• Tribology and Lubricants
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• v.11 no.5
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• pp.114-121
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• 1995

An ultrasonic technique using normal-incident compressional waves was used to evaluate the surface and subsurface damage in ceramics produced by Hertzian indentation. Damage was produced by a blunt indenter (tungsten carbide ball) in glass-ceramic, green glass and silicon nitride. The damage was classified into two types; (1) Hertzian cone crack, in green glass and fine grain silicon nitride, and (2) distributed subsurface micro fractures, without surface damage, produced in glass ceramic. The ultrasonic technique was successful in detecting cone craks. The measurement results with the Hertzian cone cracks indicated that cracks perpendicular to the surface could be detected by the normal-incident compressional waws. Also shown is the capability of normal-incident compressional waves in detection distributed micro-sized cracks size of subsurface microfractures.

• Journal of the Korean Ceramic Society
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• v.35 no.12
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• pp.1257-1265
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• 1998

Hertzian contact tests were used to investigate the evolution of fracturedamage in the coating layer as functions of contact load and coating thickness by studying crack patterns in porcelain on glass-infiltrated alumina bilayer system conceived to simulate the crown structure of a tooth. Cone cracks initiated at the coating top surface without delamination at interface and crack propagation to substrate. Preferentially the cracks made multi-cracks at the coating top surface rather than proceeding to interface. The cracks were highly stabilized with wide ranges between the loads to initiate first cracking and to cause final failure im-plying damage-tolerant capability. Finite element modelling was used to evaluate the stress distribution. Maximum tensile stress were responsible for the cracking at the coating layer and had a profound influence on the crack pattern and fracture damage in the layered structure materials.

• Journal of Powder Materials
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• v.5 no.1
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• pp.22-27
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• 1998

The effect of the $\alpha$/$\beta$ phase fraction on the mechanical properties in silicon nitrides was investigated in part 1. In part II, we describe the role of microstructure on the mechanical properties and contact damage of silicon nitrides with coarse/equiaxed and coarse/elongated microstructures. Grain sizes and shapes were controlled by starting powder. Hertzian indentation using spherical indenter was also used to investigate contact damage behavior. Cone cracks from the spherical indentation were suppressed when the silicon nitride contains coarse and elongated grains. Coarse and elongated grains played an important role of cone crack suppression. The size of quasi-plastic zone does not depend on grain size or shape but depends on the fraction of $\alpha$/$\beta$ phase. A quasi-plastic zone was consisting of microcracks by shear stress during indentation.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.4
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• pp.787-793
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• 2002

In this study, a bar impact test of low velocity was carried out to gain an insight into the damage mechanism and sequence induced in alumina plates(AD 85 and AD 90) under impact conditions. An experimental setup utilizing an instrumented long bar impact was devised, that can measure directly the impact force applied to the specimen and supply a compressive contact pressure to the specimen. During the bar impact testing, the influences of the contact pressure applied along the impact direction to the specimen on the fracture behavior were investigated. The measured impact force profiles explained well the damage behavior induced in alumina plates. The higher contact pressure to the specimen led to the less damage due to the suppression of radial cracks due to the increase in the apparent flexural stiffness of plate. It had produced the change of damage pattern developed in the specimen; from the radial cracks to the local contact stress dominant damage. It would contribute to the improvement of the ballistic property in ceramic plates. The observed results showed the following sequence in damage developed: The development of cone crack at impact region, the formation of radial cracks from the rear surface of plate depending on the plate thickness, the occurrence of crushing within the cone envelope and the fragmentation.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.10 no.4
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• pp.330-336
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• 2000

Effects of microstructure and indentation stress on fracture behavior of glass-infiltrated alumina composite for dental restorative application were investigated by the Hertzian and Vickers indentation method. Indentation stress-strain curve of glass-infiltrated alumina has showed the quasi-plastic behavior - deviation from linearity at high stress and the classical Hertzian cone crack, which could be confirmed the subsurface damage micrographs using bonded-interface specimen technique. The indentation stress-strain curves for the starting preforms are strongly dependent on porosity and microstructure of the preforms. On the other hand, the curves for the infiltrated composites are relatively insensitive to these factors. The failure of composite is originated at quasi-plastic deformation region. Damage and fracture behavior due to Hertzian stress field is theoretically examined, so that the indentation stress field plays a great role in material degradation. After Hertzian indentation annealing processing changes fracture behavior of alumina composite, so that stress field in material is healed through annealing.

• Journal of the Korean Ceramic Society
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• v.35 no.12
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• pp.1343-1350
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• 1998

A study is made of mechanical properties of unglazed matrix as a funtion of sintering temperature and crack patterns in layer structur pottery consisting of glaze and substrate and in matrix which is sintered at 120$0^{\circ}C$ and 130$0^{\circ}C$ respectively. The mechanical properties of matrix are increased due to density and vitrification to 130$0^{\circ}C$ The interface of glazed bilayer reveals the reactive intermediate layer. Herzian indentation testing is used to investigate the evolution of damage modes as a function of load. In the materials sintered at 120$0^{\circ}C$ quasi-plastic deformation is developed at the matrix and the cone-like cracks initiate at the glazing top surface and additionally upward-extending transverse cracks initiate at the internal in-just initiate at the glazing top surface which pass through the interface with increasing of indentation load. Finally the dominant damage mode shifts from substrate quasi-plasticity to coating fracture with increasing sintering temperature.

• Korean Journal of Materials Research
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• v.8 no.4
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• pp.293-298
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• 1998

The fracture behavior of $Si_3N_4N$, coated $Si_3N_4N$-BN composite was studied by the Hertzian indentation technique. New types of contact-induced cracks were found, and it was confirmed that these cracks have cone crack geometry. Contact damage was distributed in the substrate layer, which can absorb energy, as well as in the coating layer, so the propagation of initiated cracks in the coating layer were suppressed.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.4
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• pp.629-636
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• 2001

In order to investigate the possibility of impact punching in brittle materials, an experimental setup was developed. In the setup, a long bar as a punch was used to apply the impact load to the specimen plate and measure the applied impact force during the impact punching process. Impact punching tests with various shape of punches were performed in soda-lime glass and silicon wafer under a different level of contact pressure. The damage appearance after the impact punching was examined according to the applied contact pressure. The minimum contact pressure required for a complete punching in glass specimens without development of radial cracks around the punched hole was sought at each condition. The minimum contact pressure increased with increasing the thickness of specimens and decreasing the end radius of punches. The profile of impact forces was measured during the impact punching experiment, and it could explain well the behavior of the punching process in brittle material plates. The measured impact force increased with increasing the contact pressure applied to the plates.

• Journal of the Korean Ceramic Society
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• v.35 no.1
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• pp.48-54
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• 1998

The effect of coating thickness on the contact fracture was studied, in Si3N4 coated Si3N4-BN system When the elastic/plastic mismatch is relatively large betwen two layers in bilayer certain critical coating thickness was required to prevent cone crack initiation and this critical thickness was decreased by de-creasing the elastic/plastic mismatch,. In addition the required critical thickness should be increased when higher loads apply. In conclusion an appropriate coating thickness should be designed by elastic/plastic mismatch between two layers and environment (applied load) to prevent the coating fracture