for shortening of c-axis, because the lattice rotation due to twin rejects fur c-axis to become parallel to ND(normal direction of plate). It was showed that the deformation texture with the pyramidal slip gives the ring type pole figure having hole in the center.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.07b
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• pp.922-925
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• 2003

The interest of self-organization materials that have uniform and regular structure in nano scale has been grown due to their utilization in various fields of nanotechnology. An attractive candidate among these materials is anodic aluminum oxide film, which are formed by anodization of aluminum in an appropriate acid solution. The anodic aluminum oxide film has a highly ordered porous structure with very uniform and nearly parallel pores that can be organized in an almost precise close-packed hexagonal structure. In this study, we attempt to make Au dot arrays, which were fabricated using anodic aluminum oxide film as an evaporation mask. The Au dot arrays have a uniform sized dots and spacing to its neighbors and the average diameter of Au dots is about 60 nm corresponding to them of the mask.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.77-80
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• 2008

Low-cycle fatigue (LCF) tests were carried out to investigate the effect of loading direction on the cyclic deformation behavior and fatigue resistance of rolled AZ31 magnesium alloy. The as-received alloy showed a strong basal texture indicating that the most of basal planes of hexagonal close-packed structure were located parallel to the rolling direction. Two types of specimens whose loading directions were oriented parallel (RD) and vertical (ND) to the rolling direction. respectively, were used for the comparison. It was found that RD specimens yielded at much lower stresses during compression, while vice versa for the ND specimens, which was mainly attributed to the formation of primary twins. This anisotropic deformation behavior resulted in the different mean stresses during the cycling of RD and ND specimens, affecting the fatigue resistance of two specimens. The ND specimen showed a superior fatigue resistance as compared to the RD specimen under strain-controlled condition.

• Transactions of Materials Processing
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• v.14 no.7 s.79
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• pp.635-641
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• 2005

The crystal structure of magnesium was hexagonal close-packed (HCP), so its formability was poor at room temperature. But formability was improved in high temperature with increasing of the slip planes. Purpose of this paper was to know about the mechanical properties of magnesium alloy (AZ31B), before warm and hot forming process. The mechanical properties were defined by the tension and compression tests in various temperature and strain-rate. As the temperature was increased, yield·ultimate strength, K-value, work hardening exponent (n) and anisotropy factor (R) were decreased. But strain rate sensitivity (m) was increased. As strain-rate increased, yield·ultimate strength, K-value, and work hardening exponent (n) were increased. Also, microstructures of grains fined away at high strain-rate. These results would be used in simulations and manufacturing factor fer warm and hot forming process.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.05a
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• pp.53-56
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• 2004

The mechanical properties and optical micrographs are studied for rolled magnesium alloy sheet with hexagonal close packed structure(HCP) at room and elevated temperatures. Tensile properties such as tensile strength, elongation, R-value and n-value are also measured for AZ31 magnesium alloy. Magnesium with strong texture of basal plane parallel to the rolling direction usually has high R-value and plastic anisotropy at room temperature. As temperature increases, the R-value for AZ31 magnesium sheet decreases. In addition, the AZ31 sheet becomes isotropy and recrystallization above $200^{\circ}C$. Formability of magnesium alloy sheets remarkably poor at room temperature is improved by increasing temperature. Sheet forming of magnesium alloy is practically possible only at high temperature range where plastic anisotropy disappears.

• Transactions of Materials Processing
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• v.17 no.2
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• pp.97-101
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• 2008

Unique constitutive behavior of magnesium alloys as one of hexagonal close packed(hcp) metals has been implemented into the commercial finite element program ABAQUS. The constitutive equations can represent asymmetry in tension-compression yield stresses and flow curves. For the verification purpose, the springback of AZ31B magnesium alloy sheet was measured using the unconstrained cylindrical bending test proposed in Numisheet'2002 benchmark committee. Besides the developed constitutive models, the isotropic models based on tensile and compressive properties were also considered for comparison purpose. The predicted results by the finite element analysis and corresponding experiments showed enhanced prediction capability in springback analysis.

• Proceedings of the KWS Conference
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• 2005.11a
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• pp.189-191
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• 2005

Dissimilar joining of AI 6013-T4 alloys and austenite stainless steel was carried out using friction stir welding technique. Microstructures near the weld zone and mechanical properties of the joint have been investigated. Microstructures in the stainless steel side and AI alloy were depended on the thermo-mechanical condition which they received. TEM micrographs revealed that the interface region was composed of the mixed layers of elongated stainless steel and ultra-fine grained AI alloy and intermetallic compound layer which was identified as the $Al_{4}Fe$ with hexagonal close packed structure. Mechanical properties were lower than those of 6013 AI alloy base metal, because tool inserting location was deviated to AI alloy from the butt line, which resulted in the lack of the stirring.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.306-309
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• 2007

Recently, magnesium alloys have been widely used in automotive, aerospace and electronic industries with the advantages such as lightweightness, high specific strength and stiffness. However, magnesium alloy has quite low formability at room temperature due to its hexagonal close-packed crystal structure. Warm deep drawing is one of the forming technologies to improve the formability of magnesium alloy sheet and the lubrication condition is an important process parameter in that. In this study, the drawing tests of AZ31 alloy sheet at elevated temperature for various kinds of lubricant were carried out and the effects of lubrication conditions on drawbility were investigated.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2007.10a
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• pp.250-253
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• 2007

Since Mg alloy has many attractive advantages among the practically used metals, many researchers have been studied to develop useful process and material. The crystal structure of Magnesium was hexagonal close-packed, so its formability was poor at room temperature. But formability was improved in high temperature with increasing of slip planes, twins, dynamic recrystallization. In this study The formability of AZ31B magnesium sheet is estimated according to the variable temperatures, forming speed, thickness, blank holding force. The results of deep drawing experiences show that the formability is well at the range from 200 to $250^{\circ}C$, 20 to 60 mm/min forming speed and 2.5 to 3KN blank holding force.